公开(公告)号：WO2015065906A3

公开(公告)日：2015-07-16

申请号：PCT/US2014062416

申请日：2014-10-27

Applicant: CHEVRON PHILLIPS CHEMICAL CO

Inventor： MATSON MICHAEL S ,  SOULES DAVID A

IPC: C08G79/04 ,  C08J5/18 ,  C08K3/00 ,  C08K5/00 ,  C08L81/00 ,  C08L81/02

CPC classification number: C08G75/14 ,  C08G79/04 ,  C08L81/00 ,  C08L81/02

Abstract: A process comprising contacting a reaction product composition comprising a poly(arylene sulfide) composition and a polar organic compound, wherein the polar organic compound comprises greater than or equal to about 1 wt.% thiophenol, with a C4-C30 α,β-unsaturated ketone, a C4-C30 α,β-unsaturated ester, a C4-C30 α,β-unsaturated amide, or any combination thereof, wherein after the contacting, the polar organic compound comprises less than about 1 wt.% thiophenol. A process comprising contacting a composition comprising a polar organic compound and greater than or equal to about 1 wt.% thiophenol with a C4-C30 α,β-unsaturated ketone, a C4-C30 α,β-unsaturated ester, a C4-C30 α,β-unsaturated amide, or any combination thereof, to form a composition comprising the polar organic compound and less than about 1 wt.% thiophenol.

Abstract translation: 一种方法，包括使包含聚（亚芳基硫醚）组合物和极性有机化合物的反应产物组合物接触，其中极性有机化合物包含大于或等于约1重量％的苯硫酚，与C 4 -C 30α，β-不饱和 酮，C 4 -C 30α，β-不饱和酯，C 4 -C 30α，β-不饱和酰胺或其任何组合，其中接触后，极性有机化合物包含小于约1重量％的苯硫酚。 一种方法，包括将包含极性有机化合物和大于或等于约1重量％的苯硫酚的组合物与C4-C30α，β-不饱和酮，C4-C30α，β-不饱和酯，C4-C30 α，β-不饱和酰胺或其任何组合，以形成包含极性有机化合物和小于约1重量％的苯硫酚的组合物。

公开(公告)号：WO2004085514A3

公开(公告)日：2004-11-25

申请号：PCT/US2004008601

申请日：2004-03-22

Applicant: CHEVRON PHILLIPS CHEMICAL CO

Inventor： VIDAURRI FERNANDO C ,  SOUTH AUBREY JR ,  SOULES DAVID A ,  FODOR JEFFREY S

IPC: C08L81/02 ,  C08G75/00

CPC classification number: C08L81/02

Abstract: Disclosed herein is a process for preparing cured arylene sulfide polymers. A first curing vessel comprising a first agitator is used to cure a poly(arylene sulfide) compacted powder. The curing proceeds until the compacted powder reaches a melt flow rate within a target range. When the melt flow rate of the compacted powder first reaches the target range, the power consumption of the first agitator is determined. A second curing vessel comprising a second agitator is charged with a second quantity of the compacted poly(arylene sulfide) powder. The second quantity of compacted powder is cured in the second vessel until the power consumption of the second agitator reaches the value at which the melt flow rate in the first curing vessel first reached the target range.

Abstract translation: 本文公开了一种制备固化亚芳基硫醚聚合物的方法。 包含第一搅拌器的第一固化容器用于固化聚（亚芳基硫醚）压实粉末。 进行固化直至压制粉末达到目标范围内的熔体流动速率。 当压实粉末的熔体流动速率首先达到目标范围时，确定第一搅拌器的功率消耗。 包含第二搅拌器的第二固化容器装有第二数量的压实聚亚芳基硫醚粉末。 第二量的压实粉末在第二容器中固化，直到第二搅拌器的功率消耗达到第一固化容器中的熔体流动速率首次达到目标范围的值。