摘要:
Only X-rays having a specific wavelength out of focusing X-rays 2 diffracted from a sample S is reflected from a monochromator 60 based on a Bragg's condition, passed through a receiving slit 30 and detected by an X-ray detector 20. The monochromator 60 is configured to be freely removable, and arranged between the sample S and a focal point 2a at which the focusing X-rays 2 diffracted from the sample S are directly focused. At this time, the monochromator 60 is approached to the focal point 2a as closely as possible. The monochromator 60 comprises a multilayer mirror having an internal interplanar spacing which varies continuously from one end to the other end.
摘要:
The present disclosure relates to a multi-modality detection method and system. The multi-modality detection system includes: a distributed radiation source (101) configured to irradiate an object under detection; a primary collimator (102) configured to separate rays of the distributed radiation source into two parts, wherein one part is for CT detection and the other part is for XRD detection; a CT detection device (103) configured to perform a CT detection to acquire a CT image of the object under detection; and an XRD detection device (104) configured to perform an XRD detection to acquire an XRD image of the object under detection, wherein the CT detection and the XRD detection are performed simultaneously.
摘要:
The invention concerns a method and apparatus for monitoring physical and chemical properties of a solid sample during a dissolution process, the sample comprising at least one soluble component. In the method, the solid sample is brought into contact with dissolution medium for producing a solution and a solid residue of the solid sample, the solution is analyzed for determining the concentration of the soluble component during the dissolution process. Simultaneously with analyzing the solution, the atom- or molecule-scale physical or chemical composition of the solid residue is analyzed. The invention provides a new method for studying phenomena taking place in the solid residue during a dissolution process.
摘要:
In an X-ray analysis apparatus, a specimen (96) to be examined is mounted on the circumference of a focus cylinder (94), which can be rolled along an auxiliary cylinder (88) arranged concentrically around the beam focus (98) of an X-ray beam (84). Independently of the movement mechanism (100) used, a fixed part of the specimen then remains continuously in the beam path. Invariably the same surface area of the specimen is irradiated by the X-ray beam. The movement mechanism (107) may have added to it a device by means of which during the movement of the specimen (96) and the detector (106) the detector is continuously optimally directed to the specimen. The specimen holder may have added to it a device for rotating and/or tilting a specimen included therein.
摘要:
Disclosed are fibers which contain identification fibers. The identification fibers can comprise one or more chemical markers, or taggants, which may vary among the fibers or be incorporated throughout all of the fibers. The disclosure also relates to the method for making and characterizing the fibers. Characterization of the fibers can include identifying chemical markers and correlating the chemical markers and a taggant chemical marker amounts of at least one of the chemical markers to manufacturer-specific taggants to determine supply chain information. The supply chain information can be used to track the fibers from manufacturing through intermediaries, conversion to final product, and/or the consumer.
摘要:
Only X-rays having a specific wavelength out of focusing X-rays 2 diffracted from a sample S is reflected from a monochromator 60 based on a Bragg's condition, passed through a receiving slit 30 and detected by an X-ray detector 20. The monochromator 60 is configured to be freely removable, and arranged between the sample S and a focal point 2a at which the focusing X-rays 2 diffracted from the sample S are directly focused. At this time, the monochromator 60 is approached to the focal point 2a as closely as possible. The monochromator 60 comprises a multilayer mirror having an internal interplanar spacing which varies continuously from one end to the other end.
摘要:
The present invention pertains to a method for obtaining and analyzing solids, preferably crystals, which method comprises the following steps: - providing a well plate, the well plate comprising a plurality of wells, each of the wells having a depth and an open upper end and each of the wells being provided with a filter having pores, which filter is arranged at a distance below the open upper end, each of the wells having an upper inner wall part above the filter that has a fluid contact surface and each filter having a top filter surface, at least both the fluid contact surface of the well and the top filter surface being of a material that is at least substantially inert for organic and/or aqueous solvents and/or mixtures of organic and aqueous solvents. - providing one or more substances and one or more solvents in at least one of the wells of the well plate, - applying conditions to dissolve the one or more substances in the one or more solvents; - applying conditions for crystallizing at least a part of the substance so that solids are formed in the at least one well, - substantially removing the part of the substance that remains in solution, thereby leaving the solids, preferably crystals, that were formed from the substance in the well of the well plate in which they were formed, - performing further investigation of the solids, preferably crystals in the well of the well plate where they were formed.
摘要:
The invention discloses a method and an apparatus for measuring lattice spacings in particular of a single crystal during the grow thereof by vapour deposition whilst located in a heating furnace.