发明授权
- 专利标题: Production method for powdered hydrophilic modified polyrotaxane
- 专利标题(中): 粉状亲水改性聚轮烷的生产方法
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申请号: US14004839申请日: 2011-12-05
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公开(公告)号: US09238696B2公开(公告)日: 2016-01-19
- 发明人: Tomoaki Yamasaki , Shinya Okazaki , Hiroki Okazaki , Shigeki Hamamoto , Yuki Hayashi , Minoru Iwata
- 申请人: Tomoaki Yamasaki , Shinya Okazaki , Hiroki Okazaki , Shigeki Hamamoto , Yuki Hayashi , Minoru Iwata
- 申请人地址: JP Hyogo
- 专利权人: Sumitomo Seika Chemicals Co., Ltd.
- 当前专利权人: Sumitomo Seika Chemicals Co., Ltd.
- 当前专利权人地址: JP Hyogo
- 代理机构: Hamre, Schumann, Mueller & Larson, P.C.
- 优先权: JP2011-055503 20110314
- 国际申请: PCT/JP2011/078019 WO 20111205
- 国际公布: WO2012/124217 WO 20120920
- 主分类号: C08L71/02
- IPC分类号: C08L71/02 ; C08L5/16 ; C08B37/16 ; C08J3/12
摘要:
The present invention aims to provide a method of producing a powdered hydrophilic modified polyrotaxane, which enables production of a powdered hydrophilic modified polyrotaxane excellent in storage stability in an industrially advantageous way. The present invention provides a method of producing a powdered hydrophilic modified polyrotaxane, comprising: a hydrophilic modification step of preparing a solution of a hydrophilic modified polyrotaxane by modifying all or part of hydroxy groups on a cyclodextrin of a polyrotaxane with hydrophilic modifying groups, the polyrotaxane containing the cyclodextrin, a polyethylene glycol included in the cavities of the cyclodextrin molecules in a skewered manner, and a capping group that is placed at each end of the polyethylene glycol and prevents dissociation of the cyclodextrin molecules from the polyethylene glycol; and a drying step of spraying the prepared solution of the hydrophilic modified polyrotaxane and drying the solution of the hydrophilic modified polyrotaxane in a heated gas stream.
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