Process for alpha-phase metal phthalocyanine pigments
    6.
    发明授权
    Process for alpha-phase metal phthalocyanine pigments 失效
    α-相金属酞菁颜料的制备方法

    公开(公告)号:US5534055A

    公开(公告)日:1996-07-09

    申请号:US295342

    申请日:1994-08-24

    摘要: This invention relates to a process for preparing alpha-phase metal phthalocyanine pigments from crude metal phthalocyanine pigments comprising(a) acid pasting or acid swelling a crude metal phthalocyanine pigment;(b) dry milling the acid-pasted or acid-swelled metal phthalocyanine pigment in the presence of 5 to 50 parts by weight of a stabilizer per 100 parts by weight of the crude metal phthalocyanine pigment until the average particle size is reduced to less than about 0.5 .mu.m;(c) finishing the milled metal phthalocyanine pigment by thoroughly mixing said milled metal phthalocyanine pigment with a finishing solvent mixture comprising 3 to 6 parts by weight, relative to the crude metal phthalocyanine pigment, of water and 0.4 to 1.0 parts by weight, relative to the crude metal phthalocyanine pigment, of an organic solvent, optionally in the presence of 0 to 45 parts by weight of a stabilizer per 100 parts by weight of the crude metal phthalocyanine pigment, with the proviso that the total amount of stabilizer used in steps (b) and (c) ranges from 5 to 50 parts by weight per 100 parts by weight of the crude metal phthalocyanine pigment; and(d) isolating the alpha-phase metal phthalocyanine pigment.

    摘要翻译: 本发明涉及一种由粗金属酞菁颜料制备α-相金属酞菁颜料的方法,包括(a)酸性粘土或酸性溶胀粗金属酞菁颜料; (b)在每100重量份粗金属酞菁颜料存在5至50重量份的稳定剂存在下,将酸性粘合或酸溶胀的金属酞菁颜料干磨,直至平均粒度降至小于 约0.5亩; (c)通过将所述碾磨的金属酞菁颜料与包含3至6重量份的粗金属酞菁颜料的水和0.4至1.0重量份的完整溶剂混合物相对于 有机溶剂的粗金属酞菁颜料,任选地在0至45重量份的稳定剂存在下,每100重量份的粗金属酞菁颜料,条件是步骤中使用的稳定剂的总量 b)和(c)的范围为5至50重量份/ 100重量份的粗金属酞菁颜料; 和(d)分离α-相金属酞菁颜料。

    Solid solutions of copper phthalocyanine compounds
    7.
    发明授权
    Solid solutions of copper phthalocyanine compounds 失效
    铜酞菁化合物的固体溶液

    公开(公告)号:US5248336A

    公开(公告)日:1993-09-28

    申请号:US787852

    申请日:1991-11-05

    CPC分类号: C09B67/0035

    摘要: This invention relates to solid solutions containing (a) about 90 to about 10% by weight of a chlorinated copper phthalocyanine containing about 14 to about 16 atoms of chlorine per molecule and (b) about 10 to about 90% by weight of a copper phthalocyanine containing about 3 to about 4 atoms of chlorine wherein said compositions are characterized by X-ray diffraction patterns that differ from the sum of the X-ray diffraction patterns of the individual components.

    摘要翻译: 本发明涉及含有(a)约90至约10重量%的每分子含有约14至约16个原子氯的氯化铜酞菁和(b)约10至约90重量%的铜酞菁 含有约3至约4个原子的氯,其中所述组合物的特征在于X射线衍射图与不同组分的X射线衍射图的总和不同。

    METHODS FOR INHIBITION OF SCARRING
    8.
    发明申请
    METHODS FOR INHIBITION OF SCARRING 审中-公开
    抑制扫描的方法

    公开(公告)号:US20110166067A1

    公开(公告)日:2011-07-07

    申请号:US13003760

    申请日:2008-12-11

    CPC分类号: A61K38/1841

    摘要: The invention provides new methods of treatment using TGF-β3 to inhibit scarring in humans, and TGF-β3 for new uses in the inhibition of scarring in humans. In a first incidence of treatment TGF-β3 is provided to each centimetre of a wound margin or each centimetre of a site at which a wound is to be formed in a first therapeutically effective amount; and in a subsequent incidence of treatment TGF-β3 is provided to each centimetre of wound margin in a larger therapeutically effective amount of TGF-β3. The incidences of treatment occur between 8 hours and 48 hours apart from one another. The TGF-β3 may be provided by intradermal injection. Also provided are kits and methods of selecting an appropriate treatment regime for inhibiting scarring associated with the healing of a human wound.

    摘要翻译: 本发明提供使用TGF-β3抑制人类瘢痕形成的新治疗方法,以及用于抑制人瘢痕形成的新用途的TGF-β3。 在治疗的第一次发生中,TGF-β1被提供给每个厘米的伤口边缘或每厘米的伤口以第一治疗有效量形成的部位; 并且在随后的治疗发生中,在更大的治疗有效量的TGF-βb中,向伤口边缘的每厘米提供TGF-β; 3。 治疗的发生发生在彼此之间8小时至48小时之间。 TGF-β可以通过皮内注射来提供。 还提供了选择用于抑制与人类伤口愈合相关的瘢痕形成的适当治疗方案的试剂盒和方法。

    Process for conditioning organic pigments
    9.
    发明授权
    Process for conditioning organic pigments 失效
    有机颜料调理方法

    公开(公告)号:US6013126A

    公开(公告)日:2000-01-11

    申请号:US200272

    申请日:1998-11-25

    CPC分类号: C09B67/0017 C09B67/0014

    摘要: This invention relates to a process for conditioning organic pigments by(a) grinding a crude organic pigment at a temperature of about 0.degree. C. to about 100.degree. C. in the presence of (i) about 1 to about 10 parts by weight, relative to the organic pigment, of an inorganic salt and (ii) about 1 to about 5 parts by weight, relative to the organic pigment, of a liquid in which the organic pigment and salt are substantially insoluble, to form a pigment paste;(b) grinding the pigment paste at a temperature of about 0.degree. C. to about 100.degree. C. in the presence of about 0.05 to about 1 parts by weight, relative to the organic pigment, of a C.sub.8 -C.sub.10 alkanoic acid to form a treated pigment paste;(c) stirring the treated pigment paste with water or water containing an acid and/or an organic liquid to complete the conditioning of the organic pigment; and(d) isolating the conditioned organic pigment.

    摘要翻译: 本发明涉及一种通过以下步骤调理有机颜料的方法:(a)在(i)约1至约10重量份的存在下,在约0℃至约100℃的温度下研磨粗有机颜料, 相对于有机颜料,无机盐和(ii)相对于有机颜料约1至约5重量份的有机颜料和盐基本上不溶的液体,以形成颜料糊料; (b)在相对于有机颜料约0.05至约1重量份的存在下,在约0℃至约100℃的温度下研磨颜料糊状物以形成C 8 -C 10链烷酸 经处理的颜料糊; (c)用含有酸和/或有机液体的水或水搅拌经处理的颜料糊,以完成有机颜料的调理; 和(d)分离调节的有机颜料。

    Preparation of phthalocyanine pigments
    10.
    发明授权
    Preparation of phthalocyanine pigments 失效
    酞菁颜料的制备

    公开(公告)号:US5393339A

    公开(公告)日:1995-02-28

    申请号:US241090

    申请日:1994-05-11

    CPC分类号: C09B47/06

    摘要: This invention relates to an improved process for preparing metal phthalocyanine pigments comprising(a) heating at a temperature of about 150.degree. C. to about 200.degree. C. a mixture comprising(i) a phthalocyanine-forming material based on phthalic acid,(ii) at least about 25 mole percent, relative to the phthalocyanine-forming material (i), of a metal donor,(iii) at least about 100 mole percent, relative to the phthalocyanine-forming material (i), of a nitrogen donor,(iv) 1 to about 20 percent by weight, relative to the phthalocyanine-forming material (i), of a catalyst, and(v) about 250 to about 400 percent by weight, relative to the phthalocyanine-forming material (i), of a di(C.sub.1 -C.sub.3 alkyl) phthalate solvent; and(b) isolating the metal phthalocyanine pigment.

    摘要翻译: 本发明涉及一种制备金属酞菁颜料的改进方法,包括(a)在约150℃至约200℃的温度下加热混合物,其包含(i)基于邻苯二甲酸的酞菁形成材料,(ii )相对于形成酞菁的材料(i)至少约25摩尔%的金属供体,(iii)相对于形成酞菁的材料(i)至少约100摩尔%的氮供体, (iv)相对于形成酞菁的材料(i)为约1至约20重量%的催化剂,和(v)相对于形成酞菁的材料(i)为约250至约400重量% 的二(C 1 -C 3烷基)邻苯二甲酸酯溶剂; 和(b)分离金属酞菁颜料。