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    VERFAHREN ZUR HERSTELLUNG VON POLYETHEROLEN
    2.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON POLYETHEROLEN 审中-公开

    公开(公告)号：EP1539855A1

    公开(公告)日：2005-06-15

    申请号：EP03748004.3

    申请日：2003-09-11

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： BOHRES, Edward ,  HIBST, Hartmut ,  STÖSSER, Michael ,  RUPPEL, Raimund ,  BAUM, Eva

    IPC分类号： C08G65/26

    CPC分类号： C08G65/2645 ,  C08G65/266

    摘要： The invention relates to a method for the production of a polyetherol, wherein at least one alkylene oxide is reacted with at least one starter compound in the presence of one catalyst of general formula (I): M1p[M2qOn(OH)2(3-n)]x, The invention also relates to polyetherols produced according one inventive method and the use thereof for polyurethane synthesis, as a fuel additive or as a surfactant.

    摘要翻译： 本发明涉及一种生产聚醚醇的方法，其中至少一种烯化氧在至少一种通式（I）的催化剂存在下与至少一种起始化合物反应：M1p [M2qOn（OH）2（3- 本发明还涉及根据一种发明方法生产的聚醚醇及其在聚氨酯合成中的用途，作为燃料添加剂或作为表面活性剂。

    DMC-KATALYSATOREN, POLYETHERALKOHOLE SOWIE VERFAHREN ZU DEREN HERSTELLUNG
    5.
    发明公开
    DMC-KATALYSATOREN, POLYETHERALKOHOLE SOWIE VERFAHREN ZU DEREN HERSTELLUNG 有权
    DMC-KATALYSATOREN，聚醚醚酮SOWIE VERFAHREN ZU DEREN HERSTELLUNG

    公开(公告)号：EP1517940A1

    公开(公告)日：2005-03-30

    申请号：EP03760639.9

    申请日：2003-06-18

    申请人： BASF AKTIENGESELLSCHAFT

    发明人： BOHRES, Edward ,  FRANKE, Dirk ,  STÖSSER, Michael ,  RUPPEL, Raimund ,  BAUM, Eva ,  HARRE, Kathrin

    IPC分类号： C08G65/26 ,  B01J27/26

    CPC分类号： B01J27/26 ,  B01J37/03 ,  C08G18/4866 ,  C08G65/2663

    摘要： The invention relates to a method for producing polyether alcohols by attaching alkylene oxides to H-functional initial substances, using multimetal cyanide compounds as catalysts, characterized by the fact that the multimetal cyanide compound is produced by a method comprising the following steps: a) a metal salt solution is added to a cyano-metal solution at a specific stirring rate e ranging between 0.05 and 10 W/l, preferably between 0.4 and 4W/l, and at a temperature ranging between 0 °C and 100 °C, preferably between 20 °C and 60 °C, during an addition time lasting between 5 and 120 minutes; b) the specific stirring rate e is reduced to between 0.03 and 0.8 W/l while a surface-active substance is added; c) the solution is heated to a maximum temperature of 100 °C, preferably between 55 °C and 75 °C, while being stirred at a specific stirring rate e ranging between 0.03 and 0.8 W/l; d) an additional amount of the metal salt solution is added and stirred at a specific stirring rate e of 0.03 to 0.8 W/l; e) the solid substance is dispersed, e.g. by stirring at an increased specific stirring rate e of > 0.7 W/l or by incorporating a transfer pump circuit comprising a corresponding pump or a dissolver, when the conductivity begins dropping; f) stirring at the specific stirring rate e used in step e) until the conductivity or the pH value remains stable; g) the multimetal cyanide compound is isolated and washed with water; and h) the catalyst is optionally dried.

    摘要翻译： 本发明涉及一种通过使用多金属氰化物化合物作为催化剂将烯化氧连接到H-官能初始物质来生产聚醚醇的方法，其特征在于所述多金属氰化物化合物通过包括以下步骤的方法生产：a）a 金属盐溶液以0.05至10W / l，优选0.4至4W / l的特定搅拌速率e，并且在0℃至100℃范围内的温度下，优选在 20℃和60℃，持续5至120分钟的加料时间; b）当添加表面活性物质时，比转速e降低到0.03和0.8W / l之间; c）将溶液加热至100℃的最高温度，优选55℃至75℃，同时在范围为0.03至0.8W / l的特定搅拌速率下搅拌; d）加入额外量的金属盐溶液并在0.03至0.8W / l的特定搅拌速率e下搅拌; e）固体物质被分散，例如， 通过在提高的> 0.7W / l的特定搅拌速率e下搅拌，或者当电导率开始下降时通过结合包括相应的泵或溶解器的输送泵回路; f）在步骤e）中使用的特定搅拌速率e下搅拌直至电导率或pH值保持稳定; g）分离多金属氰化物并用水洗涤; 和h）任选地干燥催化剂。