摘要:
The invention is directed to an improvement in operation of wash columns, and more in particular to an apparatus for separating solid particles from a slurry and to a process for separating solid particles from a mother liquor slurry. The apparatus of the invention comprises a wash column (1), which comprises a melting circuit (8,10,11,21), wherein means (22,23) are present to introduce a compound or composition to said wash column between a wash front (6b) formed in said wash column in operation and a product outlet and/or in the melting circuit. The process of the invention comprises separating the liquid from the solid particles by filtration with the aid of at least one filtering element (4), while a packed bed of solid particles coming from the mother liquid slurry forms near said filtering element (4), and wherein a wash front (6b) forms which is obtained by bringing a washing liquid in counter current to the solid particles in the bed, the bed being subjected to a movement in the direction of said wash front (6b), while a product stream comprising the material of said solid particles is obtained by continuously discharging a portion of said washing liquid, wherein a portion of said bed is continuously disintegrated, characterized in that a compound or composition is introduced into said wash column (1) between the wash front (6b) and a product outlet and/or in a melting circuit (8,10,11,21), and wherein the introduction of the said compound or composition decreases the equilibrium temperature of the contents of the melting circuit (8,10,11,21), further characterized by the feature that the introduced compound or composition is completely miscible with the product suspension and/or molten product being present in the said melting circuit (8,10,11,21).
摘要:
The invention is in the field of recycling plastic waste. In particular, the invention is directed to a method separate polyolefins from plastic waste based on a dissolution/precipitation approach. The method according to the present invention may be used to separate polyolefins with a high selectivity by using at least a first and a second cooling surface. The invention is particularly suitable to at least partially separate LLDPE and LDPE or polypropylene and polyethylene from plastic waste.
摘要:
The invention is in the field of recycling plastic waste. In particular, the invention is directed to a method to separate polycarbonate and a first-component from plastic waste. In particular, the method according to the present invention may be used to efficiently separate polycarbonate and the first component with high purity and yield. The method is based on nonselective dissolution and selective precipitation.
摘要:
A rotating knife is disclosed for disintegrating a crystal bed formed in a washing column for processing suspension of solid particles in a liquid. The rotating knife is provided with a spoke support. The spoke support comprises at least two spokes. The relative angle of the spokes is between approximately 20° and approximately 80°.
摘要:
The invention is directed to a method for the preparation, in particular for the purification of 2,5-furandicarboxylic acid or a salt thereof, comprising crystallization of a 2,5-furandicarboxylic acid mono salt and then crystallizing 2,5-furandicarboxylic diacid from this mono salt. Preferably, the method is at least partially carried out in a continuous or semi-continuous manner, preferably at least partially in one or more continuous mixed-suspension mixed product removal (MSMPR) crystallizers in series.
摘要:
A wash column for processing a suspension of solid particles in a liquid comprising a bed forming chamber in which a packed bed of solid particles can be formed, filtrate extraction means for extracting liquid from the suspension as to form the packed bed of solid particles in the bed forming chamber, and a suspension supply line for supplying the suspension directly to an end of the bed forming chamber, wherein the suspension supply line ends in the bed forming chamber.
摘要:
The invention relates to a method and apparatus for processing a suspension. According to the invention, a suspension is led into a washing column in which at least one filter element is present, so that near the filtering element, a packed bed of particles forms. The bed is disintegrated under the influence of the impulse of a washing liquid, while particles from the bed are incorporated in the washing liquid.