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1.发明授权公开(公告)号：US08092604B2
公开(公告)日：2012-01-10
申请号：US12464333
申请日：2009-05-12
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/00 , C23C16/448 , C23C16/18
CPC分类号： C30B25/14 , C23C16/4481 , Y10T428/13
摘要： A solid organometallic compound novel filled container stably supplies an apparatus for vapor phase epitaxial growth such as an MOCVD apparatus with a solid organometallic compound over a long term. The solid organometallic compound-filled container has a carrier gas inlet and a carrier gas outlet. The interior of the filled container is separated into a plurality of vertical compartments. A carrier gas introduced via the carrier gas inlet flows through each of the vertical compartments and is then discharged via the carrier gas outlet.
摘要翻译： 固体有机金属化合物新型填充容器长期稳定地供给诸如具有固体有机金属化合物的MOCVD装置的气相外延生长装置。 固体有机金属化合物填充容器具有载气入口和载气出口。 填充容器的内部被分成多个垂直隔室。 通过载气进口引入的载气流过每个垂直隔室，然后通过载气出口排出。
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2.发明申请DIETHYLZINC COMPOSITION, METHOD FOR HEAT STABILIZATION, AND COMPOUND FOR HEAT STABILIZATION 有权二氯乙烯组合物，热稳定化方法和用于热稳定化合物公开(公告)号：US20120184432A1
公开(公告)日：2012-07-19
申请号：US13394129
申请日：2010-09-01
申请人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
发明人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
IPC分类号： C08F4/50 , C07C13/48 , C07C13/16 , C07C13/465
CPC分类号： C07F3/06 , C08F4/50 , C08F2410/01
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Solving Means]Use a diethylzinc composition added a compound which is added an aromatic compound as an additive which has isopropenyl group bonded as a side chain.
摘要翻译： 本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。 并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决方法]使用二乙基锌组合物，加入加入芳族化合物作为侧链键合有异丙烯基的添加剂的化合物。
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3.发明授权公开(公告)号：US07547363B2
公开(公告)日：2009-06-16
申请号：US10865880
申请日：2004-06-14
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/448 , C23C16/18 , C23C16/00
CPC分类号： C30B25/14 , C23C16/4481 , Y10T428/13
摘要： A solid organometallic compound novel filled container stably supplies an apparatus for vapor phase epitaxial growth such as an MOCVD apparatus with a solid organometallic compound over a long term. The solid organometallic compound-filled container has a carrier gas inlet and a carrier gas outlet. The interior of the filled container is separated into a plurality of vertical compartments. A carrier gas introduced via the carrier gas inlet flows through each of the vertical compartments and is then discharged via the carrier gas outlet.
摘要翻译： 固体有机金属化合物新型填充容器长期稳定地供给诸如具有固体有机金属化合物的MOCVD装置的气相外延生长装置。 固体有机金属化合物填充容器具有载气入口和载气出口。 填充容器的内部被分成多个垂直隔室。 通过载气进口引入的载气流过每个垂直隔室，然后通过载气出口排出。
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4.发明申请公开(公告)号：US20050008799A1
公开(公告)日：2005-01-13
申请号：US10865880
申请日：2004-06-14
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/448 , C30B25/14 , F16L1/00
CPC分类号： C30B25/14 , C23C16/4481 , Y10T428/13
摘要： A novel filled container is provided, which can stably supply an apparatus for vapor phase epitaxial growth such as an MOCVD apparatus with a solid organometallic compound over a long term. The solid organometallic compound-filled container has a carrier gas inlet and a carrier gas outlet. The interior of the filled container is separated into a plurality of vertical compartments. A carrier gas introduced via the carrier gas inlet flows through each of the vertical compartments and is then discharged via the carrier gas outlet.
摘要翻译： 提供了一种新颖的填充容器，其可以长期稳定地供应诸如具有固体有机金属化合物的MOCVD装置的气相外延生长装置。 固体有机金属化合物填充容器具有载气入口和载气出口。 填充容器的内部被分成多个垂直隔室。 通过载气进口引入的载气流过每个垂直隔室，然后通过载气出口排出。
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公开(公告)号：US08673413B2
公开(公告)日：2014-03-18
申请号：US11340739
申请日：2006-01-27
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
CPC分类号： C23C16/4481 , Y10T428/13
摘要： A method for packing a solid organometallic compound into a container for packing the compound is provided, wherein the solid organometallic compound can be stably supplied to a vapor phase epitaxial growth apparatus such as an MOCVD apparatus at a constant concentration for a long period of time. In the method for packing a solid organometallic compound into a container for packing, the compound is composed of grains having a grain size of 8 mm or less and the grains of the compound essentially comprise grains having a grain size of 2.5 to 6 mm.
摘要翻译： 提供了一种将固体有机金属化合物填充到用于填充化合物的容器中的方法，其中固体有机金属化合物可以长时间稳定地供给到恒定浓度的诸如MOCVD装置的气相外延生长装置。 在将固体有机金属化合物填充到用于包装的容器中的方法中，化合物由粒径为8mm以下的晶粒构成，该化合物的晶粒基本上包含粒径为2.5〜6mm的晶粒。
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公开(公告)号：US20070175397A1
公开(公告)日：2007-08-02
申请号：US11340739
申请日：2006-01-27
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/00
CPC分类号： C23C16/4481 , Y10T428/13
摘要： A method for packing a solid organometallic compound into a container for packing the compound is provided, wherein the solid organometallic compound can be stably supplied to a vapor phase epitaxial growth apparatus such as an MOCVD apparatus at a constant concentration for a long period of time. In the method for packing a solid organometallic compound into a container for packing, the compound is composed of grains having a grain size of 8 mm or less and the grains of the compound essentially comprise grains having a grain size of 2.5 to 6 mm.
摘要翻译： 提供了一种将固体有机金属化合物填充到用于填充化合物的容器中的方法，其中固体有机金属化合物可以长时间稳定地供给到恒定浓度的诸如MOCVD装置的气相外延生长装置。 在将固体有机金属化合物填充到用于包装的容器中的方法中，化合物由粒径为8mm以下的晶粒构成，化合物的粒子基本上包含粒径为2.5〜6mm的晶粒。
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7.发明授权Diethylzinc composition, method for heat stabilization, and compound for heat stabilization 有权二乙基锌组合物，热稳定化方法和热稳定化合物公开(公告)号：US09156857B2
公开(公告)日：2015-10-13
申请号：US13989660
申请日：2011-12-15
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Means for Solving Problem]Use a diethylzinc composition added a compound which has particular carbon-carbon double bond to a diethylzinc.
摘要翻译： 本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。 并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决问题的方法]使用二乙基锌组合物加入具有特定碳 - 碳双键的化合物至二乙基锌。
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8.发明授权Diethylzinc composition, method for heat stabilization, and compound for heat stabilization 有权二乙基锌组合物，热稳定化方法和热稳定化合物公开(公告)号：US08722561B2
公开(公告)日：2014-05-13
申请号：US13394129
申请日：2010-09-01
申请人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
发明人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
IPC分类号： C08F4/50 , C07C13/48 , C07C13/16 , C07C13/465
CPC分类号： C07F3/06 , C08F4/50 , C08F2410/01
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Solving Means]Use a diethylzinc composition added a compound which is added an aromatic compound as an additive which has isopropenyl group bonded as a side chain.
摘要翻译： 本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。 并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决方法]使用二乙基锌组合物，加入加入芳族化合物作为侧链键合有异丙烯基的添加剂的化合物。
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9.发明申请DIETHYLZINC COMPOSITION, METHOD FOR HEAT STABILIZATION, AND COMPOUND FOR HEAT STABILIZATION 有权二氯乙烯组合物，热稳定化方法和用于热稳定化合物公开(公告)号：US20130281724A1
公开(公告)日：2013-10-24
申请号：US13989660
申请日：2011-12-15
IPC分类号： C07F3/06
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Means for solving problem]Use a diethylzinc composition added a compound which has particular carbon-carbon double bond to a diethylzinc.
摘要翻译： 本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。 并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决问题的方法]使用二乙基锌组合物向二乙基锌中加入特定碳 - 碳双键的化合物。
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10.发明申请公开(公告)号：US20090283041A1
公开(公告)日：2009-11-19
申请号：US12464333
申请日：2009-05-12
申请人： Shizuo TOMIYASU , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo TOMIYASU , Kohichi Tokudome , Kenichi Haga
CPC分类号： C30B25/14 , C23C16/4481 , Y10T428/13
摘要： A solid organometallic compound novel filled container stably supplies an apparatus for vapor phase epitaxial growth such as an MOCVD apparatus with a solid organometallic compound over a long term. The solid organometallic compound-filled container has a carrier gas inlet and a carrier gas outlet. The interior of the filled container is separated into a plurality of vertical compartments. A carrier gas introduced via the carrier gas inlet flows through each of the vertical compartments and is then discharged via the carrier gas outlet.
摘要翻译： 固体有机金属化合物新型填充容器长期稳定地供给诸如具有固体有机金属化合物的MOCVD装置的气相外延生长装置。 固体有机金属化合物填充容器具有载气入口和载气出口。 填充容器的内部被分成多个垂直隔室。 通过载气进口引入的载气流过每个垂直隔室，然后通过载气出口排出。
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