METHOD FOR PRODUCING EPOXY COMPOUND
    2.
    发明公开
    METHOD FOR PRODUCING EPOXY COMPOUND 有权
    生产环氧化合物的方法

    公开(公告)号:EP2913331A1

    公开(公告)日:2015-09-02

    申请号:EP13849469.5

    申请日:2013-10-21

    IPC分类号: C07D405/14

    摘要: There is provided a method for producing an epoxy compound having an epoxy ring bonded to a triazinetrione ring via a long chain alkylene group, an olefin compound having a specific structure is used to efficiently obtain an epoxy compound of which an olefin moiety is epoxidized in high yield. A method for producing an epoxy compound of Formula (2):

    comprising reacting a triolefin compound of the following Formula (1):

    (In the above-mentioned Formulae, R 1 to R 9 are each independently a hydrogen atom or a methyl group; and n1 to n3 are each independently an integer of 1 to 4) with hydrogen peroxide, a nitrile compound, and an alkaline substance in a solvent. The nitrile compound is an aliphatic nitrile compound or an aromatic nitrile compound. The alkaline substance is phosphate, carbonate, or an alkaline metal hydroxide.

    摘要翻译: 本发明提供一种环氧化合物的制造方法,该环氧化合物具有通过长链亚烷基与三嗪三酮环键合的环氧环,具有特定结构的烯烃化合物用于有效地获得高烯烃部分环氧化的环氧化合物 产量。 式(2)的环氧化合物的制造方法,其特征在于,使下述式(1)表示的三烯烃化合物与上述式(1)中的R 1〜 n3各自独立地为1〜4的整数)与过氧化氢,腈化合物和碱性物质在溶剂中进行反应来制造。 腈化合物是脂族腈化合物或芳族腈化合物。 碱性物质是磷酸盐,碳酸盐或碱金属氢氧化物。

    METHOD FOR PRODUCING EPOXY COMPOUND

    公开(公告)号:EP2913331B1

    公开(公告)日:2018-09-12

    申请号:EP13849469.5

    申请日:2013-10-21

    IPC分类号: C07D405/14

    摘要: There is provided a method for producing an epoxy compound having an epoxy ring bonded to a triazinetrione ring via a long chain alkylene group, an olefin compound having a specific structure is used to efficiently obtain an epoxy compound of which an olefin moiety is epoxidized in high yield. A method for producing an epoxy compound of Formula (2): comprising reacting a triolefin compound of the following Formula (1): (In the above-mentioned Formulae, R 1 to R 9 are each independently a hydrogen atom or a methyl group; and n1 to n3 are each independently an integer of 1 to 4) with hydrogen peroxide, a nitrile compound, and an alkaline substance in a solvent. The nitrile compound is an aliphatic nitrile compound or an aromatic nitrile compound. The alkaline substance is phosphate, carbonate, or an alkaline metal hydroxide.

    HIGHLY SOLUBLE TRIS-(2,3-EPOXYPROPYL)-ISOCYANURATE AND METHOD FOR PRODUCING SAME
    5.
    发明公开
    HIGHLY SOLUBLE TRIS-(2,3-EPOXYPROPYL)-ISOCYANURATE AND METHOD FOR PRODUCING SAME 审中-公开
    HOCHLÖSLICHESTRIS-(2,3-EPOXYPROPYL)-ISOCYANURAT UND VERFAHREN ZUR HERSTELLUNG DAVON

    公开(公告)号:EP2944634A1

    公开(公告)日:2015-11-18

    申请号:EP14737645.3

    申请日:2014-01-07

    IPC分类号: C07D405/14 C08G59/32

    摘要: There is provided an epoxy composition which has difficulty in precipitating a crystal during storage, is homogeneous and can be stored for a long period; and a cured product of the composition having excellent transparency, heat resistance, and light resistance can be obtained on curing. An α-type tris-(2,3-epoxypropyl)-isocyanurate crystal comprising β-type tris-(2,3-epoxypropyl)-isocyanurate in the crystal in a ratio of 2% by mass to 15% by mass. A method for producing the α-type tris-(2,3-epoxypropyl)-isocyanurate crystal comprising step (i) separating β-type tris-(2,3-epoxypropyl)-isocyanurate contained in a tris-(2,3-epoxypropyl)-isocyanurate solution from the solution as a solid to obtain a crystal with an increased content ratio of α-type tris-(2,3-epoxypropyl)-isocyanurate.

    摘要翻译: 提供了一种在储存期间难以沉淀晶体的环氧组合物,是均匀的并且可以长时间储存​​; 并且在固化时可以获得具有优异透明性,耐热性和耐光性的组合物的固化产物。 在结晶中含有2质量%〜15质量%的2型三(2,3-环氧丙基) - 异氰脲酸酯的±型三(2,3-环氧丙基) - 异氰脲酸酯晶体。 一种制备±型三 - (2,3-环氧丙基) - 异氰脲酸酯晶体的方法,包括步骤(i)分离三 - (2,3-二氧代丙基) - 异氰脲酸酯晶体中所含的2-(2,3-环氧丙基) 环氧丙基) - 异氰脲酸酯溶液作为固体,得到具有增加的±型三 - (2,3-环氧丙基) - 异氰脲酸酯的含量比的晶体。