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    POLYMERIC MATERIALS
    2.
    发明公开
    POLYMERIC MATERIALS 审中-公开

    公开(公告)号：EP3502163A1

    公开(公告)日：2019-06-26

    申请号：EP19152608.6

    申请日：2014-06-25

    申请人： Victrex Manufacturing Limited

    发明人： WILSON, Brian ,  CHAPLIN, Adam ,  MATTHEWS, Alice Victoria Mary ,  BEARDSALL, Carlie Ann ,  AINSWORTH, Richard Luke ,  CAPRA, Carlo

    IPC分类号： C08G65/40 ,  C08K3/04 ,  C08K7/06 ,  C08K7/14 ,  C08L71/12 ,  C08L101/04

    摘要： A polymeric material having a repeat unit of formula

             -O-Ph-O-Ph-CO-Ph-     I

    and a repeat unit of formula

             -O-Ph-Ph-O-Ph-CO-Ph-     II

    wherein Ph represents a phenylene moiety;
    wherein the repeat units I and II are in the relative molar properties I:II of from 65:35 to 95:5;
    wherein the polymer material has a crystallinity of at least 25% measured by differential scanning calorimetry as described in Example 31.
    A process for the production of a polymeric material having a repeat unit of formula

             -O-Ph-O-Ph-CO-Ph-     I

    and a repeat unit of formula

             -O-Ph-Ph-O-Ph-CO-Ph-     II

    wherein Ph represents a phenylene moiety, said process comprising polycondensing a mixture of at least one dihydroxybenzene compound and at least one dihydroxybiphenyl compound in the molar proportions 65:35 to 95:5 with at least one dihalobenzophenone in the presence of sodium carbonate and potassium carbonate wherein:
    (i) the mole% of said potassium carbonate is at least 2.5 and/or
    (ii) the following relationship (referred to as the "D50/mole% relationship") applies the D 50 of said sodium carbonate in µm mole % of potassium carbonate = 46.

    POLYMERIC MATERIALS
    4.
    发明公开
    POLYMERIC MATERIALS 审中-公开
    聚合物材料

    公开(公告)号：EP3013888A1

    公开(公告)日：2016-05-04

    申请号：EP14737311.2

    申请日：2014-06-25

    申请人： Victrex Manufacturing Limited

    发明人： WILSON, Brian ,  CHAPLIN, Adam ,  MATTHEWS, Alice Victoria Mary ,  BEARDSALL, Carlie Ann ,  AINSWORTH, Richard Luke ,  CAPRA, Carlo

    IPC分类号： C08G65/40

    CPC分类号： C08G65/4012 ,  C08G65/40 ,  C08G65/4087 ,  C08G65/4093 ,  C08G2650/40 ,  C08K3/04 ,  C08K7/06 ,  C08K7/14 ,  C08L71/12 ,  C08L101/04 ,  C08L27/12

    摘要： A polymeric material has a repeat unit of formula —O-Ph-O-Ph-CO-Ph- I and a repeat unit of formula —O-Ph-Ph-O-Ph-CO-Ph- II wherein Ph represents a phenylene moiety; wherein the repeat units I and II are in the relative molar properties I:II of from 65:35 to 95:5; wherein log10 (X %)>1.50−0.26 MV; wherein X % refers to the % crystallinity measured as described in Example 31 and MV refers to the melt viscosity measured as described in Example 30. A process for making the polymeric material comprises polycondensing a mixture of at least one dihydroxybenzene compound and at least one dihydroxybiphenyl compound in the molar proportions 65:35 to 95:5 with at least one dihalobenzophenone in the presence of sodium carbonate and potassium carbonate wherein: (i) the mole % of said potassium carbonate is at least 2.5 and/or (ii) the following relationship applies (formula III).

    摘要翻译： 聚合物材料具有式-O-Ph-O-Ph-CO-Ph-I的重复单元和式-O-Ph-Ph-O-Ph-CO-Ph-II的重复单元，其中Ph表示亚苯基 部分; 其中重复单元I和II的相对摩尔性质I:II为65:35至95:5; 其中log10（X％）> 1.50-0.26MV; 其中X％是指如实施例31中所述测量的％结晶度，MV是指如实施例30中所述测量的熔体粘度。制备聚合物材料的方法包括缩聚至少一种二羟基苯化合物和至少一种二羟基联苯 化合物以摩尔比65:35至95:5与至少一种二卤代二苯甲酮在碳酸钠和碳酸钾存在下反应，其中：（i）所述碳酸钾的摩尔％至少为2.5和/或（ii）以下 关系适用（公式三）。

    POLYMERIC MATERIALS
    5.
    发明公开
    POLYMERIC MATERIALS 审中-公开

    公开(公告)号：EP3828223A1

    公开(公告)日：2021-06-02

    申请号：EP20216941.3

    申请日：2014-06-25

    申请人： Victrex Manufacturing Limited

    发明人： WILSON, Brian ,  CHAPLIN, Adam ,  MATTHEWS, Alice Victoria Mary ,  BEARDSALL, Carlie Ann ,  AINSWORTH, Richard Luke ,  CAPRA, Carlo

    IPC分类号： C08G65/40 ,  C08K3/04 ,  C08K7/06 ,  C08K7/14 ,  C08L71/12 ,  C08L101/04

    摘要： A polymeric material in the form of granules or pellets, having a repeat unit of formula

             -O-Ph-O-Ph-CO-Ph-     I

    and a repeat unit of formula

             -O-Ph-Ph-O-Ph-CO-Ph-     II

    wherein Ph represents a phenylene moiety;
    wherein the repeat units I and II are in the relative molar properties I:II of from 65:35 to 95:5; wherein the polymer material has a crystallinity of at least 25% measured by differential scanning calorimetry as described in Example 31.
    A process for the production of a polymeric material having a repeat unit of formula

             -O-Ph-O-Ph-CO-Ph-     I

    and a repeat unit of formula

             -O-Ph-Ph-O-Ph-CO-Ph-     II

    wherein Ph represents a phenylene moiety, said process comprising polycondensing a mixture of at least one dihydroxybenzene compound and at least one dihydroxybiphenyl compound in the molar proportions 65:35 to 95:5 with at least one dihalobenzophenone in the presence of sodium carbonate and potassium carbonate wherein:
    (i) the mole% of said potassium carbonate is at least 2.5 and less than 5% and/or
    (ii) the following relationship (referred to as the "D50/mole% relationship") applies
    the D 50 of said sodium carbonate in µm mole % of potassium carbonate = 46.

    POLYMERIC MATERIALS
    7.
    发明公开
    POLYMERIC MATERIALS 有权
    聚合物材料

    公开(公告)号：EP3110613A1

    公开(公告)日：2017-01-04

    申请号：EP15705068.3

    申请日：2015-02-13

    申请人： Victrex Manufacturing Limited

    发明人： CHAPLIN, Adam ,  WOOD, Alan ,  MATTHEWS, Alice Victoria Mary

    IPC分类号： B29C67/00 ,  C08G65/40

    CPC分类号： B29C67/0077 ,  B29C64/153 ,  B29C64/35 ,  B33Y10/00 ,  B33Y30/00 ,  B33Y70/00 ,  C08G65/4012 ,  C08G2650/40 ,  C08L71/00

    摘要： A process for manufacturing an object by sintering comprises: (i) selecting a powder comprising a polymeric material having a repeat unit of formula -O-Ph-O-Ph-CO-Ph-, and a repeat unit of formula -O-Ph-Ph-O-Ph-CO-Ph- wherein Ph represents a phenylene moiety; and (ii) selectively sintering the powder to produce the object. The polymer used can be advantageously recycled and blended with virgin material to produce a blend which has very similar mechanical properties and crystallinity compared to the virgin material. In preferable embodiments the Ph- moiety is linked via para positions on the ring. Preferably the sintering is laser sintering.

    摘要翻译： 通过激光烧结制造物体的方法包括：（i）选择包含具有式-O-Ph-O-Ph-CO-Ph-I重复单元和式-O的重复单元的聚合材料的粉末 Ph-Ph-O-Ph-CO-Ph-II其中Ph代表亚苯基部分; 和（ii）选择性地烧结粉末以产生物体。 发现使用的聚合物可以有利地再循环并与原始材料共混以产生与原始材料相比具有非常相似的机械性能和结晶度的共混物。 因此，聚合物可以成本有效地用于激光烧结。