Process for the production of polyarenazole polymer
    2.
    发明申请
    Process for the production of polyarenazole polymer 有权
    聚赖氨酸聚合物生产工艺

    公开(公告)号:US20060287475A1

    公开(公告)日:2006-12-21

    申请号:US11390898

    申请日:2006-03-27

    IPC分类号: C08G63/02

    摘要: The present invention concerns a process for making a polyareneazole polymer comprising the steps of: a) contacting azole-forming monomers, metal powder, and optionally P2O5, in polyphosphoric acid to form a mixture; b) blending the mixture at a temperature of from about 50° C. to about 110° C.; c) further blending the mixture at a temperature of up to about 145° C. to form a solution comprising an oligomer; d) optionally, degassing the solution; and e) reacting the oligomer solution at a temperature of about 160° C. to about 250° C. for a time sufficient to form a polymer.

    摘要翻译: 本发明涉及一种制备聚azole唑聚合物的方法,包括以下步骤:a)使形成吡咯的单体,金属粉末和任选的P 2 O 5 O 5在多磷酸 酸形成混合物; b)在约50℃至约110℃的温度下混合该混合物; c)在高达约145℃的温度下进一步混合该混合物以形成包含低聚物的溶液; d)任选地,使溶液脱气; 和e)在约160℃至约250℃的温度下使所述低聚物溶液反应足以形成聚合物的时间。

    Processes for preparing high inherent viscosity polyareneazoles using metal powders
    5.
    发明申请
    Processes for preparing high inherent viscosity polyareneazoles using metal powders 失效
    使用金属粉末制备高特性粘度聚芳唑的方法

    公开(公告)号:US20070010654A1

    公开(公告)日:2007-01-11

    申请号:US11390849

    申请日:2006-03-27

    IPC分类号: C08G73/00

    CPC分类号: C08G73/18 C08G73/22

    摘要: Disclosed are processes for preparing polyareneazole polymers that include contacting, in polyphosphoric acid, azole-forming monomers and metal powder, the metal powder added in an amount of from about 0.05 to about 0.9 weight percent, based on the total weight of the azole-forming monomers, and reacting the azole-forming monomers to form the polyareneazole polymers. Polyareneazoles, filaments and yarns are also disclosed.

    摘要翻译: 公开了制备聚are唑聚合物的方法,其包括在多磷酸中形成吡唑形成单体和金属粉末,金属粉末的添加量为基于吡唑形成的总重量的约0.05至约0.9重量% 单体,并使形成唑的单体反应形成聚芳腈聚合物。 还公开了聚芳ne唑,长丝和纱线。