公开(公告)号：WO01039856A1

公开(公告)日：2001-06-07

申请号：PCT/EP2000/011468

申请日：2000-11-17

IPC: B29B13/00 ,  B01D1/04 ,  B01D1/06 ,  B01D3/00 ,  B01D19/00 ,  B29C47/76 ,  B29K25/00 ,  C08F6/00 ,  C08F6/10

CPC classification number: B01D1/06 ,  B01D1/04 ,  B01D3/008 ,  B01D19/0021 ,  B29C47/0019 ,  B29C47/003 ,  B29C47/76 ,  C08F6/003 ,  Y10S159/10 ,  Y10S159/15

Abstract: The invention relates to a strand evaporator comprising a degassing vessel (6), a product entry (11), a product distributor (17), a product discharge (13), and a vapor discharge (12). The invention is characterized in that the product distributor (17) is configured as a manifold distributor that is provided with at least one distributing pipe (1) and with a multitude of parallelly arranged nozzle pipes (2), which have a multitude of openings (15) in the pipe wall. The invention is also characterized in that the nozzle tubes (2) are preferably arranged one above the other in a number of planes and such that they are laterally offset.

Abstract translation: 它将与一个脱气容器（6），产物入口（11），一个产品分配器（17），一个产品排出（13）和一个Brüdenaustrag（12）一个链蒸发器为管分配器来描述，其特征在于，在该产品分发器（17）与至少一个 分配器管（1）并具有多个（2），其具有在管道壁的多个开口（15）平行排列的喷嘴管的形成和布置成使得管芯管（2）优选在几个平面一个在另一个之上并彼此横向偏移。

公开(公告)号：WO2005012817A2

公开(公告)日：2005-02-10

申请号：PCT/US2004/024122

申请日：2004-07-27

Applicant: FINA TECHNOLOGY, INC. ,  REIMERS, Jay

Inventor： REIMERS, Jay

IPC: F28C

CPC classification number: B01D1/06 ,  B01D1/0011 ,  C08F6/001 ,  Y10S159/10 ,  Y10S159/15 ,  Y10S159/32

Abstract: Disclosed is a process for devolatilizing a polymer comprising the polymer through a devolatizer comprising a plate heat exchanger wherein the plate heat exchanger are heated by a plurality of heating tubes and wherein the heating tube comprises a return tube nested inside of a supply tube. The use of the disclosed invention allows for a comparatively small heat profile across heating plates as compared to prior art plate heat exchangers.

Abstract translation: 公开了一种通过包含板式换热器的脱挥器将包含聚合物的聚合物脱挥发分的方法，其中板式热交换器被多个加热管加热，并且其中加热管包括嵌套在供应管内的回流管。 与现有技术的板式换热器相比，使用所公开的发明允许加热板上的相对较小的热分布。

公开(公告)号：WO1998029460A1

公开(公告)日：1998-07-09

申请号：PCT/JP1997004789

申请日：1997-12-24

Applicant: CHISSO CORPORATION ,  MATSUDA, Etsuro ,  ITO, Yuichi ,  KURAZONO, Toshinobu

Inventor： CHISSO CORPORATION

IPC: C08F06/24

CPC classification number: C08F6/003 ,  Y10S159/10 ,  Y10S203/09 ,  C08L27/06

Abstract: A method and an apparatus for removing residual monomers from a slurry containing polyvinyl chloride while preventing degradation of polyvinyl chloride and the drop of its quality. The apparatus comprises a cylindrical column main body (46), a plurality of porous plates (32 to 38) disposed in a vertical direction inside the column main body, a plurality of chambers defined on the porous plates by using these porous plates as their bottom surfaces, slurry introduction portions (19 to 24) provided to at least two of these chambers, flow-down portions (13 to 18) disposed between the porous plates so as to allow the slurry to sequentially flow down from the porous plates of the upper chambers to the porous plates of the lower chambers, a steam inlet (10) disposed at the bottom of the column main body, a vent (11) disposed at the top of the column main body, a slurry discharge port (12) disposed in a chamber below a chamber having a slurry inlet, and hot water injection means (25 to 31) disposed immediately below the porous plates in such a manner as to face at least the lower surfaces of the porous plates, wherein a slurry introduction pipe (48) is connected to the slurry inlet (50) through an on/off valve (49) and the inner diameter of the slurry introduction pipe (48) is progressively expanded towards the slurry inlet (50) up to at least 1.2 times.

Abstract translation: 一种用于从含有聚氯乙烯的浆料中除去残留单体的方法和装置，同时防止聚氯乙烯的降解及其质量下降。 该装置包括圆柱形主体（46），在柱主体内沿垂直方向设置的多个多孔板（32至38），通过使用这些多孔板作为底部在多孔板上限定多个室 设置在这些室中的至少两个的表面，浆料引入部分（19至24），设置在多孔板之间的下降部分（13至18），以使浆料从上部的多孔板顺序地向下流动 室到下室的多孔板，设置在塔主体底部的蒸汽入口（10），设置在塔主体顶部的排气口（11），设置在塔主体的顶部的排出口 在具有浆料入口的腔室下方的腔室和设置在多孔板正下方的热水喷射装置（25至31），以至少面向多孔板的下表面，其中浆料引入管（48至48） ）连接到s 毛刺入口（50）通过开/关阀（49），并且浆料引入管（48）的内径朝向浆料入口（50）逐渐膨胀至至少1.2倍。

公开(公告)号：WO2004018522A3

公开(公告)日：2005-03-03

申请号：PCT/US0324954

申请日：2003-08-07

Applicant: FINA TECHNOLOGY

Inventor： BERTI DOUGLAS A ,  SOSA JOSE ,  GRIFFITH ARON T

IPC: B01D1/00 ,  B01D3/06 ,  B01D5/00 ,  C08F20060101 ,  C08F2/00 ,  C08F6/00 ,  C08F6/04 ,  C08F6/10 ,  C08J11/02

CPC classification number: B01D3/06 ,  C08F6/005 ,  Y10S159/10

Abstract: The present invention provides an apparatus (100) and method of reducing volatiles in a mass processable polymer. The apparatus comprises a multi-chambered devolatilizer (160) having first and second collectors (220, 225) contained therein. In one embodiment, the invention provides a method that includes passing the mass processable polymer stream from a polymerization process to a first devolatilizer (130). The method continues by passing the polymer stream from the first devolatilizer to the multi-chambered devolatilizer. The apparatus and method allows for the production of a polymer having less than 100 ppm of volatiles.

Abstract translation: 本发明提供减少可加脂聚合物中的挥发物的装置（100）和方法。 该设备包括具有容纳在其中的第一和第二收集器（220,225）的多室脱挥器（160）。 在一个实施方案中，本发明提供了一种方法，其包括将可聚合聚合物流从聚合过程传递到第一脱挥发物（130）。 该方法通过使聚合物流从第一脱挥发物流入多室脱挥发剂而继续。 该装置和方法允许生产具有小于100ppm挥发物的聚合物。

公开(公告)号：WO99067002A1

公开(公告)日：1999-12-29

申请号：PCT/EP1999/004023

申请日：1999-06-11

IPC: B01D1/22 ,  B01D3/06 ,  C08G64/40

CPC classification number: B01D3/06 ,  C08G64/406 ,  Y10S159/08 ,  Y10S159/10

Abstract: The invention relates to the evaporation of a viscous polymer solution having at least 30 wt.%, preferably at least 50 to 70 wt.%, solvents and monomers. According to the inventive method, the polymer solution to be evaporated is guided through a heated helical tube (5) as a film flow with a vapor exit velocity ranging from 200 to 300 m/s and flows into a heated separator (6) afterwards. Heating of the helical tube (5) and of the separator (6) is realized in such a way that the temperatures of the heating means in the helical tube (5) and in the separator (6) are above the softening point of the polymer. An additional important method criterion is characterized in that the two-phase mixture which is made of a polymer melt, solvent vapors, and monomer vapors and which is formed in the helical tube (5) is relieved to a pressure ranging from 10 mb to 800 mbabs in the heated vapor separator (6).

Abstract translation: 该方法涉及含有至少30重量％，优选至少50至70种重量％的溶剂和单体的粘性聚合物溶液的蒸发。 聚合物溶液是出通过加热的螺旋（5）M被蒸发，与200〜300秒的蒸气出口速度的薄膜流/并然后流入加热的分离器（6）。 螺旋管（5）和所述分离器（6）的加热器被设计成使水的温度在上述螺旋管（5）和所述分离器（6）位于所述聚合物的软化点以上。 另一个重要的程序的标准是，在上述螺旋管（5）在10毫巴范围内的压力特形成的聚合物熔体和溶剂和单体蒸气的两相混合物进入加热的蒸汽分离器（6），以800个mbarabs。

公开(公告)号：WO2005012817A3

公开(公告)日：2007-05-31

申请号：PCT/US2004024122

申请日：2004-07-27

Applicant: FINA TECHNOLOGY ,  REIMERS JAY

Inventor： REIMERS JAY

IPC: B01D1/06 ,  B01D1/00 ,  C08F6/00

CPC classification number: B01D1/06 ,  B01D1/0011 ,  C08F6/001 ,  Y10S159/10 ,  Y10S159/15 ,  Y10S159/32

Abstract: Disclosed is a process for devolatilizing a polymer comprising the polymer through a devolatizer comprising a plate heat exchanger wherein the plate heat exchanger are heated by a plurality of heating tubes and wherein the heating tube comprises a return tube nested inside of a supply tube. The use of the disclosed invention allows for a comparatively small heat profile across heating plates as compared to prior art plate heat exchangers.

Abstract translation: 公开了一种通过包含板式换热器的脱挥器将包含聚合物的聚合物脱挥发分的方法，其中板式热交换器被多个加热管加热，并且其中加热管包括嵌套在供应管内的回流管。 与现有技术的板式换热器相比，使用所公开的发明允许加热板上的相对较小的热分布。

公开(公告)号：WO02051606A1

公开(公告)日：2002-07-04

申请号：PCT/EP2001/014818

申请日：2001-12-14

IPC: B01D1/00 ,  B01D3/06 ,  B01D19/00 ,  B01J4/00 ,  B01J19/24 ,  B29B13/00 ,  B01D3/00 ,  B01J19/32

CPC classification number: B29B13/00 ,  B01D3/06 ,  B01D19/0047 ,  B01J4/001 ,  B01J19/24 ,  B29B2013/005 ,  B29K2069/00 ,  Y10S159/10

Abstract: The invention relates to a device for carrying out material exchange processes for high-viscosity liquids, especially for evaporating and/or degasifying polymer melts. The inventive device consists of at least one vertical container (1) having a supply line (4) for the liquid to be treated, an outlet (7) for volatile constituents and an outlet (6) for the treated liquid. Said supply line (4) is provided with a distribution element (3) having a plurality of openings (8, 10) for distributing the high-viscosity liquid to be treated between a plurality of individual currents. Said distribution element is characterised in that essentially vertically arranged wire loops (2) are arranged near the openings (8, 10). The high-viscosity liquid flows over said wire loops under the effect of gravity.

Abstract translation: 它是用于执行与所述的高粘度液体，特别是传质过程对熬煮和/或脱挥发的聚合物熔体的装置，具有一个进料（4），用于向待处理的液体，一个出口包括至少一个直立的容器（1）的（7） 用于处理液的挥发成分和出口（6），供给器（4）与（3），具有用于处理高粘度的液体的分配成多个单独的流的多个开口（8，10）中的分配器元件， 其特征在于，在所述开口（8，10）的区域中被安装大致垂直布置的线环（2）在其上的高粘度的液体在重力的作用下流出。

公开(公告)号：WO1995024252A1

公开(公告)日：1995-09-14

申请号：PCT/US1995000420

申请日：1995-01-12

Applicant: THE DOW CHEMICAL COMPANY

Inventor： THE DOW CHEMICAL COMPANY ,  CUMMINGS, Clark, J. ,  MEISTER, Bernard, J.

IPC: B01D03/06

CPC classification number: F28D9/0062 ,  B01D1/221 ,  B01D3/06 ,  C08F6/00 ,  F28D7/0041 ,  F28D9/0018 ,  F28F3/086 ,  F28F13/08 ,  Y10S159/10

Abstract: An improved polymer devolatilization apparatus comprising a flat plate heater (22) comprising a polymer solution supply means (20), and a liquid/vapor collection and separation means, said flat plate heater further comprising a multiplicity of flat plates defining a plurality of channels (10), each channel having a substantially uniform height, but varying width over the total channel length, each channel comprising three zones: a first zone (12), having a beginning (18) and a terminus, said beginning in operative communication with the polymer solution supply means, characterized by decreasing width as a function of distance from its beginning, a second zone (14) having a beginning at the terminus of the first zone and a terminus, characterized by at least one occurrence of a restrictive cross-sectional area, and a third zone (16) having a beginning at the terminus of the second zone and terminating at a liquid/vapor collection and separation region operating at reduced pressure, said third zone characterized by increasing width as a function of distance from its beginning, and provided further that the ratio of maximum width of the third zone to the maximum width of the second zone is from 2:1 to 20:1.

Abstract translation: 一种改进的聚合物脱挥发装置，包括包括聚合物溶液供应装置（20）的平板加热器（22）和液体/蒸汽收集和分离装置，所述平板加热器还包括限定多个通道的多个平板 每个通道具有基本均匀的高度，但在总通道长度上具有变化的宽度，每个通道包括三个区域：具有开始（18）和末端的第一区域（12），所述第一区域（12）开始与 聚合物溶液供应装置，其特征在于将宽度从其开始减小为距离的函数;第二区域（14），其具有在第一区域的末端的起始点和末端，其特征在于至少一次出现限制性横截面 区域和第三区域（16），其具有在第二区域的末端处的开始并且终止于在减压下操作的液体/蒸气收集和分离区域，所述第二区域 第三区域的特征在于宽度随着距离开始的距离而增加，并且进一步提供了第三区域的最大宽度与第二区域的最大宽度的比率为2:1至20:1。

公开(公告)号：WO1993013843A1

公开(公告)日：1993-07-22

申请号：PCT/US1993000298

申请日：1993-01-13

Applicant: QUANTUM CHEMICAL CORPORATION

Inventor： QUANTUM CHEMICAL CORPORATION ,  SUNG, Chieh-Yuan, F.

IPC: B01D03/06

CPC classification number: B01J8/005 ,  B01D3/06 ,  B01J2219/00006 ,  C08F6/003 ,  Y02P20/57 ,  Y10S159/02 ,  Y10S159/03 ,  Y10S159/10 ,  C08L23/00

Abstract: A highly energy efficient process for removing hydrocarbons from polymer slurries is disclosed. The process includes feeding a hydrocarbon-containing polymer slurry to a flash tank to flash a portion of the hydrocarbon from the slurry. Thereafter, the resulting slurry is fed to a fluid bed dryer wherein additional hydrocarbon is stripped from the polymer. Subsequently, the resulting polymer powder is transferred to a powder silo wherein further hydrocarbon is removed from the polymer utilizing a heated purge gas flowing countercurrent to the polymer powder. The polymer output preferably has a low hydrocarbon content, on the order of 100 ppm or less.

Abstract translation: 公开了一种用于从聚合物浆料中除去碳氢化合物的高效节能工艺。 该方法包括将含烃聚合物浆料进料到闪蒸罐中以从浆料中闪蒸一部分烃。 此后，将得到的浆料送入流化床干燥器，其中从聚合物中除去附加的烃。 随后，将所得聚合物粉末转移到粉末料仓，其中使用与聚合物粉末逆流流动的加热的净化气体，从聚合物中除去其它烃。 聚合物输出优选具有低于100ppm或更低的烃含量。

公开(公告)号：WO2004018522A2

公开(公告)日：2004-03-04

申请号：PCT/US2003/024954

申请日：2003-08-07

Applicant: FINA TECHNOLOGY, INC.

Inventor： BERTI, Douglas, A. ,  SOSA, Jose ,  GRIFFITH, Aron, T.

IPC: C08F

CPC classification number: B01D3/06 ,  C08F6/005 ,  Y10S159/10

Abstract: The present invention provides an apparatus and method of reducing volatiles in a mass processable polymer. The apparatus comprises a multi-chambered devolatilizer having first and second collectors contained therein. In one embodiment, the invention provides a method that includes passing the mass processable polymer stream from a polymerization process to a first devolatilizer. The method continues by passing the polymer stream from the first devolatilizer to the multi-chambered devolatilizer. The apparatus and method allows for the production of a polymer having less than 100 ppm of volatiles.

Abstract translation: 本发明提供一种在可加脂聚合物中还原挥发物的装置和方法。 该设备包括多室脱挥器，其中包含第一和第二收集器。 在一个实施方案中，本发明提供了一种方法，其包括将可加工聚合物流从聚合过程传递到第一脱挥发物。 该方法通过使聚合物流从第一脱挥发物流入多室脱挥发剂而继续。 该装置和方法允许生产具有小于100ppm挥发物的聚合物。