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    SYNTHESIS OF AMONNIUM DINITRAMIDE, ADN
    1.
    发明公开
    SYNTHESIS OF AMONNIUM DINITRAMIDE, ADN 审中-公开
    合成蛋黄（ADN）

    公开(公告)号：EP3099652A1

    公开(公告)日：2016-12-07

    申请号：EP15743454.9

    申请日：2015-01-29

    申请人： Totalförsvarets Forskningsinstitut

    发明人： EK, Stefan ,  SKARSTIND, Martin ,  LATYPOV, Nikolaj ,  SKIFS, Henrik ,  JOHANSSON, Jonas

    IPC分类号： C06B25/34 ,  C01B21/082

    CPC分类号： C01B21/087 ,  B01D15/20 ,  B01D15/22 ,  B01J20/20 ,  B01J2220/52

    摘要： The invention concerns a method for making ADN from GUDN in one single process step. GUDN is reacted with an ammonium source (ammonium- sulfamate, ammonium-sulfate) and an ion-change gives ADN from GUDN in one process stage. The advantages are that the process gives pure ADN without potassium contaminants and that a smaller amount of solvent is necessary. GUDN and the ammonium source are heated together with water until everything is solved into a solution. Thereafter, an alcohol is added and the precipitate formed is filtered off. The filtrate is concentrated and the residue is suspended in an alcohol. The precipitate is filtered off and ADN is obtained by concentrating the filtrate. An alternative is to, after adding the alcohol, partially concentrate the then formed mixture. The filtering off of the particles from this mixture yields a solution of ADN in alcohol. Evaporation of this solution yields clean ADN after only one filtering stage. Ammonia can also be used as a source of ammonium. GUDN is then dissolved in ammonia where after then formed ammonium-dinitramide and guanylurea are separated through separation on a column filled with active carbon. The eluted solution is concentrated until dry which yields ADN. GUDN can also be reacted with ammonium-sulfate in alcohol creating a precipitate which is filtered off. The filtrate is concentrated and the remainder is suspended in alcohol. The un-soluted particles are filtered off and ADN is obtained through concentrating

    摘要翻译： 本发明涉及在一个单一过程步骤中从GUDN制备ADN的方法。 GUDN与铵反应。 来源（氨基磺酸铵，硫酸铵，氨）和离子交换在一个工艺阶段从GUDN得到ADN。 其优点是该方法产生纯的不含钾污染物的纯ADN，并且需要较少量的溶剂。