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    METHOD OF MANUFACTURING CYCLOPHOSPHAZENE DERIVATIVES
    2.
    发明申请
    METHOD OF MANUFACTURING CYCLOPHOSPHAZENE DERIVATIVES 审中-公开
    制备环磷酰胺衍生物的方法

    公开(公告)号：WO2014195299A1

    公开(公告)日：2014-12-11

    申请号：PCT/EP2014/061462

    申请日：2014-06-03

    Applicant: SOLVAY SPECIALTY POLYMERS ITALY S.P.A.

    Inventor： VALSECCHI, Roberto ,  PICOZZI, Rosaldo ,  GUARDA, Pier Antonio

    IPC: C07F9/6593 ,  C07F9/6581 ,  C08G79/02 ,  G11B5/725

    CPC classification number: C07F9/65815 ,  C07F9/65812 ,  C07F9/65817 ,  C08G65/007 ,  C08G65/3356 ,  C08G65/337 ,  C10M105/74 ,  G11B5/725

    Abstract: A method of manufacturing cyclophosphazenes PFPE derivatives to be used in the lubrication of magnetic recording media is herein provided. The method comprises: a) a (per)fluoropolyether (PFPE) polyol [PFPE (P pol )] comprising a fluoropolyoxyalkylene chain (R f ) having two chain ends, each chain end comprising at least one hydroxy group, and b) the corresponding alkoxide of perfluoropolyether (P pol ) [PFPE (P alk )] wherein the equivalent concentration of PFPE (P alk ) in PFPE (P pol ) is lower than 30%, preferably ranging from 5% to 15%; 2) contacting mixture (M) with a perhalocyclophosphazene (CP halo ) to provide a mixture (M1) containing an equivalent ratio of PFPE (P alk )/(CP halo ) of at least 1; 3) allowing mixture (M1) to react until complete disappearance of P-Cl groups to provide a mixture (M2); 4) submitting mixture (M2) to hydrolysis to provide a mixture (M3); 5) optionally removing (P pol ) from mixture (M3) to provide a mixture (M4). A method of purifying mixture (M4) is also herein provided.

    Abstract translation: 本文提供了制造用于润滑磁记录介质的环磷腈PFPE衍生物的方法。 该方法包括：a）包含具有两个链端的氟聚氧化烯链（Rf）的（全）氟聚醚（PFPE）多元醇[PFPE（Ppol）]，每个链端包含至少一个羟基，和b）相应的醇盐 全氟聚醚（Ppol）[PFPE（Palk）]，其中PFPE（Ppol）中PFPE（Palk）的当量浓度低于30％，优选5％至15％; 2）使混合物（M）与全卤代环丙腈（CPhalo）接触，以提供含有至少1的PFPE（Palk）/（CPalO）的当量比的混合物（M1） 3）允许混合物（M1）反应直到P-Cl基团完全消失以提供混合物（M2）; 4）将混合物（M2）进行水解以提供混合物（M3）; 5）任选地从混合物（M3）中除去（Ppol）以提供混合物（M4）。 还提供了一种纯化混合物（M4）的方法。

    LUBRICATION METHOD WITH ALKOXYLATED PERFLUOROPOLYETHER
    5.
    发明申请
    LUBRICATION METHOD WITH ALKOXYLATED PERFLUOROPOLYETHER 审中-公开
    使用烷氧基全氟丙基醚的润滑方法

    公开(公告)号：WO2016020232A1

    公开(公告)日：2016-02-11

    申请号：PCT/EP2015/067354

    申请日：2015-07-29

    Applicant: SOLVAY SPECIALTY POLYMERS ITALY S.P.A.

    Inventor： MACCONE, Patrizia ,  GUARDA, Pier Antonio ,  BOCCALETTI, Giovanni

    IPC: C10M147/04

    CPC classification number: C10M147/04 ,  C10M2213/04 ,  C10M2213/0626 ,  C10N2220/021 ,  C10N2230/02 ,  C10N2230/06 ,  C10N2230/10 ,  C10N2250/10 ,  C10N2270/00 ,  C10M2209/103 ,  C10M2209/108

    Abstract: A lubrication method comprising applying to a surface to be lubricated a polymer comprising a partially or fully fluorinated, straight or branched, polyoxyalkylene chain (chain R f ) having two chain ends, wherein one or both chain end(s) bear(s) a hydroxy- or alkoxy-terminated polyoxyalkylene chain free from fluorine atoms (chain R a ), said chain comprising from 4 to 50 fluorine-free oxyalkylene units, said units being the same or different from one another and being selected from -CH 2 CH 2 O- and -CH 2 CH(J)O-, wherein J is independently straight or branched alkyl or aryl, with the proviso that, if both chain ends bear a hydroxy-terminated chain Ra comprising only -CH 2 CH 2 O- units, chain Rf does not consist only of -CF 2 CF 2 O-units. Lubricant compositions containing the polymer and methods for preparing the polymer are also herein disclosed.

    Abstract translation: 一种润滑方法，其包括将待润滑的表面施加到包含部分或完全氟化的具有两个链端的直链或全氟化的直链或支链的聚氧化烯链（链Rf）的聚合物，其中一个或两个链端承载羟基 - 或不含氟原子的烷氧基封端的聚氧化烯链（链Ra），所述链包含4至50个无氟氧化烯单元，所述单元彼此相同或不同，并且选自-CH 2 CH 2 O-和-CH 2 CH（ J）O-，其中J独立地是直链或支链的烷基或芳基，条件是如果两个链端都具有仅包含-CH 2 CH 2 O-单元的羟基封端的链Ra，则链Rf不仅由-CF 2 CF 2 O单元 。 含有聚合物的润滑组合物和制备聚合物的方法也在此公开。

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