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公开(公告)号：EP2791098A1
公开(公告)日：2014-10-22
申请号：EP12808776.4
申请日：2012-12-13
申请人： Rhodia Operations
IPC分类号： C07C45/00 , C07C47/565
CPC分类号： C07C45/80 , C07C47/565 , C07C47/58
摘要： A method is described for purifying vanillin, and derivatives thereof, from a solution of vanillin or of a vanillin derivative in a solvent S1 containing impurities, comprising the following steps: a) a step of evaporating the solvent S1 in the presence of water so as to obtain an aqueous solution of vanillin or of a vanillin derivative; b) a step of liquid/liquid extraction by bringing the aqueous solution obtained at the end of step a) into contact with a solvent S2, at a pH of greater than 8 and less than 10, so as to obtain an organic phase and an aqueous phase containing vanillin or a vanillin derivative and residual solvent S2; c) a step of precipitating, at a pH between 4 and 7.5, the vanillin contained in the aqueous phase obtained at the end of step b), and d) a step of isolating the vanillin or a derivative thereof.
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2.发明授权PROCEDE DE PURIFICATION DE LA VANILLINE PAR EXTRACTION LIQUIDE-LIQUIDE 有权VERFAHREN ZUR REINIGUNG VON VANILLIN DURCHFLÜSSIG-FLÜSSIG-EXTRAKTION
公开(公告)号：EP2791098B1
公开(公告)日：2017-04-19
申请号：EP12808776.4
申请日：2012-12-13
申请人： Rhodia Operations
CPC分类号： C07C45/80 , C07C47/565 , C07C47/58
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3.发明授权NOUVELLE UTILISATION D'UN COMPOSÉ DE VANILLINE ET D'ÉTHYLVANILLINE DANS UN PRODUIT ALIMENTAIRE 有权在EINEM LEBENSMITTELPRODUKT中，VERWENDUNG EINER VERBINDUNG AUS VANILLIN在ETHYLVANILLIN
公开(公告)号：EP2833737B1
公开(公告)日：2016-01-06
申请号：EP13712814.6
申请日：2013-03-28
申请人： Rhodia Operations
发明人： GIANNOTTA, Dominique , COCHENNEC, Corine , COLAS DES FRANCS, Tristan , BODIN, Sandrine , BARLET, Bernard
CPC分类号： A21D13/08 , A21D2/14 , A21D13/50 , A21D13/80 , A23G1/32 , A23G3/346 , A23G3/36 , A23K20/111 , A23L27/204 , A23L27/88 , A23V2002/00 , A23G2200/00
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4.发明公开
公开(公告)号：EP2747582A1
公开(公告)日：2014-07-02
申请号：EP12743467.8
申请日：2012-08-07
申请人： Rhodia Operations
CPC分类号： A23P10/20 , A23L27/20 , A23L27/204 , C07B2200/13 , C07C47/58
摘要： The invention relates to a method for preparing an aromatic powder composition having a melting temperature Tf, including: i) feeding at least two basic powder solids having organoleptic properties into a mixer, the enclosure of which has been preheated to a temperature T lower than Tf, said solids being separately fed into said mixer; ii) mixing said solids in said mixer, in the absence of any outside liquid phase, at a temperature T lower than temperature Tf, at least one of said basic powder solids being fed into said mixer at a temperature Ti, such that the mixing occurs under isothermal conditions at a temperature set at said temperature T; and iii) recovering said aromatic powder composition. Said method is particularly suitable for preparing a composition essentially including a vanillin and ethylvanillin compound.
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5.发明授权
公开(公告)号：EP2747582B1
公开(公告)日：2016-12-21
申请号：EP12743467.8
申请日：2012-08-07
申请人： Rhodia Operations
CPC分类号： A23P10/20 , A23L27/20 , A23L27/204 , C07B2200/13 , C07C47/58
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公开(公告)号：EP2763947B1
公开(公告)日：2016-02-10
申请号：EP12768852.1
申请日：2012-10-05
申请人： Rhodia Operations
IPC分类号： C07C45/64 , C07C47/575
CPC分类号： C07C45/64 , C07C47/575
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7.发明公开NOUVELLE UTILISATION D'UN COMPOSÉ DE VANILLINE ET D'ÉTHYLVANILLINE DANS UN PRODUIT ALIMENTAIRE 有权甲链路从香兰素和乙基香草醛在食品中的新用途
公开(公告)号：EP2833737A1
公开(公告)日：2015-02-11
申请号：EP13712814.6
申请日：2013-03-28
申请人： Rhodia Operations
发明人： GIANNOTTA, Dominique , COCHENNEC, Corine , COLAS DES FRANCS, Tristan , BODIN, Sandrine , BARLET, Bernard
CPC分类号： A21D13/08 , A21D2/14 , A21D13/50 , A21D13/80 , A23G1/32 , A23G3/346 , A23G3/36 , A23K20/111 , A23L27/204 , A23L27/88 , A23V2002/00 , A23G2200/00
摘要： The present invention concerns a new use for a compound of vanillin and ethyl vanillin, in a food product and more particularly in a food product with a reduced fat and/or sugar content. The present invention also concerns food compositions comprising said compound of vanillin and ethyl vanillin.
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8.发明公开
公开(公告)号：EP2763947A1
公开(公告)日：2014-08-13
申请号：EP12768852.1
申请日：2012-10-05
申请人： Rhodia Operations
IPC分类号： C07C45/64 , C07C47/575
CPC分类号： C07C45/64 , C07C47/575
摘要： The present invention relates to a method for preparing a compound of formula (I), comprising the reaction of vanillin and vanillyl alcohol in the presence of a base.
摘要翻译： 本发明涉及制备式（I）化合物的方法，其包括香草醛和香草醇在碱存在下反应。
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