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    DESULFURIZED TALL OIL AND DERIVATIVES THEREOF
    2.
    发明公开
    DESULFURIZED TALL OIL AND DERIVATIVES THEREOF 审中-公开

    公开(公告)号：EP3741833A1

    公开(公告)日：2020-11-25

    申请号：EP20176063.4

    申请日：2020-05-22

    申请人： Kraton Polymers Research B.V.

    发明人： DING, Ruidong ,  TIAN, Jason ,  REITER, Chad

    IPC分类号： C11B13/00 ,  C11C1/08 ,  C09F1/02

    摘要： A process for reducing or removing at least 90% of sulfur in a tall oil composition, e.g., to a level of 15 ppm or less is disclosed. The process employs at least a first desulfurization and a second desulfurization treatment in parallel or in series. The first treatment comprises adsorptive desulfurization, wherein the adsorbent material comprises silica adsorbent having an average pore size between 50-200 Å, BET surface area of at least 300 mm 2 /, pore volume of 1.20 to 3.00 cc/g, and a silanol [Si-OH] level of 0.5 to 5 unit/nm 2 . The second desulfurization treatment is selected from adsorptive treatment, heat treatment, distillation, extraction, oxidation, reduction, hydrogenation, and sulfur scavenging for a reduced sulfur content.

    BLOCK COPOLYMERS AND USES THEREOF
    3.
    发明公开
    BLOCK COPOLYMERS AND USES THEREOF 审中-公开

    公开(公告)号：EP3736129A1

    公开(公告)日：2020-11-11

    申请号：EP20172712.0

    申请日：2020-05-04

    申请人： Kraton Polymers Research B.V.

    发明人： MUYLDERMANS, Xavier ,  DING, Ruidong ,  DE WIT, Frank ,  VAN DUIN, Koen

    IPC分类号： B32B15/00 ,  C08J5/24 ,  H05K1/03 ,  C08K5/3492 ,  C08L53/00 ,  B32B27/30 ,  C08F297/04 ,  C08L53/02 ,  C08J5/18

    摘要： A polymer composition comprising a star-branched copolymer having a plurality of arms is disclosed. Each polymer arm has a molecular weight of from 1 kg/mol to 50 kg/mol and comprises polymerized units (i) derived from a first vinyl aromatic monomer comprising a radical-reactive group, wherein from greater than 10 mol % to 100 mol % of the units (i) are unhydrogenated; and optionally, polymerized units (ii) comprising hydrogenated and unhydrogenated forms of polymerized units derived from a high Tg monomer, and hydrogenated form of polymerized units (i) or hydrogenated form of polymerized styrene units; and optionally, polymerized units (iii) comprising (a) hydrogenated form of polymerized units derived from one or more acyclic conjugated dienes, and (b) polymerized units derived from one or more of a second vinyl aromatic monomer; wherein less than 10 wt. % of units (a) are unhydrogenated.

    Process for preparing a bituminous binder composition
    4.
    发明公开
    Process for preparing a bituminous binder composition 有权
    Polymerzusammensetzung zur Herstellung einerbituminösenBinderzusammensetzung

    公开(公告)号：EP2589624A1

    公开(公告)日：2013-05-08

    申请号：EP13153162.6

    申请日：2006-11-13

    申请人： KRATON Polymers Research B.V.

    发明人： Kluttz, Robert, Q. ,  Stephens, Keith, E.

    IPC分类号： C08L25/00 ,  C08L95/00 ,  C08L25/10

    CPC分类号： C08L95/00 ,  C08F297/044 ,  C08L53/02 ,  C08L53/00 ,  C08L2666/24

    摘要： The present invention is directed to a process for preparing a polymer modified bituminous binder composition in the substantial absence of crosslinking agents by heating a bitumen component in a stirred tank to a temperature from 185 °C to 221 °C; adding a block copolymer composition to the bitumen component while the bitumen component is being stirred to form a homogeneous mixture of the bitumen component and the block copolymer composition; and continuing to stir the homogeneous mixture while maintaining the temperature from 185 °C to 221 °C for a period of time from 4 hours to 30 hours thereby forming a cured polymer modified bituminous binder composition. The block copolymer composition utilized in the process comprises a diblock copolymer comprising one block of a monovinylaromatic hydrocarbon and one block of a conjugated diene having a peak molecular weight from 30,000 to 78,000 and a vinyl content from 35 to 80 mol percent based on the number of repeat monomer units in the conjugated diene block, and optionally one or more block copolymers comprising at least two blocks of monovinylaromatic hydrocarbon and at least one block of conjugated diene, the block copolymer selected from linear triblock copolymers having a peak molecular weight that is 1.5 to 3.0 times the peak molecular weight of the diblock copolymer, multiarm coupled block copolymers having a peak molecular weight that is 1.5 to 9.0 times the peak molecular weight of the diblock copolymer, and mixtures thereof, wherein each block copolymer has a vinyl content from 35 to 80 mol percent based on the number of repeat monomer units in the conjugated diene block, wherein when both (i) and (ii) are present in the block copolymer composition, the ratio of (i) to (ii) is greater than 1:1. The present invention is further related to an alternative to this process, a specific class of bituminous binder compositions and concentrates and a specific class of block copolymer compositions.

    摘要翻译： 本发明涉及通过将搅拌釜中的沥青组分加热至185℃至221℃的温度，基本上不存在交联剂制备聚合物改性沥青粘合剂组合物的方法; 在沥青组分被搅拌以形成沥青组分和嵌段共聚物组合物的均匀混合物时，向沥青组分中加入嵌段共聚物组合物; 并继续搅拌均匀混合物，同时保持温度从185℃至221℃，持续4小时至30小时，由此形成固化的聚合物改性沥青粘合剂组合物。 该方法中使用的嵌段共聚物组合物包括二嵌段共聚物，其包含一个单乙烯基芳族烃嵌段和一个共轭二烯嵌段，峰分子量为30,000至78,000，乙烯基含量为35至80mol％，基于 共轭二烯嵌段中的重复单体单元和任选的包含至少两个单乙烯基芳烃嵌段和至少一个共轭二烯嵌段的嵌段共聚物，该嵌段共聚物选自具有峰分子量为1.5至 二嵌段共聚物的峰值分子量的3.0倍，峰值分子量为二嵌段共聚物的峰值分子量的1.5〜9.0倍的多臂偶联嵌段共聚物及其混合物，其中各嵌段共聚物的乙烯基含量为35〜 基于共轭二烯嵌段中的重复单体单元的数量为80摩尔％，其中当 （i）和（ii）都存在于嵌段共聚物组合物中，（i）与（ii）的比例大于1:1。 本发明还涉及该方法的替代方案，特定类型的沥青粘合剂组合物和浓缩物以及特定类型的嵌段共聚物组合物。

    BITUMINOUS COMPOSITION
    5.
    发明授权
    BITUMINOUS COMPOSITION 有权
    沥青组合物

    公开(公告)号：EP1492844B1

    公开(公告)日：2012-01-18

    申请号：EP03745275.2

    申请日：2003-03-24

    申请人： KRATON Polymers Research B.V.

    发明人： TROMMELEN, Eric, A., T. ,  VAN DIJK, Martin, C.

    IPC分类号： C08L95/00 ,  C08L53/02 ,  C08F297/04

    CPC分类号： C08L95/00 ,  C08F297/04 ,  C08L53/02 ,  C08L53/00

    摘要： A bituminous composition which comprises a bituminous component and a block copolymer which comprises at least two blocks of a conjugated diene and at least two blocks of a monovinylaromatic hydrocarbon, being of the general formula: S1-B1-S2-B2 wherein B1 is a block of polymerized conjugated diene comprising at least 50 mole% isoprene having an apparent molecular weight of from 180,000 to 400,000, S1 and S2 are blocks of polymerized monovinylaromatic hydrocarbon having a weight average molecular weight of 12,000 to 40,000, and B2 is a block of polymerized conjugated diene comprising at least 50 mole% isoprene having an apparent molecular weight of from 15,000 to 60,000; wherein the weight ratio W of B1 over B2 is in the range of 3.0 to 12.0; and wherein the content of polymerized monovinylaromatic hydrocarbon is in the range from 10 to 35 wt.%.

    HYDROGENATED STYRENIC BLOCK COPOLYMER COMPOSITIONS WITH IMPROVED HIGH TEMPERATURE OVERMOLDING PROPERTIES
    8.
    发明授权
    HYDROGENATED STYRENIC BLOCK COPOLYMER COMPOSITIONS WITH IMPROVED HIGH TEMPERATURE OVERMOLDING PROPERTIES 有权
    氢化乙烯基芳族组合物与成形性改善的高温

    公开(公告)号：EP1732982B1

    公开(公告)日：2008-09-10

    申请号：EP05717116.7

    申请日：2005-03-21

    申请人： KRATON Polymers Research B.V.

    发明人： MARIS, Catherine A.L. ,  COIGNOUL, Emmanuelle, KRATON Polymers Research S.A

    IPC分类号： C08L53/02 ,  C08L23/26 ,  C08L23/00 ,  C09D153/02 ,  B29C70/00

    CPC分类号： C08F297/04 ,  C08L51/06 ,  C08L53/025 ,  C08L2666/24

    摘要： A hydrogenated styrenic block copolymer composition for overmolding onto a polar substrate is provided, comprising: a) 100 pbw of a hydrogenated styrenic block copolymer having at least two resinous endblocks of polymerized monovinyl arene and an elastomeric midblock of polymerized and subsequently hydrogenated conjugated diene or dienes, b) from 25 to 60 pbw of a functionalized polyolefin, and optionally c) from 0 to 100 pbw of a plasticizer, d) from 0 to 200 pbw of one or more fillers and filler deactivators, e) from 0 to 2 pbw of antioxidants, f) from 0 to 100 pbw of a polar engineering thermoplast, wherein component (a) is a linear hydrogenated styrenic block copolymer having an apparent molecular weight in the range of from 200,000 to 500,000 or a radial hydrogenated styrenic block copolymer having an apparent molecular weight in the range of from n times 100,000 to 250,000, n equals the number of polymer arms, and component (a) has a content of hydrogenated 1,2-polymerized conjugated dienes (vinyl content) of greater than 40% and a content of poly(monovinyl arene) in the range of from 20 to 50%,and component (b) is an acid, anhydride or ester functionalized polyolefin having a grafting level of 0.5 to 5%w and a melt flow rate (MFR, ASTM D 1238-95 at Condition L) equal to or greater than 20 g/10 minutes.

    ASPHALT BINDER FOR POROUS PAVEMENTS
    10.
    发明公开
    ASPHALT BINDER FOR POROUS PAVEMENTS 有权
    ASPHALTBINDEMITTELFÜRPORÖSEPFLASTER

    公开(公告)号：EP1951817A1

    公开(公告)日：2008-08-06

    申请号：EP06807309.7

    申请日：2006-10-16

    申请人： KRATON Polymers Research B.V.

    发明人： SCHOLTEN, Erik Jan

    IPC分类号： C08L95/00

    CPC分类号： C08L95/00 ,  C08L2666/24 ,  C08L53/00

    摘要： An asphalt binder is provided, comprising 85 to 97.5 parts by weight of a bitumen and 16 to 2.5 parts by weigh of a polymer composition, wherein the polymer composition comprises:(i) from 2 to 8, preferably from 3 to 6 parts by weight of a styrenic block copolymer having at least two blocks of monovinylaromatic hydrocarbon (A) and at least one block of a conjugated diene (B), wherein the block copolymer composition has a vinyl content of at least 25% by weight, preferably from 25 to 40% by weight, based on the total diene content; (ii) from 0 to 5, preferably from 1 to 3 parts by weight of a styrenic diblock copolymer having one block of monovinylaromatic hydrocarbon (A) and one block of a conjugated diene (B); and (iii) from 0.5 to 3, preferably from 1 to 2.5 parts by weight of an ethylene-vinyl acetate copolymer, wherein the weight ratio of (i) + (ii):(iii) is from 2:1 to 6:1, preferably from 3:1 to 4:1. In addition, an asphalt mix is provided comprising 2 to 8 parts by weight of the asphalt binder of the present invention and 98 to 92 parts by weight of gap-graded aggregate or open-graded aggregate material. Furthermore, a porous pavement is claimed, produced from the open or gap-graded mixes, by compacting the asphalt mix mentioned above.

    摘要翻译： 提供沥青粘合剂，其包含85至97.5重量份的沥青和16至2.5重量份的聚合物组合物，其中所述聚合物组合物包含：（i）2至8，优选3至6重量份 具有至少两个单乙烯基芳族烃（A）和至少一个共轭二烯（B）的嵌段的苯乙烯嵌段共聚物，其中嵌段共聚物组合物的乙烯基含量为至少25重量％，优选为25至 40重量％，基于总二烯含量; （ii）0至5，优选1至3重量份具有一个单乙烯基芳族烃（A）和一个共轭二烯（B）嵌段的苯乙烯二嵌段共聚物; 和（iii）0.5至3重量％，优选1至2.5重量份的乙烯 - 乙酸乙烯酯共聚物，其中（i）+（ii）：（iii）的重量比为2:1至6:1 ，优选为3：1至4：1。 此外，提供了包含2至8重量份本发明的沥青粘合剂和98至92重量份的间隙聚集体或开放分级骨料材料的沥青混合料。 此外，通过压实上述沥青混合料，要求由开放或间隙分级的混合物生产的多孔路面。