- Patent Title: Methods respectively for producing 2,4,6-tris (2-hydroxy-3-methyl-4-alkoxyphenyl)-1,3,5-triazine compound and 2,4,6-tris(2,4-dihydroxy-3-methylphenyl)-1,3,5-triazine
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Application No.: US15758807Application Date: 2016-09-01
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Publication No.: US10351538B2Publication Date: 2019-07-16
- Inventor: Koji Machida , Akira Nishiyama
- Applicant: KANEKA CORPORATION
- Applicant Address: JP Osaka-shi
- Assignee: KANEKA CORPORATION
- Current Assignee: KANEKA CORPORATION
- Current Assignee Address: JP Osaka-shi
- Agency: Oblon, McClelland, Maier & Neustadt, L.L.P.
- Priority: JP2015-177994 20150909
- International Application: PCT/JP2016/075705 WO 20160901
- International Announcement: WO2017/043416 WO 20170316
- Main IPC: C07D251/24
- IPC: C07D251/24 ; C07D251/28 ; G02B1/14 ; B32B7/02 ; G02B5/30

Abstract:
The present invention provides methods respectively for producing a 2,4,6-tris(2-hydroxy-3-methyl-4-alkoxyphenyl)-1,3,5-triazine compound and 2,4,6-tris(2,4-dihydroxy-3-methylphenyl)-1,3,5-triazine, both of which are improved in yield and quality. The methods according to the present invention are characterized in that a reaction of 2,4,6-tris(2,4-dihydroxy-3-methylphenyl)-1,3,5-triazine with an alkylating agent is carried out using a base in the presence of an alcohol or water, and are also characterized in that an ester compound is used as an additive in a reaction of cyanuric chloride with 2-methylresorcinol.
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