VERFAHREN ZUR HERSTELLUNG VON IMIDAZOLIUMSALZEN
    23.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON IMIDAZOLIUMSALZEN 审中-公开
    用于生产咪唑

    公开(公告)号:EP2203428A1

    公开(公告)日:2010-07-07

    申请号:EP08803874.0

    申请日:2008-09-09

    Applicant: BASF SE

    CPC classification number: C07D233/56 C07D233/58

    Abstract: A method for producing imidazolium salts of the formula (I), where R1 and R3, independently of one another, denote an organic residue having 1 to 20 carbon atoms, R2, R4, and R5, independently of one another, denote an H atom or an organic residue having up to 20 carbon atoms, and A denotes an anion except for a carbonate anion, characterized in that, in a first step of the method an imidazolium salt of the formula (Il) is produced by the reaction of imidazoles of the formula (III), where the residues R have the above meanings, with an alkyl carbonate of the formula (IV), where R3 has the above meaning, and in a second step of the method, the obtained imidazolium salts of the formula (Il) are reacted with acids or salts containing the anion A in order to form the imidazolium salt (I), the reaction being performed in both steps of the method in the presence of methanol, and the content of methanol in the first step of the method being at least 100 parts by weight of methanol and in the second step of the method being at least 50 parts by weight, relative to 100 parts by weight of the sum of the materials used of the formulas (III) + (IV) employed in the first step of the method in each case.

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