- Patent Title: Guest-compound-enveloping polymer-metal-complex crystal, method for producing same, method for preparing crystal structure analysis sample, and method for determining molecular structure of organic compound
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Application No.: US16217086Application Date: 2018-12-12
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Publication No.: US10684198B2Publication Date: 2020-06-16
- Inventor: Makoto Fujita , Yasuhide Inokuma , Shota Yoshioka , Junko Ariyoshi
- Applicant: JAPAN SCIENCE AND TECHNOLOGY AGENCY
- Applicant Address: JP Kawaguchi-shi, Saitama
- Assignee: JAPAN SCIENCE AND TECHNOLOGY AGENCY
- Current Assignee: JAPAN SCIENCE AND TECHNOLOGY AGENCY
- Current Assignee Address: JP Kawaguchi-shi, Saitama
- Agency: Westerman, Hattori, Daniels & Adrian, LLP
- Priority: com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@10bdd352 com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@4a3d30c1
- Main IPC: C30B29/54
- IPC: C30B29/54 ; G01N1/28 ; C07D401/14 ; C07D311/30 ; C07D307/92 ; C30B7/06 ; C30B29/58 ; B05D1/18 ; G01N23/207 ; G01N31/22
Abstract:
The present invention is a method for preparing a crystal structure analysis sample in which a molecule of an organic compound for which a molecular structure is to be determined, is arranged in pores and voids of a polymer-metal complex crystal in an ordered manner. The method includes immersing a polymer-metal complex crystal including a guest compound in a solvent solution that includes the organic compound, the polymer-metal complex crystal including a guest compound being the polymer-metal complex crystal comprising a polymer-metal complex that comprises a ligand having two or more coordinating moieties. A ratio of an amount of the guest compound (A) present in the pores and the voids to a total amount of the guest compound included in the pores and the voids being 60 mol % or more.
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