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    FLUOROCARBON-GRAFTED POLYSILOXANES
    3.
    发明申请
    FLUOROCARBON-GRAFTED POLYSILOXANES 审中-公开
    氟聚合多晶硅

    公开(公告)号：WO2006083818A8

    公开(公告)日：2007-04-26

    申请号：PCT/US2006003330

    申请日：2006-01-31

    Applicant: DU PONT ,  PABON MARTIAL JEAN-JACQUES ,  SEVERAC ROMAIN ,  PUCHOIS EMMANUEL ABEL ,  PERDON MATTHIEU

    Inventor： PABON MARTIAL JEAN-JACQUES ,  SEVERAC ROMAIN ,  PUCHOIS EMMANUEL ABEL ,  PERDON MATTHIEU

    IPC: C08K3/00 ,  B32B17/10 ,  C08K3/22 ,  C08K7/00 ,  C08L23/08 ,  C08L29/14 ,  C08L67/00

    CPC classification number: C03C17/30 ,  C03C2217/75 ,  C03C2217/76 ,  C04B41/4961 ,  C04B2111/203 ,  C04B2111/27 ,  C08G77/392 ,  C08L83/08 ,  C09D183/08 ,  D06M15/65 ,  D06M15/657 ,  D06M2200/11 ,  D06M2200/12 ,  Y10T428/31663 ,  C04B41/00 ,  C08L2666/02

    Abstract: A composition useful to provide oil repellency, water repellency, and stain resistance to substrates comprising a polymer prepared by contacting a polytluoroalkyl sulfonyl halide with a compound of Formula II: (E-(O) q ) 3 Si-O-(Si(R 2 ) 2 -O) m [Si(R 3 -NHR 4 )(R 2 )O] n -Si-((O) q -E) 3, Formula III: HR 4 N-R 3 -Si(R 2 ) 2 -O-[Si(R 2 ) 2 -O] m [Si(R 3 -NHR 4 )(R 2 )O] n -Si-(R 2 ) 2 -R 3 -NHR 4 or Formula IV: HR 4 N-R 3 -Si(R 2 ) 2 -O-[Si(R 2 ) 2 -O] m Si-((O) q -E) 3 , wherein each R 2 is independently a C 1 to C 8 alkyl, each R 3 is independently a divalent group containing carbon, oxygen, and optionally at least one of nitrogen oxygen and sulfur, each R 4 is independently H or C 1 to C 8 alkyl, each E is independently a C 1 to C 8 branched or linear alkyl, each q is independently zero or 1, m is a positive integer, and n is independently zero or a positive integer, such that n/(m+n) is zero or a positive fraction having a value up to about 0.7, and the polymer viscosity is less than or equal to 10000 mPa.s under a shear rate of 0.1 s -1 at a temperature of 20° C.

    Abstract translation: 用于提供拒油性，拒水性和对基材的耐污性的组合物，其包含通过使聚氟烷基磺酰卤与式II化合物接触而制备的聚合物：（E-（O） > 3 Si-O-（Si（R 2）2 -O）m）[Si（R 3） -NHR 4 ）（R 2 ）O] 名词 -Si - （（O） q -E）3，式III：HR 4 NR 3 -Si（R 2） 2 -O - [Si（R 2）2 -O] m [Si（R 3） SUP> -NHR 4 ）（R 2 ）O] 名词 -Si-（R 2 ） 2 3 -NHR 4或式IV：HR 4 NR 3 -Si （R 2 ） 2 -O- [硅（R 2 ） 2 -O] 米 Si - （（O）q -E）3，其中每个R 2独立地是C 1 - / SUB> C 8烷基，每个R 3独立地是含有碳，氧和任选的至少一个氮的二价基团 氧和硫，每个R 4独立地为H或C 1至C 8烷基，每个E独立地为C 1〜 每个q独立地为0或1，m为正整数，n为独立为0或正整数，使得n /（m + n ）为零或具有高达约0.7的值的正级分，并且在20℃的温度下，在0.1s -1的剪切速率下聚合物粘度小于或等于10000mPa.s C。

    FLUOROBETAINE COPOLYMER AND FIRE FIGHTING FOAM CONCENTRATES THEREFROM
    4.
    发明申请
    FLUOROBETAINE COPOLYMER AND FIRE FIGHTING FOAM CONCENTRATES THEREFROM 审中-公开
    氟代苯乙烯共聚物和消泡剂的消泡浓度

    公开(公告)号：WO2008115457A3

    公开(公告)日：2008-11-06

    申请号：PCT/US2008003477

    申请日：2008-03-14

    Applicant: DU PONT ,  SEVERAC ROMAIN ,  PABON MARTIAL JEAN-JACQUES ,  DEGUERRY ISABELLE ,  GAMBLIN GUILLAUME

    Inventor： SEVERAC ROMAIN ,  PABON MARTIAL JEAN-JACQUES ,  DEGUERRY ISABELLE ,  GAMBLIN GUILLAUME

    IPC: C08F220/24 ,  C08F220/38

    CPC classification number: C08F214/18 ,  C08F214/20 ,  C08F220/24 ,  C08F220/38

    Abstract: It has been discovered by in present invention that, compared with a fluorosurfactant having only one betaine group per molecule, a fluorosurfactant having a plurality of betaine groups per molecule is superior in its ability to undergo electrostatic interaction with other components of a fire fighting composition thereby improving the performance of the fire fighting composition. Previously known fluorosurfactants comprise only one betaine group per molecule. In contrast, the present invention provides for a fluorobetaine copolymer containing a plurality of betaine groups.

    Abstract translation: 在本发明中已经发现，与每分子仅具有一个甜菜碱基团的含氟表面活性剂相比，每分子具有多个甜菜碱基团的含氟表面活性剂的耐受性与其它消防组合物的其它组分的静电相互作用相比是优异的 提高消防组合的表现。 以前已知的含氟表面活性剂每分子仅包含一个甜菜碱基团。 相反，本发明提供含有多个甜菜碱基团的氟代甜菜碱共聚物。

    FLUOROCARBON-GRAFTED POLYSILOXANES
    6.
    发明申请
    FLUOROCARBON-GRAFTED POLYSILOXANES 审中-公开
    氟聚合多晶硅

    公开(公告)号：WO2006083818A1

    公开(公告)日：2006-08-10

    申请号：PCT/US2006/003330

    申请日：2006-01-31

    Applicant: E.I. DUPONT DE NEMOURS AND COMPANY ,  PABON, Martial, Jean-Jacques ,  SEVERAC, Romain ,  PUCHOIS, Emmanuel, Abel ,  PERDON, Matthieu

    Inventor： PABON, Martial, Jean-Jacques ,  SEVERAC, Romain ,  PUCHOIS, Emmanuel, Abel ,  PERDON, Matthieu

    IPC: C08K3/00 ,  C08K3/22 ,  C08K7/00 ,  C08L23/08 ,  C08L29/14 ,  C08L67/00 ,  B32B17/10

    CPC classification number: C03C17/30 ,  C03C2217/75 ,  C03C2217/76 ,  C04B41/4961 ,  C04B2111/203 ,  C04B2111/27 ,  C08G77/392 ,  C08L83/08 ,  C09D183/08 ,  D06M15/65 ,  D06M15/657 ,  D06M2200/11 ,  D06M2200/12 ,  Y10T428/31663 ,  C04B41/00 ,  C08L2666/02

    Abstract: A composition useful to provide oil repellency, water repellency, and stain resistance to substrates comprising a polymer prepared by contacting a polytluoroalkyl sulfonyl halide with a compound of Formula II: (E-(O) q ) 3 Si-O-(Si(R 2 ) 2 -O) m [Si(R 3 -NHR 4 )(R 2 )O] n -Si-((O) q -E) 3, Formula III: HR 4 N-R 3 -Si(R 2 ) 2 -O-[Si(R 2 ) 2 -O] m [Si(R 3 -NHR 4 )(R 2 )O] n -Si-(R 2 ) 2 -R 3 -NHR 4 or Formula IV: HR 4 N-R 3 -Si(R 2 ) 2 -O-[Si(R 2 ) 2 -O] m Si-((O) q -E) 3 , wherein each R 2 is independently a C 1 to C 8 alkyl, each R 3 is independently a divalent group containing carbon, oxygen, and optionally at least one of nitrogen oxygen and sulfur, each R 4 is independently H or C 1 to C 8 alkyl, each E is independently a C 1 to C 8 branched or linear alkyl, each q is independently zero or 1, m is a positive integer, and n is independently zero or a positive integer, such that n/(m+n) is zero or a positive fraction having a value up to about 0.7, and the polymer viscosity is less than or equal to 10000 mPa.s under a shear rate of 0.1 s -1 at a temperature of 20° C.

    Abstract translation: 用于提供拒油性，拒水性和耐污染性的组合物，其包含通过使聚氟烷基磺酰卤与式II化合物接触而制备的聚合物：（E-（O） > 3 Si-O-（Si（R 2）2 -O）m）[Si（R 3） -NHR 4 ）（R 2 ）O] 名词 -Si - （（O） q -E）3，式III：HR 4 NR 3 -Si（R 2）2 2 O [Si（R 2）2 -O] m [Si（R 3） SUP> -NHR 4 ）（R 2 ）O] 名词 -Si-（R 2 ） 2 3 -NHR 4或式IV：HR 4 NR 3 -Si （R 2 ） 2 -O- [硅（R 2 ） 2 -O] 米 Si - （（O）q -E）3，其中每个R 2独立地是C 1 - / SUB> C 8烷基，每个R 3独立地是含有碳，氧和任选的至少一个氮的二价基团 氧和硫，每个R 4独立地为H或C 1至C 8烷基，每个E独立地为C 1〜 分支或直链烷基，各q独立地为0或1，m为正整数，n为独立为0或正整数，使得n /（m + n ）为零或具有高达约0.7的值的正级分，并且在20℃的温度下，在0.1s -1的剪切速率下，聚合物粘度小于或等于10000mPa.s C。

    AMPHOTERIC FLUOROCHEMICALS FOR PAPER
    7.
    发明申请
    AMPHOTERIC FLUOROCHEMICALS FOR PAPER 审中-公开
    用于纸张的AMPHOTERIC FLUOROCHEMICALS

    公开(公告)号：WO2009009280A1

    公开(公告)日：2009-01-15

    申请号：PCT/US2008/067828

    申请日：2008-06-23

    Applicant: E. I. DU PONT DE NEMOURS AND COMPANY ,  HUANG, Hsu-nan ,  PABON, Martial, Jean-Jacques ,  SEVERAC, Romain ,  HEUZE, Lamia

    Inventor： HUANG, Hsu-nan ,  PABON, Martial, Jean-Jacques ,  SEVERAC, Romain ,  HEUZE, Lamia

    IPC: C08F220/24 ,  C08F220/68 ,  C08L33/16 ,  C09D133/16 ,  D06M15/277

    CPC classification number: C09D133/18 ,  C08F220/06 ,  C08F220/24 ,  C08F220/34 ,  D21H17/11 ,  D21H17/36 ,  D21H17/37 ,  D21H21/14 ,  D21H21/16 ,  Y10T428/31895 ,  Y10T442/2279 ,  Y10T442/2287

    Abstract: A method of imparting oil repellency to flexible, fibrous, nonwoven substrates comprising contacting the substrate with a composition prepared from polymerization of monomers in the following percentages by weight: (a) from about 60% to about 90% of a monomer of Formula 1 or a mixture thereof: R f -Q-CO-CR=CH 2 Formula 1 wherein: R f is a straight- or branched-chain perfluoroalkyl group of 2 to about 20 carbon atoms, R is H or CH 3 , Q is -(C n H 2n O) p SO 2 NR 1 (C n H 2n O) y , wherein the -(C n H 2n ) is bonded to R f , and R 1 is H or C 1 -C 20 alkyl; (b) from about 10% to about 25% of a monomer of Formula 2 or a mixture thereof: CH 2 =C(R)COZ(CH 2 )q(CHR) r NR 2 R 3 Formula 2 wherein R 2 and R 3 are each independently C 1 - C 4 alkyl, hydroxyethyl, or benzyl or R 2 and R 3 together with the nitrogen atom form a morpholine, pyrrolidine, or piperidine ring, and Z is -O- or -NR 4 - wherein R 4 is H or C 1 - C 4 alkyl; and (c) from about 1% to about 15% of a monomer of Formula 3 or a mixture thereof: CH 2 =CR(R 5 ) e -COOH Formula 3 wherein R 5 is CO(CH 2 ) 5 , CO-O-(CH 2 ) 2, C 6 H 4 CHR, or CONRR 6 , and R 6 is C 6 H 4 OCH 2 , (CH 2 ) d , or C(CH 3 ) 2 CH 2 .

    Abstract translation: 包括使柔性纤维状非织造基材赋予拒油性的方法，包括使底物与按单体聚合制备的组合物接触，重量百分比如下：（a）约60％至约90％的式1单体或 其混合物：Rf -Q-CO-CR = CH 2式1其中：Rf为2-约20个碳原子的直链或支链全氟烷基，R为H或CH3，Q为 - （CnH2nO）pSO2NR1（ C n H 2n O）y，其中 - （C n H 2n）键合到R f，并且R 1是H或C 1 -C 20烷基; （b）约10％至约25％的式2单体或其混合物：CH 2 = C（R）COZ（CH 2）q（CHR）r NRR2R 3式2其中R 2和R 3各自独立地为C 1 -C 4烷基 ，羟乙基或苄基或R2和R3与氮原子一起形成吗啉，吡咯烷或哌啶环，Z是-O-或-NR4-，其中R4是H或C1-C4烷基; 和（c）约1％至约15％的式3单体或其混合物：CH2 = CR（R5）e-COOH式3其中R5为CO（CH2）5，CO-O-（CH2） 2，C6H4CHR或CONRR6，R6是C6H4OCH2，（CH2）d或C（CH3）2CH2。

    TRIAZOLE-CONTAINING FLUOROCARBON-GRAFTED POLYSILOXANES
    8.
    发明申请
    TRIAZOLE-CONTAINING FLUOROCARBON-GRAFTED POLYSILOXANES 审中-公开
    含有三氟甲烷的氟代聚硅氧烷

    公开(公告)号：WO2007075285A1

    公开(公告)日：2007-07-05

    申请号：PCT/US2006/046630

    申请日：2006-12-06

    Applicant: E. I. DU PONT DE NEMOURS AND COMPANY ,  ACOSTA, Erick, Jose ,  HERZOG, Axel, Hans-Joachim ,  PABON, Martial, Jean-Jacques

    Inventor： ACOSTA, Erick, Jose ,  HERZOG, Axel, Hans-Joachim ,  PABON, Martial, Jean-Jacques

    IPC: C08G77/388 ,  C08G77/26 ,  C08G77/24

    CPC classification number: C08G77/26 ,  C08G77/24 ,  C08G77/388 ,  Y10T428/31663

    Abstract: A polymer for imparting repellency and stain resistance to substrates is disclosed of Formula (1): (W) a (R 2 ) b -Si(R 1 ) 2 -O-[Si(R 1 ) 2 -O] n -[Si(W) c (R 1 ) d (R 2 ) e -O] m -Si(R 1 ) 2 -(W) f (R 2 ) g wherein: a, b, c, d, e, f and g are each independently 0 or 1, provided that (a + b) is 1, (f + g) is 1, and (c + d + e) is 2, each R 1 is divalently a C 1 to C 8 alkyl, each R 2 is independently H or C 1 to C 8 alkyl, optionally containing oxygen, nitrogen, or sulfur, or a combination thereof, n = 0 to 500, m = 1 to 100, each W is independently (R f -X-A-X) p -Y wherein: R f is a straight or branched perfluoroalkyl group having from about 2 to about 20 carbon atoms, or a mixture thereof, which is optionally interrupted by at least one oxygen atom, each X is independently an organic divalent linking group having from about 1 to about 20 carbon atoms, optionally containing oxygen, nitrogen, or sulfur, or a combination thereof, A is a 1, 2, 3-triazole, p = 0 to 2, and Y is O, OR, N, NR or N(R) 2 wherein R is H or C 1 to C 20 alkyl, optionally containing oxygen, nitrogen, or sulfur, or a combination thereof.

    Abstract translation: 式（1）公开了一种用于赋予对基材的排斥性和耐污性的聚合物：（W）a（R 2）b -Si （R 1 ） 2 -O- [硅（R 1 ） 2 -O] ñ 个 - [Si（W） C （R 1 ）ð（R 2 ）电子 -O] 米 -Si（R 1 ） 2 - （W）˚F 其中：a，b，c，d，e，f和g各自独立地为0或1，条件是（a + b）为1 ，（f + g）为1，（c + d + e）为2，每个R 1为C 2〜C 8， 每个R 2独立地为H或C 1至C 8烷基，任选地含有氧，氮或硫，或 其组合，n = 0至500，m = 1至100，每个W独立地为（R x -X-X））其中：R f为 / SUB>是具有约2至约20个碳原子的直链或支链全氟烷基或其混合物，其任选地被 至少一个氧原子，每个X独立地为具有约1至约20个碳原子的有机二价连接基团，任选地含有氧，氮或硫，或其组合，A是1,2,3,4-三唑，p = 0至2，Y为O，OR，N，NR或N（R）2，其中R为H或C 1至C 20， 任选地含有氧，氮或硫的烷基，或其组合。

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