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公开(公告)号：US06660869B2
公开(公告)日：2003-12-09
申请号：US10041666
申请日：2002-01-10
申请人： Rudolfus A. T. M. Van Benthem , Jacobus A. Loontjens , Patrick H. M. Hendriks , Bartholomeus J. M. Plum
发明人： Rudolfus A. T. M. Van Benthem , Jacobus A. Loontjens , Patrick H. M. Hendriks , Bartholomeus J. M. Plum
IPC分类号： C07D26302
CPC分类号： C09D5/033 , C07D263/10 , C07D263/14
摘要： The invention relates to a process for the preparation of an aromatic bisoxazoline in which, in a first step, an aromatic carboxylic acid or an ester hereof reacts with an alkanolamine, after which the hydroxyalkylamide obtained is in a second step converted into an aromatic bisoxazoline in the presence of a catalyst. The catalyst is phosphinic acid, a (C1-C26) alkyl phosphinic acid, a (C6-C20)aryl phosphinic acid or an ester or an anhydride derived from one of these acids.
摘要翻译： 本发明涉及一种制备芳族双恶唑啉的方法，其中在第一步中芳族羧酸或其酯与烷醇胺反应，之后得到的羟基烷基酰胺在第二步中转化为芳族双恶唑啉， 催化剂的存在。 催化剂是次膦酸，（C 1 -C 26）烷基次膦酸，（C 6 -C 20）芳基次膦酸或衍生自这些酸之一的酯或酸酐。
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2.发明授权公开(公告)号：US06448394B1
公开(公告)日：2002-09-10
申请号：US09815268
申请日：2001-03-23
IPC分类号： C07D22310
CPC分类号： C08G18/8074 , C07D223/10 , C08G2150/20 , C08G2390/40
摘要： The invention relates to a process for the preparation of an N-alkyl or N-aryl carbamoyl derivative in which an amine is contacted with a carbonic acid derivative according to the general formula: where fragments X in the form of XH are a lactam, oxime, imide or triazole. In particular the invention relates to the preparation of a blocked isocyanate according to a process in which no isocyanate is used. The invention also relates to the use of the N-alkyl or N-aryl carbamoyl derivative prepared according to the process according to the invention in a coating.
摘要翻译： 本发明涉及一种制备N-烷基或N-芳基氨基甲酰基衍生物的方法，其中胺与根据通式的碳酸衍生物接触：其中XH形式的片段X为内酰胺，肟 ，酰亚胺或三唑。 特别地，本发明涉及根据其中不使用异氰酸酯的方法制备封端异氰酸酯。 本发明还涉及根据本发明的方法制备的N-烷基或N-芳基氨基甲酰基衍生物在涂层中的用途。
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公开(公告)号：US06750316B2
公开(公告)日：2004-06-15
申请号：US10125611
申请日：2002-04-19
IPC分类号： C08G6900
CPC分类号： C08G69/48 , C08G63/916 , C08G69/18 , C08G69/20
摘要： The invention relates to a process for preparing a high-molecular polyamide or polyester by melt-mixing polyamide or polyester having a lower molecular weight with a carbonyl bislactam having formula 1, in which n=an integer of between 3 and 15. With the process according to the invention a permanent increase in the molecular weight of a polyamide is obtained within 2 minutes, whereas this takes at least 10 minutes under comparable conditions using a bislactam according to the state of the art.
摘要翻译： 本发明涉及通过将具有较低分子量的聚酰胺或聚酯与具有式1的羰基双内酰胺熔融混合制备高分子量聚酰胺或聚酯的方法，其中n = 3至15的整数。通过该方法 根据本发明，在2分钟内获得聚酰胺的分子量的永久增加，而根据现有技术，使用双内酰胺在相当的条件下至少需要10分钟。
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公开(公告)号：US06395869B2
公开(公告)日：2002-05-28
申请号：US09772870
申请日：2001-01-31
IPC分类号： C08G6914
CPC分类号： C08G69/48 , C08G63/916 , C08G69/18 , C08G69/20
摘要： A high molecular weight polyester-amide block copolymer is produced by reacting a mixture of lower molecular weight polyester and polyamide in the melt with a carbonyl bislactam, especially carbonyl biscaprolactam. The higher molecular weight block copolymer may be obtained in as short a time as 2 minutes, whereas, at least about 10 minutes is required in a conventional process, under comparable conditions, using a bislactam.
摘要翻译： 通过使熔体中的低分子量聚酯和聚酰胺的混合物与羰基双内酰胺，特别是羰基双己内酰胺反应来制备高分子量聚酯酰胺嵌段共聚物。 较高分子量嵌段共聚物可以在2分钟的短时间内获得，而在常规方法中，在相当的条件下，使用双内酰胺需要至少约10分钟。
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公开(公告)号：US06683151B1
公开(公告)日：2004-01-27
申请号：US09511984
申请日：2000-02-24
IPC分类号： C09D17500
CPC分类号： C08G18/6674 , C08G18/3851 , C08G18/4854 , C08G83/008 , Y10T428/2929 , Y10T428/2933 , Y10T428/2938 , Y10T428/2964
摘要： The invention relates to a compound comprising a reaction product of (A) an isocyanate functional compound of which at least 40 wt. %, relative to the total amount of (A), has a molecular weight of at least about 500, and (B) a nitrogen-containing compound capable of reacting with said isocyanate functional compound (A). The reaction product has a molecular weight of less then about 20,000 and comprises an effective amount of groups that are able to form reversible intermolecular physical interactions such that a resulting compound shows polymeric mechanical properties at a temperature below a transition temperature. The nitrogen-containing compound is, for instance, melamine, urea, acetoguanamine, benzoguanamine, cyanamide, dicyanamide, thiourea, isocytosine, pyrimidone or aminopyridine. The supramolecular compound comprising a suitable amount of the reaction products exhibits a relatively high elongation at break.
摘要翻译： 本发明涉及包含（A）异氰酸酯官能化合物的反应产物的化合物，其中至少40重量％ 相对于（A）的总量的％具有至少约500的分子量，和（B）能够与所述异氰酸酯官能化合物（A）反应的含氮化合物。 反应产物的分子量小于约20,000，并且包含有效量的能够形成可逆分子间物理相互作用的基团，使得所得化合物在低于转变温度的温度下显示出聚合物的机械性能。 含氮化合物是例如三聚氰胺，脲，乙酰胍胺，苯并胍胺，氨腈，二氰胺，硫脲，异胞嘧啶，嘧啶酮或氨基吡啶。 包含适量的反应产物的超分子化合物表现出较高的断裂伸长率。
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公开(公告)号：US06228980B1
公开(公告)日：2001-05-08
申请号：US09421525
申请日：1999-10-20
IPC分类号： C08G6914
CPC分类号： C08G69/48 , C08G63/916 , C08G69/18 , C08G69/20
摘要： The invention relates to a process for preparing a high-molecular polyamide or polyester by melt-mixing polyamide or polyester having a lower molecular weight with a carbonyl bislactam having formula 1, in which n=an integer of between 3 and 15. With the process according to the invention a permanent increase in the molecular weight of a polyamide is obtained within 2 minutes, whereas this takes at least 10 minutes under comparable conditions using a bislactam according to the state of the art.
摘要翻译： 本发明涉及通过将具有较低分子量的聚酰胺或聚酯与具有式1的羰基双内酰胺熔融混合制备高分子量聚酰胺或聚酯的方法，其中n = 3至15的整数。通过该方法 根据本发明，在2分钟内获得聚酰胺的分子量的永久增加，而根据现有技术，使用双内酰胺在相当的条件下至少需要10分钟。
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