公开(公告)号：JP2005095887A

公开(公告)日：2005-04-14

申请号：JP2004255191

申请日：2004-09-02

申请人： Cem Corp ,  シーイーエム・コーポレーション

发明人： COLLINS MICHAEL JOHN JR ,  HARGETT WYATT PRICE JR ,  KING EDWARD EARL ,  LAMBERT JOSEPH JOSHUA ,  THOMAS JAMES EDWARD

IPC分类号： B01J3/00 ,  B01J4/02 ,  B01J19/12 ,  H05B6/80

CPC分类号： B01J19/126 ,  B01J4/02 ,  B01J2219/00164 ,  B01J2219/1218 ,  B01J2219/1239 ,  B01J2219/126 ,  H05B6/6408 ,  H05B6/806

摘要： PROBLEM TO BE SOLVED: To provide a controlled flow instrument which treats high viscosity liquid and a heterogeneous mixture by a semi-continuous system with high pressure and microwave assistance.
SOLUTION: A controlled flow microwave instrument is disclosed for chemical synthesis using heterogeneous or highly viscous starting materials. The instrument includes a microwave source for generating electromagnetic radiation in the microwave frequencies, a microwave cavity 11 in wave communication with the source for exposing compositions placed therein to microwave radiation, a microwave permeability pressure resistant reaction vessel 13 in the cavity, source reservoirs 15, 16 for starting materials and related compositions, a pump 17 in communication with the source reservoir for pumping heterogeneous or highly viscous materials from the source reservoirs to the reaction vessel and a pressure-resistant valve 34 arranged between the pump and the reaction vessel for isolating the reaction vessel 13 from the pump and the source reservoir during application of microwave energy to the compositions in the vessel and from any resulting high pressure generated therein.
COPYRIGHT: (C)2005,JPO&NCIPI

摘要翻译： 要解决的问题：提供一种受高压和微波辅助的半连续系统处理高粘度液体和异质混合物的受控流量仪表。 解决方案：公开了一种用于使用异质或高粘度起始材料进行化学合成的受控流动微波仪器。 该仪器包括用于产生微波频率的电磁辐射的微波源，与源放射在其中以将微波辐射放置的组合物与源波相通的微波空腔11，腔内的微波渗透压力反应容器13， 16，用于起始材料和相关组合物，与源储存器连通的泵17，用于将不均匀或高粘度物质从源储存器泵送到反应容器;以及耐压阀34，其设置在泵和反应容器之间，用于隔离 在将微波能量施加到容器中的组合物和从其中产生的任何所得到的高压时，来自泵和源储存器的反应容器13。 版权所有（C）2005，JPO＆NCIPI

公开(公告)号：JP2010234369A

公开(公告)日：2010-10-21

申请号：JP2010113981

申请日：2010-05-18

申请人： Cem Corp ,  シーイーエム・コーポレーション

发明人： HARGETT WYATT PRICE JR ,  KING EDWARD EARL

IPC分类号： B01J19/12 ,  B01J3/03 ,  B01J3/04 ,  B01J19/02 ,  F16J12/00 ,  F16J13/02 ,  G01N1/44 ,  G01N35/00 ,  H05B6/64 ,  H05B6/80

CPC分类号： H05B6/806 ,  B01J3/048 ,  B01J19/0073 ,  B01J19/02 ,  B01J19/126 ,  B01J2219/0245 ,  B01J2219/0295 ,  B01J2219/1209 ,  B01J2219/1215 ,  B01J2219/1218 ,  F16J13/02 ,  G01N1/44 ,  G01N2035/00405 ,  H05B6/6408 ,  Y10T428/131 ,  Y10T428/1314 ,  Y10T428/1321 ,  Y10T428/1366 ,  Y10T428/1369 ,  Y10T428/139 ,  Y10T428/1393

摘要： PROBLEM TO BE SOLVED: To provide an improved vessel for a high-pressure micro-wave assisted chemical reaction which has the characteristics of qualities of synthetic material and also improves an existing structure. SOLUTION: A self sealing vessel assembly for the high-pressure micro-wave assisted chemical reaction consists of a polymer reaction cylinder, a circular polymer cap for the cylinder and a chalk cylinder suspending from a downward bevelling edge of the cap, wherein he polymer reaction cylinder is closed at one end, and opened at the other end as to receive the cap, an opened end of the polymer reaction cylinder consisting of a lip bevelled inward therefrom; the circular polymer cap has the downward bevelling edge which engages to the bevelled lip when the cap is put on the polymer cylinder; and the chalk cylinder has an outer diameter nearly equal to an inner diameter of the polymer cylinder so that the chalk supplies a self sealing mechanism for the polymer cylinder when the pressure from a chemical reaction increases in the polymer cylinder. COPYRIGHT: (C)2011,JPO&INPIT

摘要翻译： 要解决的问题：提供具有合成材料质量特性的高压微波辅助化学反应的改进容器，并且还改善了现有的结构。 解决方案：用于高压微波辅助化学反应的自密封容器组件由聚合物反应圆筒，用于气缸的圆形聚合物盖和从盖的向下倾斜边缘悬挂的白垩圆筒组成，其中 聚合物反应缸在一端封闭，另一端开口以接收盖，聚合物反应缸的开口端由向内倾斜的唇部组成; 圆形聚合物盖具有向下倾斜的边缘，当盖被放置在聚合物圆筒上时，该倾斜边缘接合到倾斜的唇缘; 并且白垩圆柱体的外径几乎等于聚合物圆筒的内径，使得当聚合物圆筒中的化学反应的压力增加时，白垩供应聚合物圆筒的自密封机构。 版权所有（C）2011，JPO＆INPIT