摘要:
A positive plate material for lithium secondary cells stably exhibiting excellent performance including the cell initial capacity, cycle characteristics, and the safety. The material is procuded by dripping an aqueous solution of a salt (e.g., cobalt sulfate) of a doping element (e.g. a transition metal, an alkaline metal, an alkaline-earth metal, B, or Al) into an alkaline solution, a carbonate solution, or a hydrogencarbonate solution in any one of which a compound (e.g., manganese oxide) of a metal (Mn, Co, Ni, or the like) which is the major component of the positive plate material so as to precipitate the compound of the doping element on the major component and to cover the major component compound, mixing the major component compound covered with the doping element with a lithium compound (e.g., lithium carbonate), and firing the mixture.
摘要:
A sputtering target for producing a metallic glass membrane characterized in comprising a structure obtained by sintering atomized powder having a composition of a ternary compound system or greater with at least one or more metal elements selected from Pd, Zr, Fe, Co, Cu and Ni as its main component (component of greatest atomic %), and being an average grain size of 50µm or less. The prepared metallic glass membrane can be used as a substitute for conventional high-cost bulk metallic glass obtained by quenching of molten metal. This sputtering target for producing the metallic glass membrane is also free from problems such as defects in the metallic glass membrane and unevenness of composition, has a uniform structure, can be produced efficiently and at low cost, and does not generate many nodules or particles. Further provided is a method for manufacturing such a sputtering target for forming the metallic glass membrane.
摘要:
In a production method for producing a compound semiconductor single crystal by LEC method using a crystal growth apparatus with a double crucible structure, it was made to grow up a crystal by covering the second crucible with a plate-like member having a pass-through slot for being capable of introducing a crystal pulling-up shaft having a seed crystal holding part at a tip into the second crucible and creating a state where an atmosphere within the second crucible scarcely changes (a semi-sealed structure).
摘要:
A method of manufacturing a compound semiconductor single crystal as a first embodiment, comprising charging compound semiconductor materials into a crucible having an inverted conical increased-diameter part at the lower end thereof and a seed crystal storing part at the center of the bottom of the increased-diameter part, enclosing the crucible into a container, placing the container in a vertical heating furnace to melt the materials by heating and solidifying the obtained material molten liquid in the upward direction by gradually cooling the liquid from below, characterized in that a crystal growth speed at the increased-diameter part of the crucible is 20 mm/hr or higher at the time of the solidification. A method of manufacturing a compound semiconductor single crystal as a second embodiment, comprising placing a bottomed cylindrical crucible supported by a supporting means in a hot zone surrounded by a tubular refractory wall and an upper lid inside a high pressure container and gradually cooling a molten compound semiconductor liquid stored in the crucible from below, characterized in that a temperature fluctuation in the hot zone is reduced by inducing by a gas flow induction means a gas stream flowing form below to above around the crucible.
摘要:
Provided is an iron-based sintered body with a rustproof function comprising a layer containing 0.01 to 5at% of indium on the surface of the iron-based sintered body, or an iron-based sintered body with a rustproof function containing 0.01 to 5at% of indium throughout the sintered body, and the iron-based sintered body having iron as its principal component is manufactured by performing sintering in a gas atmosphere containing indium vapor or indium. Thereby obtained is an iron-based sintered body, as well as the manufacturing method thereof, capable of easily improving the rustproof effect without having to hardly change the conventional process.
摘要:
The invention is intended to establish means for stably producing manganese oxide high in tap density, suitable for use as a raw material for producing a positive plate material of a lithium secondary cell at high production yield and with high work efficiency. The means comprise the steps of employing a rotary kiln as a roasting furnace when producing manganese oxide by roasting of manganese carbonate, starting the roasting by supplying the manganese carbonate through a material charging port of the rotary kiln while filling up the roasting furnace with a low oxidizing atmosphere, (for example, in the atmosphere with oxygen concentration not more than 15%) and continuing the roasting of material for roasting while blowing an oxygen-containing gas (for example, a gas with oxygen concentration not less than 15%) onto the material for roasting, placed at a position inside the roasting furnace, away at a distance from the material charging port. Atmospheric temperature inside the roasting furnace is preferably kept in a range of 400 to 600°C.
摘要:
Stable supply of a cathode material for a lithium secondary battery that excels in sinterbility and composition stability and can exhibit satisfactory battery performance is accomplished by reducing to 100 ppm or less both the contents of Na and S being impurity elements in multiple oxides as materials for a cathode material for a lithium secondary battery and carbonic salts as precursor materials for the production of a cathode material for a lithium secondary battery.
摘要:
A method of electroless plating, which comprises applying a silane coupling agent having a functional group capable of capturing a metal, further applying a solution in an organic solvent of a palladium compound such as palladium chloride, and then performing an electroless plating. The method allows the preparation of a semiconductor wafer having an electroless plating layer which is thin, uniform and smooth, is formed with good adhesiveness, and further is suitable also as a seed layer. Specifically, a semiconductor wafer having a film thickness of 70 to 500 Å and an average surface roughness (Ra) of 10 to 100 Å can be prepared.