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    EXTRACTION SELECTIVE D'UN ACIDE OMEGA-FONCTIONNALISE APRES COUPURE OXYDANTE D'UN ACIDE GRAS INSATURE ET DERIVES
    135.
    发明公开
    EXTRACTION SELECTIVE D'UN ACIDE OMEGA-FONCTIONNALISE APRES COUPURE OXYDANTE D'UN ACIDE GRAS INSATURE ET DERIVES 审中-公开
    AFTER不饱和脂肪酸和衍生物的氧化断裂OMEGA功能化的ACID选择性提取

    公开(公告)号：EP2917176A1

    公开(公告)日：2015-09-16

    申请号：EP13795840.1

    申请日：2013-11-07

    申请人： Arkema France

    发明人： BRANDHORST, Markus

    IPC分类号： C07C253/34 ,  C07C51/34 ,  C07C51/48

    CPC分类号： C07C253/34 ,  C07C51/34 ,  C07C51/48 ,  C07C55/18

    摘要： The invention concerns a method for the selective extraction of a reaction product, originating from an oxidative cleavage of an unsaturated fatty acid or of an ester derivative or of an unsaturated nitrile derivative, said reaction product being a co-functionalised acid chosen from the C
    6 to C15 diacids, ester-acids and nitrile-acids, using, as the selective extraction solvent, a composition comprising a mixture of water and C1-C4 carboxylic acid. The invention also concerns the use of said method and the extraction solvent composition for the preparation of C6 to C15 amino acid, diacid or ester-acid monomers for the production of polycondensation polymers, in particular polyamides.

    METHOD FOR PRODUCING CYANOALKENYLCYCLOPROPANECARBOXYLIC ACID SALT
    139.
    发明公开
    METHOD FOR PRODUCING CYANOALKENYLCYCLOPROPANECARBOXYLIC ACID SALT 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON CYANO-ALKENYL-CYCLOPROPAN-CARBOXYLSÄURESALZ

    公开(公告)号：EP2537828A1

    公开(公告)日：2012-12-26

    申请号：EP11742383.0

    申请日：2011-02-10

    申请人： Sumitomo Chemical Company, Limited

    发明人： KOMOTO, Ichiro ,  SOMYO, Toshio ,  HIROTA, Masaji

    IPC分类号： C07C253/34 ,  C07C255/31

    CPC分类号： C07C253/34 ,  C07B2200/09 ,  C07C211/07 ,  C07C211/35 ,  C07C253/30 ,  C07C255/31 ,  C07C2601/02 ,  C07C2601/08 ,  C07C2601/14

    摘要： A method for producing a salt of an amine with a cyanoalkenylcyclopropanecarboxylic acid, the method comprising a first step of mixing a carboxylic acid compound represented by formula (2C) and at least one amine selected from the group consisting of primary amines and secondary amines in an organic solvent; a second step of depositing a salt of the amine with a cyanoalkenylcyclopropanecarboxylic acid represented by formula (2) from the mixture obtained in the first step; and a third step of recovering the salt deposited in the second step;

    wherein, R represents an alkyl group optionally having a substituent or a halogen atom.

    摘要翻译： 一种用氰基链烯基环丙烷羧酸生产胺盐的方法，该方法包括将式（2C）表示的羧酸化合物与至少一种选自伯胺和仲胺的胺在 有机溶剂; 从第一步骤获得的混合物中，用式（2）表示的氰基链烯基环丙烷羧酸沉积胺盐; 以及回收在第二步中沉积的盐的第三步骤; 其中，R表示任选具有取代基的烷基或卤素原子。

    Method for the manufacture of escitalopram
    140.
    发明公开
    Method for the manufacture of escitalopram 审中-公开
    Verfahren zur Herstellung von Escitalopram

    公开(公告)号：EP2397461A1

    公开(公告)日：2011-12-21

    申请号：EP11172640.2

    申请日：2008-09-10

    申请人： H. Lundbeck A/S

    发明人： De Faveri, Carla ,  Huber, Florian, Anton, Martin ,  Dancer, Robert

    IPC分类号： C07C253/34 ,  C07C255/53 ,  C07D307/87

    CPC分类号： C07D307/87 ,  C07C253/34 ,  C07C255/59

    摘要： This patent discloses a method for resolution of 4-[4-(dimethylamino)-1-(4'-fluorophenyl)-1-hydroxybutyl]-3-(hydroxymethyl)-benzonitrile as a racemic or non-racemic enantiomer mixture into its isolated enantiomers, said method comprising the step of fractionally crystallising 4-[4-(dimethylamino)-1-(4'-fluorophenyl)-1-hydroxybutyl]-3-(hydroxymethyl)-benzonitrile as a salt with the (+)-(S,S)-or (-)-(R,R)-enantiomer of O , O' -di- p -toluoyl-tartaric acid in a solvent system comprising 1-propanol, ethanol or acetonitrile.

    摘要翻译： 该专利公开了一种将外消旋或非外消旋对映异构体混合物中的4- [4-（二甲基氨基）-1-（4'-氟苯基）-1-羟基丁基] -3-（羟基甲基） 所述方法包括将（+） - （（+） - （4-甲氧基苯基）-1-（4-甲氧基）-1-羟基丁基] S，S）-OR（ - ） - （R，R） - 对映异构体，包括1-丙醇，乙醇或乙腈的O，O'-二 - 对甲酰基 - 酒石酸。