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    METHOD FOR PREPARING ADAMANTYLTRIMETHYLAMMONIUM HYDROXIDE, AND AQUEOUS QUATERNARY AMMONIUM BASE SOLUTION PREPARED THEREBY
    1.
    发明公开
    METHOD FOR PREPARING ADAMANTYLTRIMETHYLAMMONIUM HYDROXIDE, AND AQUEOUS QUATERNARY AMMONIUM BASE SOLUTION PREPARED THEREBY 审中-公开

    公开(公告)号：EP4137476A1

    公开(公告)日：2023-02-22

    申请号：EP21904615.8

    申请日：2021-07-15

    申请人： Kente Catalysts Inc.

    发明人： WU, Jianping ,  XIANG, Feiyong ,  LU, Jinyin ,  HUANG, Xiaodong ,  PAN, Qunyang ,  SHI, Xusheng ,  PAN, Xiaochu

    IPC分类号： C07C209/68 ,  C07C211/62 ,  C07C209/00 ,  C07C68/06 ,  C07C69/96

    摘要： Disclosed are a preparation method of adamantyltrimethylammonium hydroxide, and an aqueous quaternary ammonium base solution prepared from the same, relating to the technical field of molecular sieve template agent production. The preparation method comprises the following steps of: S1, salification: weighing dimethyladamantanamine, adding dimethyl carbonate, evenly mixing the mixture to prepare a quaternized mixture, and under a helium sealing atmosphere, heating the quaternized mixture to 135°C to 150°C for reaction for no less than 6 hours to obtain an adamantyltrimethylammonium carbonate monomethyl ester salt; and S2, hydrolysis: dissolving the adamantyltrimethylammonium carbonate monomethyl ester salt into water, adding calcium hydroxide, blowing nitrogen from a lower part of a liquid level, heating the mixture until a boiling state is reached, simultaneously removing a byproduct methanol to form the adamantyltrimethylammonium hydroxide, and recovering a product to prepare the aqueous quaternary ammonium base solution. The preparation method of the adamantytrimethylammonium hydroxide disclosed by the invention has the advantage that an impurity content can be reduced.

    PROCESS FOR PREPARATION OF TERTIARY ALKYL PRIMARY AMINES
    10.
    发明公开
    PROCESS FOR PREPARATION OF TERTIARY ALKYL PRIMARY AMINES 有权
    VERFAHREN ZUR HERSTELLUNG VONPRIMÄRENTERTIÄRALKYLAMINEN

    公开(公告)号：EP2953924A2

    公开(公告)日：2015-12-16

    申请号：EP14726808.0

    申请日：2014-04-02

    申请人： Dow Global Technologies LLC ,  Rohm and Haas Company

    发明人： CHHEDA, Bharati D. ,  PENDERGAST, John G. ,  RANGAVAJJULA, Sivam ,  TRAUTH, Daniel M.

    IPC分类号： C07C209/00 ,  C07C209/60

    CPC分类号： C07C209/62 ,  C07C209/44 ,  C07C211/07

    摘要： A method for producing an amine. The first step is contacting a cyanide, an acid, water and a substrate compound capable of generating a carbonium ion by reaction with the acid to generate a first reaction intermediate. The second step is contacting the first reaction intermediate with water to form a second reaction intermediate. The third step is removing cyanide present in the second reaction intermediate to a concentration less than 10 ppm. The fourth step is contacting the second reaction intermediate with an alkali metal hydroxide to form the amine

    摘要翻译： 一种制备胺的方法。 第一步是使氰化物，酸，水和能与酸反应产生碳鎓离子的底物化合物接触，生成第一反应中间体。 第二步是使第一反应中间体与水接触以形成第二反应中间体。 第三步是将第二反应中间体中存在的氰化物除去至少于10ppm的浓度。 第四步是使第二反应中间体与碱金属氢氧化物接触以形成胺。