Concentrated analysis apparatus and method

    公开(公告)号:JP4118745B2

    公开(公告)日:2008-07-16

    申请号:JP2003155219

    申请日:2003-05-30

    发明人: 貞司 高橋

    摘要: PROBLEM TO BE SOLVED: To provide an enrichment analyzer and a method for enrichment analysis capable of highly sensitively and stably analyzing a component difficult to separate an impurity component from a main component by a column as in analyzing arsine as an impurity in a monosilane. SOLUTION: This method comprises a process for enriching primarily the impurity component by making a sample gas flow in the first cooled concentration tube 21, a process for making a primarily enriched gas enriched in the process hereinbefore flow in the second concentration tube 22 to enrich secondarily the impurity component, a process for making a secondarily enriched gas enriched in the process hereinbefore flow into a precolumn 23 to separate preliminarily the impurity component, a process for making a preseparated gas separated preliminarily in the process hereinbefore flow into a main column 24 to separate the impurity component into a single component, and an analytical process for introducing, into an analyzer 17, the impurity component separated into the single component isolated in the process hereinbefore to be analyzed. COPYRIGHT: (C)2005,JPO&NCIPI

    Microreactor
    6.
    发明专利
    Microreactor 审中-公开
    微反应器

    公开(公告)号:JP2006112836A

    公开(公告)日:2006-04-27

    申请号:JP2004298184

    申请日:2004-10-12

    摘要: PROBLEM TO BE SOLVED: To provide a microreactor capable of preventing clogging of a fine channel or a liquid chromatograph even when two substrates where a recess for the fine channel or a recess for the liquid chromatograph is formed are stuck by an adhesive. SOLUTION: This microreactor comprises a lower substrate where protrusions are formed so as to enclose the recess for the fine channel having the width of 0.1-3,000 μm, and an upper substrate where a protrusion insertable into the recess for the fine channel is formed and recesses capable of inserting the protrusions formed on the lower substrate are formed on both sides across the protrusion. The microreactor is formed by inserting each protrusion into each recess on the other substrate and by laminating the lower substrate and the upper substrate, and has the fine channel having the width and the height of 0.1-3,000 μm, formed between the lower substrate and the upper substrate. COPYRIGHT: (C)2006,JPO&NCIPI

    摘要翻译: 要解决的问题:即使当通过粘合剂粘合用于形成用于精细通道的凹槽或用于液相色谱的凹槽的两个基板时,提供能够防止细小通道或液相色谱仪堵塞的微反应器。 解决方案:这种微反应器包括下部基板,其中形成突起以包围宽度为0.1-3,000μm的细槽的凹槽,以及上基板,其中可插入到精细通道的凹槽中的突起是 形成有能够插入形成在下基板上的突起的凹部形成在突出部的两侧。 微反应器通过将每个突起插入到另一基板上的每个凹部中并且通过层叠下基板和上基板而形成,并且具有形成在下基板和下基板之间的宽度和高度为0.1-3,000μm的细通道 上基板。 版权所有(C)2006,JPO&NCIPI

    Method and apparatus for preparing sample for use in analyzing dioxins, and sampling device for sample used in analyzing dioxins
    8.
    发明专利
    Method and apparatus for preparing sample for use in analyzing dioxins, and sampling device for sample used in analyzing dioxins 有权
    用于分析二氧化铅的样品的制备方法和装置,以及分析二氧化硅中使用的样品的采样装置

    公开(公告)号:JP2005009940A

    公开(公告)日:2005-01-13

    申请号:JP2003172531

    申请日:2003-06-17

    摘要: PROBLEM TO BE SOLVED: To simply prepare a hydrophilic sample for use in analyzing dioxins from a hydrophobic solvent solution of dioxins.
    SOLUTION: The method for preparing the sample for use in analyzing dioxins includes a process of supplying the hydrophobic solvent solution of dioxins refined in a first column 101 to a second column 102 packed with alumina to make the same pass through the column 102, a process of supplying a hydrophilic solvent, capable of dissolving dioxins from a hydrophilic solvent supply part 106, and a process of ensuring the hydrophilic solvent, which passed through the second column 102, through an analyzing sample discharge pipe 107. The hydrophobic solvent solution is, for example, an n-hexane solution and the hydrophilic solvent is, for example, dimethylsulfoxide.
    COPYRIGHT: (C)2005,JPO&NCIPI

    摘要翻译: 要解决的问题:简单地制备用于从二恶英的疏水溶剂溶液中分析二恶英的亲水样品。 解决方案:用于分析二恶英的样品的制备方法包括将在第一塔101中精制的二恶英的疏水性溶剂溶液供给到填充有氧化铝的第二塔102以使相同的通过塔102的方法 提供能够从亲水性溶剂供给部106溶解二氧diox类物质的亲水性溶剂的供给工序,以及通过分析用试料排出管107确保通过第二塔102的亲水性溶剂的工序。疏水性溶剂溶液 是例如正己烷溶液,亲水性溶剂是例如二甲基亚砜。 版权所有(C)2005,JPO&NCIPI