Preparation of alpha-beta-unsaturated c3-c6 carboxylic acids
    9.
    发明公开
    Preparation of alpha-beta-unsaturated c3-c6 carboxylic acids 失效
    Herstellung von alpha-beta-ungesättigtenC3-C6-Carbonsäuren。

    公开(公告)号:EP0675100A2

    公开(公告)日:1995-10-04

    申请号:EP95301386.9

    申请日:1995-03-03

    IPC分类号: C07C51/43 C07C57/07

    摘要: The present invention provides a process for the preparation of an α,β-unsaturated C 3 -C 6 carboxylic acid of greater than 98% purity, which combines fractional distillation and melt crystallization procedures. One embodiment of the process of the invention is depicted schematically in Figure 1 wherein 1 represents a dehydrogenation reactor in which a C 3 -C 6 carboxylic acid is dehydrogenated to produce on α,β-unsaturated C 3 -C 6 carboxylic acid, 3 represents a distillation unit and 6 represents a melt crystallizer.

    摘要翻译: 本发明提供了一种制备大于98%纯度的α,β-不饱和C 3 -C 6羧酸的方法,其结合分馏和熔融结晶方法。 在图1中示意性地描述了本发明方法的一个实施方案,其中1表示脱氢反应器,其中C3-C6羧酸被脱氢生成α,β-不饱和C3-C6羧酸,3表示蒸馏装置, 6表示熔融结晶器。