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公开(公告)号：EP1907112A2
公开(公告)日：2008-04-09
申请号：EP06787640.9
申请日：2006-07-17
CPC分类号： B01F7/163 , B01F7/162 , B01J3/02 , B01J3/03 , B01J4/001 , B01J19/0066 , B01J19/0073 , B01J19/02 , B01J19/123 , B01J19/126 , B01J19/127 , B01J19/128 , B01J19/129 , B01J19/18 , B01J19/1806 , B01J2219/00078 , B01J2219/00083 , B01J2219/00094 , B01J2219/00779 , B01J2219/0236 , B01J2219/0245 , B01J2219/0286 , B01J2219/0295 , B01J2219/0869 , B01J2219/0871 , B01J2219/185 , B01J2219/1943 , C07C17/087 , C07C19/075 , Y02P20/149
摘要： Reactors including a chamber having a mixing apparatus within the chamber are provided. Reactors are also provided that include a chamber with a separation apparatus and/or a catalyst apparatus within the chamber. Reactor assemblies are provided that can include: a base configured to define at least a portion of a reaction chamber volume, a separation apparatus within the reaction chamber volume, a catalyst apparatus within the reaction chamber volume, and a lid coupled to both the separation and catalyst apparatuses. Production processes are provided that can include combining at least two reactants within a chamber to form a gas-phase reaction mixture and mechanically mixing the mixture within the chamber to form a product.
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2.发明公开CHEMICAL PRODUCTION PROCESSES, CHEMICAL PRODUCTION SYSTEMS, AND METHODS FOR MONITORING AND ALTERING REACTOR CONDITIONS 审中-公开化学品生产工艺，化工生产系统和监测方法和反应器条件的变化
公开(公告)号：EP1718951A1
公开(公告)日：2006-11-08
申请号：EP04704096.9
申请日：2004-01-21
CPC分类号： B01J19/0006 , B01D3/00 , B01D17/00 , B01D17/0214 , B01J2208/00707 , B01J2219/00173 , C07B39/00 , C07C17/206 , Y02P20/582 , C07C19/08 , C07C19/10
摘要： The present invention includes chemical production processes and systems as well as methods for monitoring and altering reactor conditions. A method for monitoring reactor conditions includes monitoring reactant recovery stream density and altering the condition when the density reaches a predetermined amount. A chemical production system is provided that includes a reactor unit receiving a reactant recovery stream from a separation unit where the stream can be monitored by a density monitor. A chemical process is also provided that includes reacting a reactant and a starting material in a reactor unit having reactor parameters and producing a product stream that includes the reactant, a product, and a by-product. A recycle stream comprising the reactant and the by-product can be separated from the product stream and returned to the reactor unit. The recycle stream density can be monitored at least periodically and the reactor parameters altered as the density indicates an increased concentration of the by-product in the recycle stream.
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公开(公告)号：EP1658261A1
公开(公告)日：2006-05-24
申请号：EP03818188.9
申请日：2003-07-29
摘要： A method for preparing tetrabromobenzoate ester from a tetrabromophthalic anhydride including the steps of reacting the tetrabromophthalic anhydride with a catalyst and an alcohol at a temperature that favors partial esterification over complete esterification of the tetrabromophthalic anhydride to form a tetrabromophthalate half-ester reaction mixture; and feeding the half-ester reaction mixture to at least one reactor having and maintaining a temperature that favors decarboxylation over esterification to produce a tetrabromobenzoate ester-containing product. The temperature favoring partial esterification of the tetrabromophthalic anhydride is between about 70°C and 130°C. The temperature favoring decarboxylation over esterification is between about 190°C and 205°C. The tetrabromobenzoate ester-containing product comprises at least about 85% tetrabromobensoate ester. The at least one reactor may include two or more reactors connected to one another in series.
摘要翻译： 由四溴邻苯二甲酸酐制备四溴苯甲酸酯的方法，包括以下步骤：使四溴邻苯二甲酸酐与催化剂和醇在有利于部分酯化的温度下反应，以完全酯化四溴邻苯二甲酸酐以形成四溴邻苯二甲酸酯半酯反应混合物; 并且将该半酯反应混合物进料到至少一个具有并保持有利于酯化脱羧的温度的反应器中以产生含有四溴苯甲酸酯的产物。 有利于四溴邻苯二甲酸酐部分酯化的温度在约70℃至130℃之间。 有利于酯化脱羧的温度在约190℃和205℃之间。 含有四溴苯甲酸酯的产物包含至少约85％的四溴苯甲酸酯。 该至少一个反应器可以包括彼此串联连接的两个或更多个反应器。
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公开(公告)号：EP1202624B1
公开(公告)日：2005-03-30
申请号：EP00948975.8
申请日：2000-07-28
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公开(公告)号：EP1202624A1
公开(公告)日：2002-05-08
申请号：EP00948975.8
申请日：2000-07-28
发明人： YEOMAN, Alan, M. , GRUNEWALD, Fredrick, A. , HOWARTH, Jonathan, N. , HARRISON, Alan, D. , SOOK, Brian, R. , KRUPPA, Thomas
CPC分类号： A01N43/70 , A01N25/04 , A01N25/08 , A01N25/22 , A01N35/08 , A01N43/08 , A01N43/66 , A01N47/48 , A01N59/00 , A01N2300/00
摘要： A method of improving the rate of dissolution in water of low solubility compounds by combining a low solubility compound with a rheology additive that is made of platelets or particles which orient together with ionic or hydrogen bonds. The inventive method also may improve the hydrolytic stability of hydrolitically unstable low solubility compounds.
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公开(公告)号：EP1095185A1
公开(公告)日：2001-05-02
申请号：EP99921935.5
申请日：1999-05-12
发明人： DÜRKES, Frank , DUBACH, Walter
摘要： A method of inhibiting the autooxidation of fatty acids in a paper product made from pulp fiber is accomplished by adding to the pulp fiber between about 2 moles/metric ton and about 10 moles/metric ton of an oxidizing halogen.
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8.发明公开Process for the production of cyclopentyl 2-thienyl ketone 审中-公开Verfahren zur Herstellung von Cyclopentylthien-2-ylketon
公开(公告)号：EP1029858A1
公开(公告)日：2000-08-23
申请号：EP00300958.6
申请日：2000-02-08
IPC分类号： C07D333/22
CPC分类号： C07D333/22
摘要： A water-scavenging solvent, such a polyphosphoric acid, can be used for the synthesis of cyclopentyl 2-thienyl ketone by the direct acylation of cyclopentanecarboxylic acid without first reacting the cyclopentanecarboxylic acid with thionylchloride to form the acid chloride, while achieving new and unexpected yields. A tiletamine-free base can be made from the cyclopentyl 2-thienyl ketone with a halide in the presence of a solvent for the cyclopentyl 2-thienyl ketone to form a halogenated cyclopentane 2-thienyl ketone; aminating the halogenated cyclopentane 2-thienyl ketone by reaction with an amine; and subjecting the reaction product to thermal rearrangement, in a suitable solvent, and at a sufficient temperature to form tiletamine free base. Each step for the formation of tiletamine free base can be accomplished using the same solvent, e.g., dichlorobenzene so that intermediates need not be isolated between reactions.
摘要翻译： 通过直接酰化环戊烷羧酸，可以使用除水溶剂（如多磷酸）合成环戊基2-噻吩基酮，无需首先使环戊烷羧酸与亚硫酰氯反应形成酰氯，同时达到新的和出人意料的产率 。 在环戊基2-噻吩基酮溶剂存在下，环戊基2-噻吩基酮与卤化物可制成不熟肉胺的碱，形成卤代环戊烷2-噻吩酮; 通过与胺反应胺化卤代环戊烷2-噻吩基酮; 并在合适的溶剂中，并在足够的温度下使反应产物进行热重排以形成未熟丝胺游离碱。 可以使用相同的溶剂例如二氯苯来实现形成泰他胺游离碱的每个步骤，使得中间体不需要在反应之间分离。
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公开(公告)号：EP1012133A2
公开(公告)日：2000-06-28
申请号：EP98930430.8
申请日：1998-06-18
发明人： STULTS, Jeffrey, S. , SCHREIER, Jeffrey, A. , MARTIN, Jim, L. , MACK, Arthur, G. , DROST, Kevin, J. , ZINGDE, Gurudas
CPC分类号： C07C69/76 , C08K5/0016 , C08K5/10
摘要： The present invention provides novel esters synthesized from organic alcohols and tetrahalophthalic anydride or tetrahalophthalic acid, processes to make such esters, and novel uses of these esters. The invention provides three Groups of dialkyltetrahalophthalate compositions which exhibit surprisingly advantageous features, including excellent plasticizing functionality and low smoke generation. The esters may be symmetrical, in that both alcohols of the ester are the same, or they may be unsymmetrical with both alcohols of the derived phthalate ester different, or they may be mixtures of symmetrical and unsymmetrical esters. Inventive esters are useful as flame-retardant plasticizers in PVC or other polymeric systems.
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10.发明公开PROCESS FOR THE MANUFACTURE OF TETRABROMOBISPHENOL-A WITH CO-PRODUCTION OF n-PROPYL BROMIDE 失效用于生产四溴双酚A WHAT THE SAME正丙基溴生产的
公开(公告)号：EP0973712A1
公开(公告)日：2000-01-26
申请号：EP98907497.6
申请日：1998-02-18
IPC分类号： C07C39/16
CPC分类号： C07C37/62 , C07C17/16 , C07C19/075 , C07C39/367
摘要： A process for producing n-propyl bromide during the bromination of bis- of trisphenols uses non-aqueous n-propanol as the bromination solvent, providing salable yields of n-propyl bromide to accompany the brominated bisphenol or trisphenol.
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