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公开(公告)号：US6114037A
公开(公告)日：2000-09-05
申请号：US379005
申请日：1999-08-23
CPC分类号： D01F2/00 , D01F2/28 , Y10T428/2913 , Y10T428/2965
摘要： The present invention is directed to a multifilament yarn having regenerated cellulose filaments.
摘要翻译： 本发明涉及一种具有再生纤维素长丝的复丝纱线。
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公开(公告)号：US5997790A
公开(公告)日：1999-12-07
申请号：US97534
申请日：1998-05-19
CPC分类号： D01F2/00 , D01F2/28 , Y10T428/2913 , Y10T428/2965
摘要： The disclosure describes a process for the preparation of regenerated cellulose filaments from an anisotropic solution including cellulose formate, phosphoric acid, and formic acid in which the formed cellulose formate filaments are dried to a moisture content of not more than 15% prior to regeneration and after regeneration the filaments are washed and dried under low tension. In this manner cellulose multifilament yarns of high breaking load and high elongation at break can be obtained, which in addition have a very regular linear density.
摘要翻译： 本公开内容描述了一种从包括甲酸纤维素，磷酸和甲酸的各向异性溶液制备再生纤维素长丝的方法，其中所形成的纤维素甲酸纤维素在再生之前和之后干燥至含水量不超过15％ 再生长丝在低张力下被洗涤和干燥。 以这种方式，可以获得高断裂负荷和高断裂伸长率的纤维素复丝纱线，此外还具有非常规则的线密度。
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公开(公告)号：US5932158A
公开(公告)日：1999-08-03
申请号：US28841
申请日：1998-02-24
摘要： An optically anisotropic solution containing cellulose and inorganic acids of phosphorus contains 94-100 wt % of the following constituents: cellulose; phosphoric acid and/or its anhydrides; and water; and 0-6 wt % of other constituents. This solution can be prepared in an apparatus in which intensive mixing is made possible by the shearing forces generated by mixers and kneaders in the apparatus. The solution can be used in making pulp, hollow fibres, staple fibre, membranes, nonwovens, or films.
摘要翻译： 包含磷的纤维素和无机酸的光学各向异性溶液含有94-100重量％的以下组分：纤维素; 磷酸和/或其酸酐; 和水; 和0-6重量％的其他成分。 该溶液可以在通过在设备中由混合器和捏合机产生的剪切力进行强烈混合的装置中制备。 该溶液可用于制造纸浆，中空纤维，短纤维，膜，无纺布或膜。
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公开(公告)号：US5817801A
公开(公告)日：1998-10-06
申请号：US793815
申请日：1997-02-25
摘要： An optically anisotropic solution containing cellulose and inorganic acids of phosphorus contains 94-100 wt % of the following constituents: cellulose; phosphoric acid and/or its anhydrides; and water; and 0-6 wt % of other constituents. This solution can be prepared in an apparatus in which intensive mixing is made possible by the shearing forces generated by mixers and kneaders in the apparatus. The solution can be used in making pulp, hollow fibres, staple fibre, membranes, nonwovens, or films.
摘要翻译： PCT No.PCT / EP95 / 03272 Sec。 371日期1997年2月25日 102（e）日期1997年2月25日PCT提交1995年8月17日PCT公布。 出版物WO96 / 06208 日期1996年2月29日含有磷酸纤维素和无机酸的光学各向异性溶液含有94-100重量％的以下成分：纤维素; 磷酸和/或其酸酐; 和水; 和0-6重量％的其他成分。 该溶液可以在通过在设备中由混合器和捏合机产生的剪切力进行强烈混合的装置中制备。 该溶液可用于制造纸浆，中空纤维，短纤维，膜，无纺布或膜。
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5.发明授权Method for preparing a cellulose formate solution by impregnating and kneading cellulose slabs 失效通过浸渍和捏合纤维素板制备甲酸纤维素溶液的方法
公开(公告)号：US6022614A
公开(公告)日：2000-02-08
申请号：US981594
申请日：1998-03-17
CPC分类号： C08J5/18 , B60C9/0042 , C08B1/02 , C08B3/04 , C08L1/10 , D01F2/28 , C08J2301/10 , Y10T428/249925 , Y10T428/249933 , Y10T428/24994 , Y10T428/31971
摘要： Process for preparing a solution of cellulose formate from cellulose plates, in particular high-density plates, without prior mechanical destruction of these plates. The plates are dissolved directly, by means of an impregnating step of the whole plates in a base liquid of formic acid, followed by an operation of kneading of the plates thus impregnated in contact with both formic acid and phosphoric acid. The process is preferably carried out in order to prepare ready-for-spinning solutions with, in particular, if necessary, an intermediate operation of adjustment of the final composition. Solutions prepared using such a process. Preparation of objects made of cellulose, starting with these solutions, in particular fibers or films. Assemblies of such fibers or films. Articles reinforced with such fibers or films or assemblies, these reinforced articles being especially tires.
摘要翻译： PCT No.PCT / EP96 / 02827 Sec。 371日期：1998年3月17日 102（e）1998年3月17日PCT PCT 1996年6月28日PCT公布。 第WO97 / 02292号公报 日期1997年1月23日从纤维素板，特别是高密度板制备纤维素甲酸酯的方法，没有这些板的预先机械破坏。 通过将整个板的浸渍步骤直接溶解在甲酸的基础液中，然后对由此浸渍的与二甲酸和磷酸接触的板进行捏合操作。 该方法优选进行以便制备即将纺丝的溶液，特别是如果必要的话，调整最终组合物的中间操作。 使用这种过程准备的解决方案。 由这些溶液，特别是纤维或薄膜开始制备由纤维素制成的物体。 这种纤维或薄膜的组件。 用这种纤维或膜或组件增强的制品，这些增强制品特别是轮胎。
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公开(公告)号：US08999212B2
公开(公告)日：2015-04-07
申请号：US13636063
申请日：2011-03-17
申请人： Bernardus Maria Koenders , Jacobus Johannes Meerman , Stephanus Maria Kamperman , Ron Folkert Waarbeek Ter , Jorrit Jong De , Angelique Antonia Theresia Hendrikus Radier , Marcin Jan Otto
发明人： Bernardus Maria Koenders , Jacobus Johannes Meerman , Stephanus Maria Kamperman , Ron Folkert Waarbeek Ter , Jorrit Jong De , Angelique Antonia Theresia Hendrikus Radier , Marcin Jan Otto
摘要： A graphene ribbon fiber manufacturing process, where a coagulation medium flows in the same direction as the graphene ribbon fibers. The process for spinning graphene ribbon fibers starts with unzipping carbon nanotubes to form graphene ribbons, purifying and drying the graphene ribbons and subsequent dissolving of the graphene ribbons in a suitable solvent, preferably a super acid to form a spin-dope. The spin-dope is spun such that the accrued fibers are guided into a coagulation medium, also known as anti-solvent, where the spun or accrued fibers are coagulated. The coagulated graphene ribbon fibers are stripped, neutralized and washed and wound on bobbins.
摘要翻译： 石墨烯丝带纤维制造方法，其中凝结介质沿与石墨烯丝带纤维相同的方向流动。 旋转石墨烯带状纤维的过程从解压缩碳纳米管开始，形成石墨烯带，净化和干燥石墨烯带，随后将石墨烯带溶解在合适的溶剂中，优选为超酸以形成纺丝原液。 将纺丝原液纺丝，使得累积的纤维被引导到凝结介质中，也称为抗溶剂，其中纺丝或累积纤维凝结。 凝结的石墨烯带纤维被剥离，中和并洗涤并缠绕在线轴上。
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7.发明申请METHOD FOR DISSOLVING ARAMID POLYMER IN SULFURIC ACID USING A DOUBLE SHAFT KNEADER 有权使用双轴KNEADER分解硫酸中的ARAMID聚合物的方法公开(公告)号：US20100063205A1
公开(公告)日：2010-03-11
申请号：US12448811
申请日：2008-01-30
CPC分类号： C08J3/097 , B29C47/0004 , B29C47/364 , B29C47/366 , B29C47/369 , C08J2377/10 , D01D1/02 , D01F6/605
摘要： A method for dissolving an aramid polymer in sulfuric acid using a double shaft kneader, comprising the steps: dosing the polymer and the solvent into the kneader, mixing the polymer and the solvent to dissolve the polymer in the solvent for obtaining a solution, degassing the solution to obtain a spin dope, and transporting the spin dope out of the kneader, wherein the polymer is an aramid polymer and the solvent is sulfuric acid, and whereby the aramid polymer is dosed into the kneader prior to dosing the sulfuric acid into the kneader.
摘要翻译： 一种使用双轴捏和机将芳族聚酰胺聚合物溶解在硫酸中的方法，包括以下步骤：将聚合物和溶剂投入到捏合机中，混合聚合物和溶剂以将聚合物溶解在溶剂中以获得溶液，脱气 溶液以获得旋涂液，并将旋转纺丝液输送出捏合机，其中聚合物是芳族聚酰胺聚合物，溶剂是硫酸，由此在将硫酸加入到捏合机中之前将芳族聚酰胺聚合物加入捏合机中 。
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公开(公告)号：US20130009337A1
公开(公告)日：2013-01-10
申请号：US13636063
申请日：2011-03-17
申请人： Bernardus Maria Koenders , Jacobus Johannes Meerman , Stephanus Maria Kamperman , Ron Folkert Waarbeek Ter , Jorrit Jong De , Angelique Antonia Theresia Hendrikus Radier , Marcin Jan Otto
发明人： Bernardus Maria Koenders , Jacobus Johannes Meerman , Stephanus Maria Kamperman , Ron Folkert Waarbeek Ter , Jorrit Jong De , Angelique Antonia Theresia Hendrikus Radier , Marcin Jan Otto
摘要： A graphene ribbon fiber manufacturing process, where a coagulation medium flows in the same direction as the graphene ribbon fibers. The process for spinning graphene ribbon fibers starts with unzipping carbon nanotubes to form graphene ribbons, purifying and drying the graphene ribbons and subsequent dissolving of the graphene ribbons in a suitable solvent, preferably a super acid to form a spin-dope. The spin-dope is spun such that the accrued fibers are guided into a coagulation medium, also known as anti-solvent, where the spun or accrued fibers are coagulated. The coagulated graphene ribbon fibers are stripped, neutralized and washed and wound on bobbins.
摘要翻译： 石墨烯丝带纤维制造方法，其中凝结介质沿与石墨烯丝带纤维相同的方向流动。 旋转石墨烯带状纤维的过程从解压缩碳纳米管开始，形成石墨烯带，净化和干燥石墨烯带，随后将石墨烯带溶解在合适的溶剂中，优选为超酸以形成纺丝原液。 将纺丝原液纺丝，使得累积的纤维被引导到凝结介质中，也称为抗溶剂，其中纺丝或累积纤维凝结。 凝结的石墨烯带纤维被剥离，中和并洗涤并缠绕在线轴上。
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9.发明授权Method for dissolving aramid polymer in sulfuric acid using a double shaft kneader 有权使用双轴捏合机将芳族聚酰胺聚合物溶解在硫酸中的方法公开(公告)号：US08309642B2
公开(公告)日：2012-11-13
申请号：US12448811
申请日：2008-01-30
IPC分类号： C08G69/26
CPC分类号： C08J3/097 , B29C47/0004 , B29C47/364 , B29C47/366 , B29C47/369 , C08J2377/10 , D01D1/02 , D01F6/605
摘要： A method for dissolving an aramid polymer in sulfuric acid using a double shaft kneader, comprising the steps: dosing the polymer and the solvent into the kneader, mixing the polymer and the solvent to dissolve the polymer in the solvent for obtaining a solution, degassing the solution to obtain a spin dope, and transporting the spin dope out of the kneader, wherein the polymer is an aramid polymer and the solvent is sulfuric acid, and whereby the aramid polymer is dosed into the kneader prior to dosing the sulfuric acid into the kneader.
摘要翻译： 一种使用双轴捏和机将芳族聚酰胺聚合物溶解在硫酸中的方法，包括以下步骤：将聚合物和溶剂投入到捏合机中，混合聚合物和溶剂以将聚合物溶解在溶剂中以获得溶液，脱气 溶液以获得旋涂液，并将旋转纺丝液输送出捏合机，其中聚合物是芳族聚酰胺聚合物，溶剂是硫酸，由此在将硫酸加入到捏合机中之前将芳族聚酰胺聚合物加入捏合机中 。
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10.发明授权公开(公告)号：US07527841B2
公开(公告)日：2009-05-05
申请号：US11663980
申请日：2005-10-20
IPC分类号： B29C70/08
CPC分类号： C08J3/05 , B29C47/6068 , B29C47/6075 , C08J2377/10 , D01D1/02 , D01F6/805 , Y10T428/1369 , Y10T428/2913 , Y10T428/2969
摘要： Described is a method for dissolving PPTA or copolymers thereof in sulfuric acid using a twin screw extruder having transporting, mixing, and kneading elements with an entering zone, an intermediate zone, a mixing zone, a negative transport zone, a degassing zone, and a pressure build-up zone. The method includes transporting PPTA or copolymer thereof into the entering zone at a transport capacity low enough as to prevent sulfuric acid entering the entering zone; introducing sulfuric acid in the intermediate zone; essentially fully filling the mixing zone to allow sufficient time to mix and dissolve PPTA or copolymer thereof in the sulfuric acid to obtain a PPTA or copolymer-sulfuric acid solution; creating after the mixing zone a negative transport zone to obtain a product lock between the mixing zone and the degassing zone; creating a thin film of the PPTA or copolymer-sulfuric acid solution in the degassing zone to degas the solution; and entering the solution into the output pressure build-up zone to partially fill this zone and to leave the twin screw extruder.
摘要翻译： 描述了使用具有输送区域，中间区域，混合区域，负运送区域，脱气区域和输送区域的输送，混合和捏合元件的双螺杆挤出机将PPTA或其共聚物溶解在硫酸中的方法。 压力积聚区。 该方法包括以足够低的运输能力将PPTA或其共聚物输送到进入区域中，以防止硫酸进入进入区域; 在中间区引入硫酸; 基本上完全填充混合区以允许足够的时间将PPTA或其共聚物混合并溶解在硫酸中以获得PPTA或共聚物 - 硫酸溶液; 在混合区之后产生负运送区，以在混合区和脱气区之间获得产品锁; 在脱气区中形成PPTA或共聚物 - 硫酸溶液的薄膜，使溶液脱气; 并将溶液进入输出压力累积区以部分填充该区域并离开双螺杆挤出机。
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