摘要:
The present invention discloses the device and method for continuously preparing high-purity AKD without solvent. The adopted device includes a kind of reactor which could make continuous mixing reaction of raw materials. The main preparation process is: firstly, the tertiary amine is continuously fed into the reactor from starting end and the acyl chloride is continuously fed from three to ten line; secondly, under the operating state of reactor, the main motor drives the internal cylinder to rotate in relation to external cylinder, forcing the fed materials to be conveyed and stirred by blades in the conveying section of annular column passage and forcing the fed materials to be sheared and mixed by relative movement of shearing blades and kneading blades at mixing section. Due to alternate arrangement of conveying section and mixing section along the axial direction of annular column passage, it causes the sufficient reaction of fed materials and controls the material temperature through internal and external heat exchange systems until the reaction products are discharged continuously from outlet. The device and process adopted by the present invention could realize the disperse generation of reaction heat and sufficient material mixture and complete reaction to make it easy to control the reaction temperature and material viscosity and decrease the generation of side reaction to ensure the high purity of products.
摘要:
A combined reactor and condenser for the synthesis of urea from ammonia and carbon dioxide, including a condenser section coupled to a reaction section, comprising inputs directed to said condenser section for a gaseous stream comprising ammonia and carbon dioxide and for a solution containing ammonium carbamate and liquid ammonia, and wherein the effluent of the condenser section is sent to the reaction section; the reaction section comprises a plurality of compartments and a plurality of mixers, at least one inside each of said compartments.
摘要:
The invention relates to a hydrocarbon conversion process and a reactor configured to carry out the hydrocarbon conversion process. The hydrocarbon conversion process is directed to increasing the overall equilibrium production of ethylene from typical pyrolysis reactions. The hydrocarbon conversion process can be carried out by exposing a hydrocarbon feed to a peak pyrolysis gas temperature in a reaction zone in the range of from 850°C to 1200°C.
摘要:
A combined reactor and condenser for the synthesis of urea from ammonia and carbon dioxide, including a condenser section coupled to a reaction section, comprising inputs directed to said condenser section for a gaseous stream comprising ammonia and carbon dioxide and for a solution containing ammonium carbamate and liquid ammonia, and wherein the effluent of the condenser section is sent to the reaction section; the reaction section comprises a plurality of compartments and a plurality of mixers, at least one inside each of said compartments.
摘要:
In a catalytic reactor including catalyst carriers inserted into a plurality of channels defined by corrugated fins, the corrugated fins include a first corrugated fin, and a second corrugated fin arranged to adjoin the first corrugated fin. When viewed from the first corrugated fin toward the second corrugated fin along the channels, at least a portion of side walls of the second corrugated fin is located between two adjacent ones of side walls of the first corrugated fin at adjoining end faces of the first and second corrugated fins.
摘要:
The invention relates to a method for the continuous esterification of halogen silanes of the formula (I) with alcohols of the formula (II) to obtain silane esters of the formula (III) in a single column (1): R 1 a SIHal b (I), R 2- (OH) (II), R 1 a Si-(OR 2 ) b (III). The method is characterized by the steps: i) feeding the halogen silane (I) in liquid form into the upper third of the column (1) [line (6)]; ii) feeding a major portion of the alcohol (II) in liquid form into the upper third of the column (1) [line (7)]; iii) feeding the remaining alcohol (II) in liquid form into the lower third of the column [by way of line (8)]. The hydrogen chloride formed during the reaction is discharged via the head of the column, the esterification product is discharged from the bottom of the column. The invention further relates to a column (1) for the continuous esterification of halogen silanes having the following characteristics: lines (6), (7), and (8) as described above, and furthermore, a rotating evaporator (3) in the lower third of the column, and a line (8) for discharging the hydrogen halide via the head of the column, and a line (10) for discharging the esterification product from the bottom of the column.
摘要:
In a catalytic reactor including catalyst carriers inserted into a plurality of channels defined by corrugated fins, the corrugated fins include a first corrugated fin, and a second corrugated fin arranged to adjoin the first corrugated fin. When viewed from the first corrugated fin toward the second corrugated fin along the channels, at least a portion of side walls of the second corrugated fin is located between two adjacent ones of side walls of the first corrugated fin at adjoining end faces of the first and second corrugated fins.
摘要:
Bei einem Verfahren zur Behandlung eines Dispersionsmaterials in einem Plasma, bei dem ein plasmabildendes Gas in eine Reaktionskammer eingeleitet und ionisiert wird und ein Dispersionsmaterial in die Reaktionskammer und in den Bereich des Plasmas eingeleitet, unter Einwirkung des Plasmas behandelt und anschließend aus dem Bereich des Plasmas entnommen wird, wird vorgeschlagen, dass die Einleitung des plasmabildenden Gases und die Einleitung des Dispersionsmaterials unabhängig voneinander und aus unterschiedlichen Richtungen erfolgen. Bei einer Vorrichtung zur Behandlung eines Dispersionsmaterials in einem Plasma, die eine Reaktionskammer mit einem Plasmagenerator umfasst, der einen ersten Einlass für ein plasmabildendes Gas aufweist, und die mit einem zweiten Einlass für das Dispersionsmaterial versehen ist, wird vorgeschlagen, dass der zweite Einlass relativ zum ersten Einlass räumlich getrennt so angeordnet ist, dass das Dispersionsmaterial von außen in das Plasma geleitet wird.
摘要:
The invention relates to a kneader mixer comprising at least two shafts (2, 3) that are embodied as hollow shafts, on the surfaces of which kneading bars (4) are disposed on webs (5). The design of the shafts is selected such that the eigenfrequencies of the shafts are provided with a distance of at least 5 percent from the excitation frequencies. At least one of the shafts is preferably penetrated by a tempering medium, the inlet being located at one end and the outlet at the other end of the shaft. Preferably, the inventive kneader mixer further comprises at least one opening above the shafts, said opening being configured as a dome that is closed by means of a displacer (22). At least one opening for removing product is also provided. The cross section of said opening can be adjusted during operation.
摘要:
Die Erfindung beschreibt eine Rührvorrichtung wenigstens bestehend aus einem Begasungsrührer (12) und einem Flüssigmischer (13) oder zwei Flüssigmischern, welche auf einer Welle (11) angeordnet sind und jeweils eine Zuführung (17, 16) und wenigstens eine Austrittsöffnung (14, 15) aufweisen, wobei die Austrittsöffnungen (14, 15) des Begasungsrührers (12) und des Flüssigmischers (13) oder der Flüssigmischer in einem Abstand zueinander stehen, wobei das Verhältnis a/d von Abstand a der Austrittsöffnungen (14, 15) zu Durchmesser d des Begasungsrührers (12) oder Flüssigmischers (13) 0,02 bis 0,5 und das Verhältnis b/d von Abstand b der Außenkanten zu Durchmesser d des Begasungsrührers (12) oder Flüssigmischers (13) 0,01 bis 0,4 beträgt.