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    CU-SAPO MOLECULAR SIEVE, SYNTHESIS METHOD THEREFOR AND CATALYTIC USE THEREOF
    31.
    发明公开
    CU-SAPO MOLECULAR SIEVE, SYNTHESIS METHOD THEREFOR AND CATALYTIC USE THEREOF 审中-公开

    公开(公告)号：EP3586960A1

    公开(公告)日：2020-01-01

    申请号：EP17897284.0

    申请日：2017-02-27

    申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences

    发明人： TIAN, Peng ,  XIANG, Xiao ,  LIU, Zhongmin ,  CAO, Lei

    IPC分类号： B01J29/85 ,  C01B37/08 ,  C01B39/54 ,  C07C1/20

    摘要： Disclosed are a Cu-SAPO molecular sieve with coexisting crystal phases of CHA and GME, a synthesis process therefor and the use thereof in a denitration reaction. A XRD diffraction pattern of the Cu-SAPO molecular sieve shows the characteristic of broad peaks and narrow peaks coexisting. An inorganic framework has the following chemical composition: wCu-(Si x Al y P z )O 2 , wherein x, y and z respectively represent the molar fractions of Si, Al and P; the molar fraction ranges thereof are respectively x = 0.01∼0.28, y = 0.35∼0.55 and z = 0.28∼0.50, with x+y+z = 1; w is the molar number of Cu per mole of (Si x Al y P z )O 2 ; and w = 0.001∼0.124. The synthesized molecular sieve can be used as a catalyst for a selective reduction of NO x .

    METHOD FOR SYNTHESIZING SAPO MOLECULAR SIEVE BY SOLVOTHERMAL METHOD AND CATALYST PREPARED THEREBY
    36.
    发明公开
    METHOD FOR SYNTHESIZING SAPO MOLECULAR SIEVE BY SOLVOTHERMAL METHOD AND CATALYST PREPARED THEREBY 审中-公开
    法合成SAPO分子七个由SOLVOTHERMISCHES过程，并在这个过程中制得的催化剂

    公开(公告)号：EP2660203A4

    公开(公告)日：2017-04-12

    申请号：EP11852524

    申请日：2011-06-24

    申请人： DALIAN INST CHEMICAL PHYSICS CAS

    发明人： TIAN PENG ,  LIU ZHONGMIN ,  ZHANG YING ,  FAN DONG ,  SU XIONG

    IPC分类号： C01B39/54 ,  B01J29/85 ,  C01B37/08

    CPC分类号： B01J29/85 ,  C01B37/08 ,  C01B39/54 ,  C07C1/20 ,  C07C2529/85 ,  Y02P30/42

    摘要： A solvothermal synthesis process of the SAPO molecular sieves and catalysts prepared thereby are provided. The synthesis process comprises the following steps: a) an organic amine, an aluminum source, a phosphorus source, a silicon source, and water are mixed in a molar ratio of 6-30 : 1 : 0.5-5 : 0.01-1.0 : 0.1-15, to obtain an initial mixture for preparing the SAPO molecular sieves, wherein the molar ratio of water to the organic amine is less than 2.0; b) the initial mixture obtained in the step a) is maintained at 30-60 °C and aged with stirring for not more than 24 hours, to obtain an initial gel; c) the initial gel obtain in the step b) is crystallized at 150-250 °C for 0.5-15 days. The SAPO molecular sieves prepared thereby are used, after being calcined at 400 - 700 °C in air, as catalysts for acid-catalyzed reactions or for conversion reactions of oxygen-containing compounds to olefins.

    摘要翻译： 设置在SAPO分子筛，并由此制得的催化剂的溶剂热合成方法。 合成方法包括以下步骤：a）以有机胺铝源，磷源，硅源，水和在6-30的摩尔比混合的，：1：0.5-5：0.01〜1.0：0.1 -15，以获得在初始混合物用于制备SAPO分子筛，worin的水的摩尔比的有机胺是小于2.0; b）在步骤a）中获得的初始混合物保持在30-60℃并老化搅拌不超过24小时，以获得在初始凝胶; c）该初始凝胶获得在步骤b）在150-250℃下结晶为0.5〜15天。 由此制备的SAPO分子筛的使用，在400煅烧至700℃的空气中，作为催化剂用于酸催化的反应或反应为含氧化合物转化成烯烃后。

    LOW SILICON SAPO-42 AND METHOD OF MAKING
    39.
    发明公开
    LOW SILICON SAPO-42 AND METHOD OF MAKING 审中-公开
    SAPO-42低硅含量和制造方法

    公开(公告)号：EP2931659A1

    公开(公告)日：2015-10-21

    申请号：EP13861883.0

    申请日：2013-09-26

    申请人： UOP LLC

    发明人： MOSCOSO, Jaime, G.

    IPC分类号： C01B37/08 ,  C01B39/54

    CPC分类号： B01J29/85 ,  B01J35/002 ,  C01B37/08 ,  C01B39/54

    摘要： A porous crystalline silico-alumino-phosphate molecular sieve is described. The molecular sieve has a framework composition on an anhydrous and calcined basis expressed by an empirical formula (SixAlyPz)O2 where x is the mole fraction of Si and has a value from 0.001 to about 0.5, y is the mole fraction of Al and has a value of at least 0.01, z is the mole fraction of P has a value of at least 0.01, and x+y+z=1, where the molecular sieve is characterized as having a LTA framework with an average crystal size of less than 5 micrometers. Methods of making the molecular sieves are also described.