摘要:
PROBLEM TO BE SOLVED: To provide a decomposition system for treating PCB-containing substance. SOLUTION: This system includes a hydrothermal oxidative decomposition apparatus 120 decomposing halogenated organic compounds (ex. PCBs) into sodium chloride, carbon dioxide through their dechlorination and oxidative decomposition in the presence of sodium carbonate in a reactor heated under pressure, an ultraviolet/visible light absorptiometer 100 for determining the decomposition products in reaction liquid or treatment liquid in the apparatus 120 with two kinds of measuring wavelengths, and a halogenated organic compound detective device 113 comprising a solid phase absorption means 111 having a solid phase adsorbent adsorbing/holding the halogenated organic compounds in the reaction liquid or the treatment liquid and a detective means 112 for determining specific halogenated organic compound(s) eluted from the means 111.
摘要:
PROBLEM TO BE SOLVED: To simply prepare a hydrophilic sample for use in analyzing dioxins from a hydrophobic solvent solution of dioxins. SOLUTION: The method for preparing the sample for use in analyzing dioxins includes a process of supplying the hydrophobic solvent solution of dioxins refined in a first column 101 to a second column 102 packed with alumina to make the same pass through the column 102, a process of supplying a hydrophilic solvent, capable of dissolving dioxins from a hydrophilic solvent supply part 106, and a process of ensuring the hydrophilic solvent, which passed through the second column 102, through an analyzing sample discharge pipe 107. The hydrophobic solvent solution is, for example, an n-hexane solution and the hydrophilic solvent is, for example, dimethylsulfoxide. COPYRIGHT: (C)2005,JPO&NCIPI
摘要:
PROBLEM TO BE SOLVED: To provide an enrichment analyzer and a method for enrichment analysis capable of highly sensitively and stably analyzing a component difficult to separate an impurity component from a main component by a column as in analyzing arsine as an impurity in a monosilane. SOLUTION: This method comprises a process for enriching primarily the impurity component by making a sample gas flow in the first cooled concentration tube 21, a process for making a primarily enriched gas enriched in the process hereinbefore flow in the second concentration tube 22 to enrich secondarily the impurity component, a process for making a secondarily enriched gas enriched in the process hereinbefore flow into a precolumn 23 to separate preliminarily the impurity component, a process for making a preseparated gas separated preliminarily in the process hereinbefore flow into a main column 24 to separate the impurity component into a single component, and an analytical process for introducing, into an analyzer 17, the impurity component separated into the single component isolated in the process hereinbefore to be analyzed. COPYRIGHT: (C)2005,JPO&NCIPI
摘要:
PROBLEM TO BE SOLVED: To provide a microreactor capable of preventing clogging of a fine channel or a liquid chromatograph even when two substrates where a recess for the fine channel or a recess for the liquid chromatograph is formed are stuck by an adhesive. SOLUTION: This microreactor comprises a lower substrate where protrusions are formed so as to enclose the recess for the fine channel having the width of 0.1-3,000 μm, and an upper substrate where a protrusion insertable into the recess for the fine channel is formed and recesses capable of inserting the protrusions formed on the lower substrate are formed on both sides across the protrusion. The microreactor is formed by inserting each protrusion into each recess on the other substrate and by laminating the lower substrate and the upper substrate, and has the fine channel having the width and the height of 0.1-3,000 μm, formed between the lower substrate and the upper substrate. COPYRIGHT: (C)2006,JPO&NCIPI
摘要:
PROBLEM TO BE SOLVED: To provide an inorganic monolithic material which can be used as a stationary phase of chromatography and to provide a manufacturing method therefor. SOLUTION: The inorganic monolithic material that contains macropores having an inner surface and nanoparticles attached to the inner surface of the macropore is provided. The macropores and the nanoparticles can be optionally attached to molecular moieties that impart a specific functionality to the monolithic material. COPYRIGHT: (C)2006,JPO&NCIPI
摘要:
PROBLEM TO BE SOLVED: To simply prepare a hydrophilic sample for use in analyzing dioxins from a hydrophobic solvent solution of dioxins. SOLUTION: The method for preparing the sample for use in analyzing dioxins includes a process of supplying the hydrophobic solvent solution of dioxins refined in a first column 101 to a second column 102 packed with alumina to make the same pass through the column 102, a process of supplying a hydrophilic solvent, capable of dissolving dioxins from a hydrophilic solvent supply part 106, and a process of ensuring the hydrophilic solvent, which passed through the second column 102, through an analyzing sample discharge pipe 107. The hydrophobic solvent solution is, for example, an n-hexane solution and the hydrophilic solvent is, for example, dimethylsulfoxide. COPYRIGHT: (C)2005,JPO&NCIPI
摘要:
PROBLEM TO BE SOLVED: To provide an organic substance analyzing apparatus that accurately and quickly performs the microanalysis of an organic substance. SOLUTION: The analyzing apparatus comprises an absorptiometer 103 measuring the absorbance of an organic substance 102 in an object 101 to be measured, a solid phase absorbing means 104 for the organic substance having a solid phase absorbent absorbing and retaining the organic substance 102 in the object 101, an organic substance detecting device 106 formed with a detecting means 105 for measuring the target organic substance 104 solved by an effluent from the solid phase absorbing means 104, and an arithmetic means 107 processing the measuring data of the absorptiometer 103 and the organic substance detecting device 105. COPYRIGHT: (C)2003,JPO