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公开(公告)号：JPH04290834A
公开(公告)日：1992-10-15
申请号：JP8082991
申请日：1991-03-19
IPC分类号： B01J27/128 , B01J31/12 , C07B37/04 , C07B61/00 , C07C49/76 , C07C63/04 , C07C69/738 , C07C69/76 , C07C253/30 , C07C255/40 , C07C255/41 , C07D307/00 , C07D333/00
摘要： PURPOSE:To monoalkylate an aryl-substituted active methylene compound containing an electron attractive group at the m-position of phenyl group by using an inexpensively obtainable aldehyde. CONSTITUTION:A compound shown by formula I [R is COOH, COOR or COR ; R is 1-6C alkyl; R is 1-10C alkyl or phenyl, 1-naphthyl, 2-naphthyl, 2-thienyl, 3-thienyl, 2-furyl or 3-furyl which may contain substituent group (halogen, 1-4C alkyl or 1-4C alkoxy); Z is COR , benzoyl, furoyl, thenoyl or CN; R is 1-2C alkyl or 1-4C alkoxy] is reacted with a compound shown by the formula R CHO [R is H, 1-8C alkyl, phenyl, naphthyl, phenyl-(1-4C alkyl), 2-thienyl, 3-thienyl, 2-furyl or 3-furyl] and a synthesis gas in the presence of a metallic catalyst of group VIII of the periodic table to industrially and advantageously give a compound shown by formula II useful for producing fine chemicals such as medicines and agricultural chemicals.
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公开(公告)号：JPH06306181A
公开(公告)日：1994-11-01
申请号：JP5210293
申请日：1993-03-12
发明人： HIRAGA TAKASHI , MORIYA TETSUO , TANAKA NORIO
摘要： PURPOSE:To obtain the film having a controlled fine structure at a lower temperature without causing the heat decomposition of optical material by spraying a solution or dispersion of an organic optical material into a high-vacuum vessel, depositing the material on a substrate, and heating the deposit. CONSTITUTION:A vacuum vessel 3 is drawn through a vacuum pump 4 to a high vacuum of 1X10 mmHg or below. A solution or dispersion of an organic optical material held in a liquid reservoir 18 is sprayed into the vessel 3 through an open/shut mechanism 2 and a control nozzle part 1 to deposit the material on a substrate 19. A substrate heater 20 is energized to heat the substrate 19, and the vapor of the solvent, etc., are trapped with a cold trap 6. After confirming that the volatile component has been completely removed from the deposit by means of a gate valve 11, an ionization apparatus 12 and a mass spectrograph 13, the deposit is optionally formed under pressure.
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公开(公告)号：JPH06263885A
公开(公告)日：1994-09-20
申请号：JP5210493
申请日：1993-03-12
发明人： HIRAGA TAKASHI , MORIYA TETSUO , TANAKA NORIO
摘要： PURPOSE:To produce a high-quality optical material by molding even from a difficultly vaporizable material, an easily heat-decomsable material or the like. CONSTITUTION:This molding process comprises mixing a solution prepared by dissolving a plurality of organic optical materials in a good solvent common to them with a poor solvent compatible to the good solvent and common to the materials to form a precipitate, filtering off the obtained precipitate, vacuum-drying the cake, grinding the dried product, heat-treating the powder in a vacuum and melt-molding the powder in a vacuum.
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公开(公告)号：JP2001026884A
公开(公告)日：2001-01-30
申请号：JP20111399
申请日：1999-07-15
申请人： DAINICHISEIKA COLOR CHEM , AGENCY IND SCIENCE TECHN , HIRAGA TAKASHI , MORIYA TETSUO , VICTOR COMPANY OF JAPAN
发明人： TANAKA NORIO , YANAGIMOTO HIROMITSU , HIRAGA TAKASHI , MORIYA TETSUO , CHIN KEIEI , TOMINAGA JUNJI , ATODA NOBUFUMI , UENO ICHIRO , TSUJITA KOJI
摘要： PROBLEM TO BE SOLVED: To modify the surface layer compsn. of the object to be coated by a sublimable substance to be interacted with it and to obtain a functional thin film having uniform film thickness and compsn. SOLUTION: As to the method for modifying a surface layer, the surface layer compsn. 1 of the object to be coated and a sublimable substance 2 to be interacted with it are placed in a closed space, moreover, the state of the inside of the space is made into the one of saturated subliming pressure of the sublimable substance 2, the vapor of the sublimable substance 2 is adhered to the surface layer compsn. 1 on the surface of the object to be coated, the adhered sublimable substance 2 is moreover infiltrated and dispersed from the surface of the surface layer compsn. 1 to the inside of the surface layer and is interacted with the surface layer compsn. 1.
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公开(公告)号：JP2000256877A
公开(公告)日：2000-09-19
申请号：JP6138099
申请日：1999-03-09
申请人： AGENCY IND SCIENCE TECHN , HIRAGA TAKASHI , MORIYA TETSUO , DAINICHISEIKA COLOR CHEM , VICTOR COMPANY OF JAPAN
发明人： HIRAGA TAKASHI , MORIYA TETSUO , CHIN KEIEI , TOMINAGA JUNJI , ATODA NOBUFUMI , TANAKA NORIO , YANAGIMOTO HIROMITSU , UENO ICHIRO , TSUJITA KOJI
IPC分类号： C23C14/12 , A61K9/00 , B29C71/00 , B29K101/00 , C08J7/06 , C08L101/00 , C23C26/00 , D06M23/00 , G02B6/00
摘要： PROBLEM TO BE SOLVED: To uniformly infiltrate and disperse the surface of a resin molding with an organic compd. having affinity with the resin and also having sublimability. SOLUTION: A resin molding and a sublimable organic compd. having affinity with the resin are charged to a sealed type vessel, the pressure and temp. at the inside are controlled, and it is placed in the saturated sublimating pressure state of the organic compd., by which the organic compd. vapor is uniformly deposited on the surface of the resin molding and is furthermore infiltrated and dispersed to the inside.
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公开(公告)号：JP2000185950A
公开(公告)日：2000-07-04
申请号：JP36644098
申请日：1998-12-24
发明人： HIRAGA TAKASHI , CHIN KUNIE , MORIYA TETSUO , TANAKA NORIO , YANAGIMOTO HIROMITSU , UENO ICHIRO , TSUJITA KOJI
摘要： PROBLEM TO BE SOLVED: To provide a stacked optical thin film having reduced light scattering, high durability and higher performance by making a sublimable, crystalline organic compound exist as an amorphous compound, a microcrystalline one or solid solution. SOLUTION: When this stacked optical thin film is produced by putting the powder or film of a meltable organic compound between the substrate surface deposited with a sublimable organic compound and the second substrate, by melting the meltable organic compound under a vacuum and heated condition and then by subjecting two substrates to compression bonding, the sublimable organic compound is in at least one kind selected from following states: (1) an amorphous state; (2) a microcrystalline state where the diameter of a crystal grain doesn't exceed one fifth times the wavelength of light applied to the stacked optical thin film; (3) solid solution where the meltable organic compound is adopted as medium.
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7.发明专利
公开(公告)号：JP2000171840A
公开(公告)日：2000-06-23
申请号：JP35842998
申请日：1998-12-02
发明人： HIRAGA TAKASHI , CHIN KUNIE , MORIYA TETSUO , TANAKA NORIO , YANAGIMOTO HIROMITSU , UENO ICHIRO , TSUJITA KOJI
IPC分类号： G02F1/19
摘要： PROBLEM TO BE SOLVED: To make it possible to exhibit optical response of sufficient magnitude and high speed by using a laser beam of low power as control light. SOLUTION: The control light is emitted from a light source 1 and signal light from a light source 2. The control light and the signal light are converged by a condenser lens 7 and is cast to the laminated thin-film optical element 8. Only the signal light is detected by a photodetector 22 through a photodetecting lens 9 and a wavelength selection filter 20. A heat lens is reversibly formed within the laminated thin-film optical element by on and off of the control light, by which the intensity modulation of the signal light may be embodied. The constitution of the thin-film optical element is composed of a laminated structure consisting of for example, a heat transmission layer film/heat insulating layer film/light absorption film/heat lens forming layer/light absorption film/heat insulating layer film/heat transmission layer. The thickness of the light absorption layer consisting of the laminated structure of the light absorption film/heat lens forming layer/light absorption film is so adjusted as not to exceed 2 times the confocal distance of the converged control light.
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公开(公告)号：JPH09179158A
公开(公告)日：1997-07-11
申请号：JP33624795
申请日：1995-12-25
申请人： AGENCY IND SCIENCE TECHN , KAGAKU GIJUTSU SHINKO JIGYODAN , DAINICHISEIKA COLOR CHEM , VICTOR COMPANY OF JAPAN
发明人： HIRAGA TAKASHI , MORIYA TETSUO , TANAKA NORIO , UENO ICHIRO
摘要： PROBLEM TO BE SOLVED: To provide an optical operation processor with which inputting/ outputting from plural functional elements to one functional element consisting of the device is enabled. SOLUTION: Concerning this optical operation processor, plural functional elements (thin film elements) 2, 4, 6 and 8 provided with the monomolecule of organic compound and nanoparticles composed of the aggregate/agglomerate of these monomolecules are arranged for processing information by operating an external signal upon incidental two-dimensional information light. At the same time, this device is provided with light sources I, II, III and IV for transferring image signals among the functional elements 2, 4, 6 and 8.
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公开(公告)号：JPH09160080A
公开(公告)日：1997-06-20
申请号：JP32063195
申请日：1995-12-08
申请人： AGENCY IND SCIENCE TECHN , KAGAKU GIJUTSU SHINKO JIGYODAN , DAINICHISEIKA COLOR CHEM , VICTOR COMPANY OF JAPAN
发明人： HIRAGA TAKASHI , MORIYA TETSUO , TANAKA NORIO , UENO ICHIRO
摘要： PROBLEM TO BE SOLVED: To obtain a full-light type optical element having higher resolution by using a thin-film element contg. nanoparticles composed of the monomolecules of org. compds. and the assemblage and aggregate thereof. SOLUTION: Incident signal light 1 or light 2 for assisting an operation is made incident on the aggregate 3 formed of single kind or plural kinds of the compds. formed of the single atoms or single molecules dispersed as the optically functional aggregate. The aggregate outputs exit signal light 4. The optically functional molecule aggregate 3 dispersed in the element functions as a min. unit element. The space resolution in executing image processing is not defined by the diffraction threshold defined by the wavelength of the signal light and is defined by the diameter of the aggregate 3 formed from the single atoms or molecules dispersed in this element. Information processing is perfected and executed within such aggregate or between pieces of the aggregate. As a result, the full-light type optical element having the high resolution is obtd.
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公开(公告)号：JP2000281821A
公开(公告)日：2000-10-10
申请号：JP9103899
申请日：1999-03-31
申请人： AGENCY IND SCIENCE TECHN , HIRAGA TAKASHI , MORIYA TETSUO , DAINICHISEIKA COLOR CHEM , VICTOR COMPANY OF JAPAN
发明人： HIRAGA TAKASHI , MORIYA TETSUO , CHIN KEIEI , TOMINAGA JUNJI , ATODA NOBUFUMI , TANAKA NORIO , YANAGIMOTO HIROMITSU , UENO ICHIRO , TSUJITA KOJI
IPC分类号： A61K9/70 , A61K9/00 , B29C71/00 , B29K101/00 , C08J7/00 , C08J7/06 , D06M23/00 , G02B1/10 , G02B6/00 , G02B6/02
摘要： PROBLEM TO BE SOLVED: To perform a modification and/or coloring of a resin surface layer by penetrating/dispersing an organic compound having an affinity to the resin and a sublimating property on the surface of the resin formed material. SOLUTION: This method for modifying and coloring a surface of a resin is provide by putting a resin formed material and an organic compound having an affinity to the resin and also a sublimating property in a hermetically closed container, and adjusting inside pressure and temperature to make a saturated sublimation pressure state for uniformly attaching the organic compound on the surface of the resin formed material and further penetrating/dispersing to its inside. Also, by modifying the surface of the resin, it is possible to impart functionality to it.
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