Invention Grant
- Patent Title: Methods of preparing positive electrode active material precursor for lithium secondary battery and positive electrode active material
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Application No.: US16333378Application Date: 2018-02-06
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Publication No.: US10892471B2Publication Date: 2021-01-12
- Inventor: Sang Soon Choi , Hyun Ah Park , Won Sig Jung
- Applicant: LG Chem, Ltd.
- Applicant Address: KR Seoul
- Assignee: LG Chem, Ltd.
- Current Assignee: LG Chem, Ltd.
- Current Assignee Address: KR Seoul
- Agency: Lerner, David, Littenberg, Krumholz & Mentlik, LLP
- Priority: KR10-2017-0016346 20170206,KR10-2018-0014230 20180205
- International Application: PCT/KR2018/001607 WO 20180206
- International Announcement: WO2018/143783 WO 20180809
- Main IPC: H01M4/04
- IPC: H01M4/04 ; C01G53/00 ; H01M10/0525 ; H01M4/505 ; H01M4/02 ; H01M4/525

Abstract:
A method of preparing a positive electrode active material precursor for a lithium secondary battery by using a batch-type reactor, which includes the steps of 1) forming positive electrode active material precursor particles while continuously adding a transition metal-containing solution including a transition metal cation, an aqueous alkaline solution, and an ammonium ion-containing solution to a batch-type reactor, 2) sedimenting the positive electrode active material precursor particles formed; 3) discharging a supernatant formed after the sedimentation of the positive electrode active material precursor particles to an outside; 4) adjusting a pH to 10 to 12 by adding the ammonium ion-containing solution; and 5) growing the positive electrode active material precursor particles while continuously again adding the transition metal-containing solution to the batch-type reactor, and a method of preparing a positive electrode active material using the same.
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