摘要:
The instant invention relates to a process allowing the encapsulation of a polymerization accelerator, said process comprising the steps of: a) providing an reverse emulsion containing, in an oil phase, a water solution/dispersion containing the polymerisation activator, the oil phase including a heat curable mixture of an isocyanate and a polyalkyldiene hydroxylated or polyol, b) pouring the reverse emulsion in a water phase to make a multiple emulsion water/oil/water, containing drops of activators as the internal water phase, and then, c) heating the multiple emulsion obtained in step b) at a temperature of between 50 and 95°C, in order to cure the polyisocyanate in polyurethane and obtain drops of activator enclosed in shells of polyurethane dispersed in water. The invention also relates to aqueous gelling systems comprising the encapsulated polymerization accelerator with water soluble or dispersable monomers and a polymerization initiator dispersed in said monomers, usefull i.a. for sealing subterranean environments or consolidation of a soil or sealing of a subterranean structure.
摘要:
A method of treating a formation that includes injecting gelling components curable by a moisture cure into a selected region of the formation; and controlling the onset of curing of the gelling components by contacting the gelling components with a drying agent is disclosed.
摘要:
The instant invention relates to a process for the encapsulation of a non-amine hydrophilic compound C, comprising the steps of: (E1) providing a reverse emulsion containing : - an oil phase (O), comprising a curable mixture of isocyanate and polyalkyldiene hydroxylated or polyol - dispersed in said oil phase, drops of an aqueous phase W 1 , containing : ˆ˜ said non-amine hydrophilic compound C ; and ˆ˜ at least 5% by weight of a compound C' carrying more than 2 amine groups ; ˆ˜€ƒ (E2) pouring the reverse emulsion of step (E1) in a second water phase W 2 to make a multiple emulsion water/oil/water ; and, then, (E3) curing into polyurethane all or part of the curable mixture contained in the oil phase.
摘要:
Viscosifying compositions having reduced toxicity are used in treatment fluids in subterranean operations; methods include providing such treatment fluids including a viscosifying composition and an aqueous base fluid, the viscosifying composition including hydroxyethyl cellulose, about 10% to about 60% by weight of 2-pyrrolidone, and about 10% to about 60% by weight of a water soluble monoalkyl ether of propylene glycol having substantially no swelling effect on the hydroxyethyl cellulose, wherein a weight ratio of hydroxyethyl cellulose to 2-pyrrolidone is in a range from about 1:2 to about 2.6:1 and the method including placing the treatment fluid in a subterranean formation.
摘要:
A method of treating a carbonate hydrocarbon-bearing formation is disclosed. The method includes contacting the hydrocarbon-bearing formation with a composition comprising solvent and a fluorinated amine oxide. Carbonate hydrocarbon-bearing formations treated according to the method are also disclosed.
摘要:
A method of treating a formation that includes injecting gelling components curable by a moisture cure into a selected region of the formation; and controlling the onset of curing of the gelling components by contacting the gelling components with a drying agent is disclosed.
摘要:
Method of treating a portion of a subterranean formation comprising: placing a prepad fluid into a portion of a subterranean formation wherein the pre-pad fluid comprises a low-viscosity aqueous tackifying composition that comprises an aqueous tackifier compound and an aqueous fluid; placing a fracturing fluid into the portion of the subterranean formation at a pressure sufficient to create or extend at least one fracture therein; and, activating the aqueous tackifier compound with an activator so as to consolidate the unconsolidated particulates. Method of consolidating unconsolidated particulates within a portion of a subterranean formation comprising: placing a foamed low-viscosity aqueous tackifying composition into a portion of a subterranean formation comprising unconsolidated particulates wherein the aqueous tackifying composition comprises an aqueous fluid, a foaming agent, and an aqueous tackifier compound; and, activating the aqueous tackifier compound with an activator so as to consolidate the unconsolidated particulates.