公开(公告)号：US20240058773A1

公开(公告)日：2024-02-22

申请号：US18260176

申请日：2021-03-25

Applicant: East China University of Science and Technology

Inventor： Hao LU ,  Qiang YANG ,  Yudong LI ,  Yiqian LIU ,  Pinyi DAI ,  Shihan WU

IPC: B01F23/41 ,  B01F23/451 ,  B01F25/20 ,  B01F25/21 ,  B01F25/10 ,  B01F25/4314 ,  B01F25/433

CPC classification number: B01F23/4105 ,  B01F23/4143 ,  B01F23/451 ,  B01F25/28 ,  B01F25/211 ,  B01F25/103 ,  B01F25/43141 ,  B01F25/4334 ,  B01F2025/916

Abstract: The invention provides a device for enhancing liquid-liquid emulsification. The device includes a jet part and a mixing part connected to the jet part. The jet part includes a feed tee for feeding major and dispersed phases, wherein the feed tee includes a first port, a second port, and a third port. The first port is used for feeding the major phase, and the second port is equipped with an ejector for feeding the dispersed phase. The ejector consists of an ejector housing and an ejector inlet section, as well as a spiral structure, a flow-guided structure, and an ejector pin structure that are connected sequentially. The mixing part includes a mixer comprising a cylindrical mixer shell, a mixer inlet section, a mixer outlet section, as well as a spiral section, a cavity section, and a variable diameter section for enhancing emulsion breakup and dispersion. A method for enhancing liquid-liquid emulsification is also disclosed. The emulsion produced by the device and method of the invention is uniformly dispersed, has long stability, and the device has a compact structure and low energy consumption. It is particularly suitable for liquid-liquid emulsification processes in fields such as chemical industry, food, coatings, and cosmetics.

公开(公告)号：US20160038854A1

公开(公告)日：2016-02-11

申请号：US14764178

申请日：2014-01-10

Applicant: EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Inventor： Qiang YANG ,  Xiao XU ,  Hao LU ,  Chaoyang WANG

IPC: B01D19/00 ,  C10G45/00

CPC classification number: B01D19/0036 ,  B01D3/06 ,  B01D19/0057 ,  C10G31/06 ,  C10G31/10 ,  C10G45/00 ,  C10G45/20 ,  C10G53/02 ,  Y02E60/324

Abstract: A method and apparatus for improving a hydrogen utilization rate in a hydrogenation hot high-pressure separation process. Hydrogenated distillate oil, a gas product and hydrogen pass through an inertia separation distributor arranged in an inlet of a hot high-pressure separator under high pressure for preliminary gas-liquid separation, and a gas phase goes to a subsequent system; a liquid phase goes into a hot low-pressure separator. Releases a part of low-pressure separated gas (mainly hydrogen) after preliminary separation through an injection flash separator in the hot low-pressure separator, and is divided into a gas phase and a liquid phase based on gravitational settling; hydrogen and some micro bubbles that are still dissolved in hot low-pressure separated oil under the pressure are separated from the oil through a centrifugal degassing device; the gas phase exits from the apparatus after carried liquid droplets are removed completely through hydrocyclone separation or coalescence separation, and distillate oil goes to a subsequent facility.

Abstract translation: 一种用于提高氢化热高压分离工艺中氢利用率的方法和装置。 氢化馏出油，气体产物和氢气通过布置在高压分离器的高压分离器的入口处的预定气液分离的惯性分离分配器，气相进入后续系统; 液相进入热的低压分离器。 通过热式低压分离器中的注射闪蒸分离器预先分离出一部分低压分离气体（主要是氢气），并基于重力沉降分为气相和液相; 在压力下仍然溶解在热的低压分离油中的氢气和一些微气泡通过离心脱气装置与油分离; 在通过水力旋流器分离或聚结分离完全移除载运液滴后，气相从设备中排出，馏出油进入后续设施。

公开(公告)号：US20180023009A1

公开(公告)日：2018-01-25

申请号：US15549385

申请日：2015-05-04

Applicant: East China University of Science and Technology

Inventor： Qiang YANG ,  Hao LU ,  Sen LIU ,  Chaoyang WANG ,  Xiao XU

IPC: C10G53/02 ,  B01D17/02 ,  B01D17/04 ,  B01D19/00

Abstract: This invention involves a method and a device for enhanced oil-water separation and desalination in a low-pressure separator. The water-containing oil is mixed with desalted water in a countercurrent way at the entrance, wherein the desalted water accounts for 0-1% of the water-containing oil by volume. The resultant oil-water mixture then enters a T-shaped liquid-gas separator (3) for degassing treatment to quickly separate gas from the mixture. In a low-pressure separator, the oil-water mixture flows, from left to right, to a flow conditioner (4) to uniformly distribute the mixture in the transverse section, and then flows to a hydrophilic droplet agglomeration module (5) and a CPI fast separation module (6) to separate water from oil, wherein part of the separated water is discharged and the oil with a trace of water (0-0.01%) passes over a partition (18) to a deep separation segment. The oil is subjected to deep water removal by a conjugated fiber water removal module and then discharged, and the water captured by the conjugated fiber water removal module is subject to a conjugated fiber oil removal module for deep oil removal and then discharged.

公开(公告)号：US20160082366A1

公开(公告)日：2016-03-24

申请号：US14764179

申请日：2014-01-10

Applicant: EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Inventor： Qiang YANG ,  Xiao XU ,  Hao LU ,  Chaoyang WANG

IPC: B01D19/00

CPC classification number: B01D19/0052 ,  B01D19/0036 ,  B01D19/0057

Abstract: The present invention relates to a device for liquid degassing by means of the swirling or the centrifugal field coupled with the pressure gradient field. This device comprises a cavity. The cavity is furnished with an inlet for liquid gas, an outlet for gas phase and an outlet for gas liquid phase. The outlet for gas phase is inserted into the cavity through the upper surface of the cavity, wherein the depth of the insertion is around 0.1-3 times of the maximum diameter of the cavity. Specifically, the outlet for gas phase is realized through an overflow pipe with the diameter gradually increasing from the bottom to the top. The end of the overflow pipe is further furnished with a bell mouth. The advantages of the present invention are: The present invention designs the structure of an inverted cone shaped outlet for gas phase which is inserted into the cavity of the swirling device. The present invention makes full use of the impact of pressure gradient in the cavity on the solubility of gas in liquid and combines the centrifugal field and the pressure gradient field to remove the gas entrained with liquid while the dissolved gas is removed under the inlet partial pressure.

Abstract translation: 本发明涉及通过与压力梯度场耦合的涡流或离心场进行液体脱气的装置。 该装置包括空腔。 空腔配有液体气体入口，气相出口和气液相出口。 用于气相的出口通过空腔的上表面插入空腔中，其中插入深度为空腔最大直径的0.1-3倍。 具体来说，气相出口通过从底部到顶部逐渐增加的溢流管实现。 溢流管的末端还配有喇叭口。 本发明的优点是：本发明设计了插入旋流装置的空腔中的用于气相的倒锥形出口的结构。 本发明充分利用空腔内的压力梯度对液体中气体溶解度的影响，结合离心场和压力梯度场来除去在入口分压下去除溶解气体时液体夹带液体 。

公开(公告)号：US20170088441A1

公开(公告)日：2017-03-30

申请号：US15312190

申请日：2014-07-21

Applicant: East China University of Science and Technology

Inventor： Qiang YANG ,  Hao LU ,  Jiabin ZHU ,  Xiao XU ,  Yiqian LIU

IPC: C02F1/40

CPC classification number: C02F1/40 ,  C02F1/006 ,  C02F1/288 ,  C02F2101/32 ,  C02F2103/10 ,  C02F2103/365

Abstract: The present invention relates to a method and a device for deep oil removal from wastewater containing a low concentration of wasteoil. Wastewater containing a low concentration of wasteoil enters the device via an inlet and passes through a flow conditioner, causing the fluid to become uniformly distributed. Then, by means of a layer of oleophilic-hydrophobic fibers and hydrophilic-oleophobic fibers woven in a certain manner, a trace of oil droplets are captured and then coalesce and grow on the layer, and a trace of oil-in-water emulsion is demulsified and separated on the layer. Finally, by means of corrugation-enhanced sedimentation and separation, the oil droplets coalesce and grow and are then separated rapidly. The invention also provides a set of devices for implementing the method, having several parts such as a housing, a feed pipe, a flow conditioner, a fiber coalescence layer, a corrugation-enhanced separation layer, and a level gauge. The present technique is highly efficient in separation, consumes little power, and can operate continuously for a long period of time. Thus, this technique can be widely used in processes for treating wastewater containing a low concentration of wasteoil.