发明授权
US08841489B2 Method for carrying out multiphase aldol condensation reactions to give mixed α, β-unsaturated aldehydes
有权
进行多相醛醇缩合反应的方法,得到混合的α,β-不饱和醛
- 专利标题: Method for carrying out multiphase aldol condensation reactions to give mixed α, β-unsaturated aldehydes
- 专利标题(中): 进行多相醛醇缩合反应的方法,得到混合的α,β-不饱和醛
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申请号: US13989455申请日: 2012-02-09
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公开(公告)号: US08841489B2公开(公告)日: 2014-09-23
- 发明人: Dirk Bermann , Guido D. Frey , Norman Nowotny , Kurt Schalapski , Heinz Strutz
- 申请人: Dirk Bermann , Guido D. Frey , Norman Nowotny , Kurt Schalapski , Heinz Strutz
- 申请人地址: DE Oberhausen
- 专利权人: Oxea GmbH
- 当前专利权人: Oxea GmbH
- 当前专利权人地址: DE Oberhausen
- 代理商 Michael W. Ferrell
- 优先权: DE102011012846 20110303
- 国际申请: PCT/EP2012/000523 WO 20120209
- 国际公布: WO2012/116775 WO 20120907
- 主分类号: C07C45/72
- IPC分类号: C07C45/72 ; C07C45/74 ; C07C45/45
摘要:
The invention relates to a continuous method for carrying out a multiphase aldol condensation reaction to obtain mixed α,β-unsaturated aldehydes by reacting a mixture of two aliphatic aldehydes having different numbers of carbon atoms, i.e. 2 to 5, in the molecule in a vertical tubular reactor in a concurrent flow in the presence of an aqueous solution of a basically reacting compound. In said method, the aldehyde mixture is dispersed in the aqueous phase in the form of drops, and the aqueous solution of the basically reacting compound flows through the tubular reactor as a continuous phase in laminar conditions.
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