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公开(公告)号：US20110144325A1
公开(公告)日：2011-06-16
申请号：US13014914
申请日：2011-01-27
IPC分类号： C07D487/22
CPC分类号： C07D403/04 , C07D487/22
摘要： A method of making a porphyrin is carried out by: (a) condensing (i) a 1,9-bis(N,N-)dialkylaminomethyl)dipyrromethane of Formula II: with (ii) a dipyrromethane to produce a reaction product; then (b) oxidizing the reaction product; and then (c) optionally demetallating said reaction product to produce the porphyrin. The reaction is particularly useful for making substituted porphyrins with a wide range of substituents at the A and/or B (the 5 and/or 15) positions.
摘要翻译： 通过以下方法进行卟啉的制备方法：（a）将（ⅰ）式Ⅱ的1,9-双（N，N-）二烷基氨基甲基）二吡咯烷与（ⅱ）二吡咯甲烷缩合生成反应产物; 然后（b）氧化反应产物; 然后（c）任选地使所述反应产物脱金属以产生卟啉。 该反应对于在A和/或B（5和/或15）位置制备具有宽范围取代基的取代卟啉是特别有用的。
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公开(公告)号：US20100173184A1
公开(公告)日：2010-07-08
申请号：US12298345
申请日：2007-11-09
申请人： Ryuji Shiozaki , Asao Iwata , Satoko Kaneko , Nobuo Ando , Masahiko Taniguchi
发明人： Ryuji Shiozaki , Asao Iwata , Satoko Kaneko , Nobuo Ando , Masahiko Taniguchi
CPC分类号： H01M10/0525 , C01G31/00 , C01P2002/72 , C01P2002/88 , C01P2004/03 , C01P2006/40 , H01M4/131 , H01M4/364 , H01M4/485 , H01M4/587 , H01M4/602 , H01M4/622 , H01M4/70 , H01M10/058
摘要： It has been found that when the potentials of the positive electrode and the negative electrode of the lithium ion secondary battery after the electrodes are short-circuited are each within a predetermined range, the battery produces high energy density. That is the present invention provides a lithium ion secondary battery having a positive electrode, a negative electrode and an electrolyte containing a lithium salt and an aprotic organic in which a positive electrode active material is a material allowing lithium ions and/or anions to be reversibly doped thereinto, and a negative electrode active material is a material allowing lithium ions to be reversibly doped thereinto, and the potentials of the positive electrode and the negative electrode after the positive electrode and the negative electrode are short-circuited are each selected to be within a range from 0.5 V to 2.0 V.
摘要翻译： 已经发现，当电极短路后锂离子二次电池的正极和负极的电位都在预定范围内时，电池产生高能量密度。 本发明提供一种具有正极，负极和含有锂盐和非质子性有机物的电解质的锂离子二次电池，其中正极活性物质是允许锂离子和/或阴离子可逆的材料 并且负极活性物质是允许锂离子被可逆地掺杂的材料，正极和负极之间的正极和负极的电位短路，分别选择在 范围从0.5 V到2.0 V.
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公开(公告)号：US07582751B2
公开(公告)日：2009-09-01
申请号：US11193562
申请日：2005-07-29
IPC分类号： C07B47/00
CPC分类号： C07D487/22 , C07D403/04
摘要： A method of making a porphyrin (I) is carried out by condensing (i) a bis(imino)dipyrromethane of Formula II: with (ii) a dipyrromethane to produce a reaction product; then (b) optionally oxidizing said reaction product with an oxidizing agent; and then (c) optionally demetallating said reaction product to produce the porphyrin. Methods of making compounds of Formula II are also described.
摘要翻译： 制备卟啉（I）的方法是通过将（ⅰ）式Ⅱ的双（亚氨基）二吡咯烷与（ⅱ）二吡咯甲烷缩合制备反应产物来进行的; 然后（b）任选地用氧化剂氧化所述反应产物; 然后（c）任选地使所述反应产物脱金属以产生卟啉。 还描述了制备式II化合物的方法。
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公开(公告)号：US20090198049A1
公开(公告)日：2009-08-06
申请号：US12361715
申请日：2009-01-29
IPC分类号： C07D471/22 , C07D403/06
CPC分类号： C07D403/04 , C07D487/22
摘要： A method of making a porphyrin is carried out by: (a) condensing (i) a 1,9-bis(N,N-)dialkylaminomethyl)dipyrromethane of Formula II: with (ii) a dipyrromethane to produce a reaction product; then (b) oxidizing the reaction product; and then (c) optionally demetallating said reaction product to produce the porphyrin. The reaction is particularly useful for making substituted porphyrins with a wide range of substituents at the A and/or B (the 5 and/or 15) positions.
摘要翻译： 通过以下方法进行卟啉的制备方法：（a）将（ⅰ）式Ⅱ的1,9-双（N，N-）二烷基氨基甲基）二吡咯烷与（ⅱ）二吡咯甲烷缩合生成反应产物; 然后（b）氧化反应产物; 然后（c）任选地使所述反应产物脱金属以产生卟啉。 该反应对于在A和/或B（5和/或15）位置制备具有宽范围取代基的取代卟啉是特别有用的。
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公开(公告)号：US20090069558A1
公开(公告)日：2009-03-12
申请号：US12271346
申请日：2008-11-14
申请人： Jonathan S. Lindsey , Masahiko Taniguchi , Doyoung Ra , Guoning Mo , Thiagarajan Balasubramanian
发明人： Jonathan S. Lindsey , Masahiko Taniguchi , Doyoung Ra , Guoning Mo , Thiagarajan Balasubramanian
IPC分类号： C07D487/22 , C07D401/14 , C07D401/12
CPC分类号： C07D207/33 , C07D207/335 , C07D207/34 , C07D207/46
摘要： A method of making chlorins comprises the steps of reacting (e.g. condensing) a dipyrrin western half intermediate with an eastern half intermediate to form a tetrahydrobilene, and then cyclizing the tetrahydrobilene to form a chlorin. Intermediates including tetrahydrobilenes useful in such reactions are also described.
摘要翻译： 制备二氢卟酚的方法包括使双吡啶西半中间体与东半中间体反应（例如缩合）以形成四氢苯乙烯的步骤，然后环化四氢苯并形成二氢卟酚。 还描述了包括在这种反应中有用的四氢噻吩的中间体。
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公开(公告)号：US20080299455A1
公开(公告)日：2008-12-04
申请号：US12127989
申请日：2008-05-28
申请人： Ryuji Shiozaki , Nobuo Ando , Satoko Kaneko , Masahiko Taniguchi
发明人： Ryuji Shiozaki , Nobuo Ando , Satoko Kaneko , Masahiko Taniguchi
CPC分类号： H01M4/131 , H01G11/46 , H01G11/50 , H01G11/86 , H01M4/133 , H01M4/1391 , H01M4/1393 , H01M10/0525 , Y02E60/13 , Y02T10/7011 , Y02T10/7022 , Y10T29/49108
摘要： An electrode laminate unit 12 of an electric storage device 10 is composed of positive electrodes 14 and negative electrodes 15, which are alternately laminated, and a lithium electrode 16 is arranged at the outermost part of the electrode laminate unit 12 so as to oppose to the negative electrode 15. A charging/discharging unit 21 having first and second energization control units 21a and 21b is connected to a positive-electrode terminal 18, negative-electrode terminal 19, and a lithium-electrode terminal 20. Electrons are moved from the lithium electrode 16 to the positive electrode 14 through the first energization control unit 21a, and lithium ions are doped into the positive electrode 14 from the lithium electrode 16. Electrons are moved from the lithium electrode 16 to the negative electrode 15 through the second energization control unit 21b, and lithium ions are doped into the negative electrode 15 from the lithium electrode 16. The lithium ions are doped into both of the positive electrode 14 and the negative electrode 15 as described above, whereby the doping time can dramatically be shortened.
摘要翻译： 蓄电装置10的电极层叠单元12由交替层叠的正极14和负极15构成，锂电极16配置在电极层叠单元12的最外侧，以与电极层叠单元12相对。 负极15.具有第一和第二通电控制单元21a和21b的充电/放电单元21连接到正极端子18，负极端子19和锂电极端子20.电子从锂 电极16通过第一通电控制单元21a连接到正极14，并且锂离子从锂电极16掺杂到正极14中。电子通过第二通电控制单元从锂电极16移动到负极15 21b，并且锂离子从锂电极16掺杂到负极15中。锂离子掺杂到两者中 如上所述，由此可以显着地缩短掺杂时间。
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公开(公告)号：US20070196777A1
公开(公告)日：2007-08-23
申请号：US11606882
申请日：2006-12-01
IPC分类号： G03C1/00
CPC分类号： G03C1/498 , G03C1/46 , G03C1/49827 , G03C1/49863 , G03C5/02 , G03C7/3041 , G03C7/344 , G03C7/346 , G03C7/36 , G03C7/383 , G03C7/3835 , G03C7/384 , G03C2200/36
摘要： The present invention provides a black and white photothermographic material having, a first image forming layer including at least a photosensitive silver halide, a non-photosensitive organic silver salt, and a reducing agent for silver ions, wherein the black and white photothermographic material further has a second image forming layer including at least a coupler, and at least one of the first image forming layer and the second image forming layer includes a color developing agent. A black and white photothermographic material which exhibits high sensitivity, excellent image tone, and excellent storage stability is provided.
摘要翻译： 本发明提供一种黑色和白色光热敏成像材料，其具有至少包含感光卤化银，非感光性有机银盐和银离子还原剂的第一图像形成层，其中黑色和白色光热敏成像材料还具有 至少包括耦合器的第二图像形成层，并且所述第一图像形成层和所述第二图像形成层中的至少一个包括彩色显影剂。 提供了具有高灵敏度，优异的图像色调和优异的储存稳定性的黑白光热敏成像材料。
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公开(公告)号：US20070065764A1
公开(公告)日：2007-03-22
申请号：US11522355
申请日：2006-09-18
IPC分类号： G03C1/00
CPC分类号： G03C1/49845 , G03C1/0051 , G03C1/09 , G03C1/498 , G03C1/49818 , G03C1/49827 , G03C5/17 , G03C7/32 , G03C2001/03558 , G03C2001/091 , G03C2001/7425
摘要： The present invention provides a black and white photothermographic material having, on a support, an image forming layer including at least a photosensitive silver halide, a non-photosensitive organic silver salt, and a compound represented by the following formula (1): wherein R101, R102, R104, and R105 each independently represent a hydrogen atom or a substituent; R103 represents a halogen atom, an alkyl group, an alkoxy group, an aryloxy group, an alkylthio group, an arylthio group, an acylamino group, or a sulfonylamino group; and P represents a group forming a phenol compound represented by formula (2) by cleavage of the O—P bond at the time of thermal development.
摘要翻译： 本发明提供一种黑色和白色光热敏成像材料，其在载体上具有至少包含光敏卤化银，非感光性有机银盐和由下式（1）表示的化合物的成像层：其中R R 102，R 104和R 105各自独立地表示氢原子或取代基; R 1，R 2，R 2， R 103表示卤素原子，烷基，烷氧基，芳氧基，烷硫基，芳硫基，酰氨基或磺酰氨基; P表示通过在热显影时裂解O-P键而形成由式（2）表示的酚化合物的基团。
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公开(公告)号：US20070027312A1
公开(公告)日：2007-02-01
申请号：US11193562
申请日：2005-07-29
IPC分类号： C07D487/22 , C07D403/02
CPC分类号： C07D487/22 , C07D403/04
摘要： A method of making a porphyrin (I) is carried out by condensing (i) a bis(imino)dipyrromethane of Formula II: with (ii) a dipyrromethaneto produce a reaction product; then (b) optionally oxidizing said reaction product with an oxidizing agent; and then (c) optionally demetallating said reaction product to produce the porphyrin. Methods of making compounds of Formula II are also described.
摘要翻译： 制备卟啉（I）的方法是通过将（ⅰ）式Ⅱ的双（亚氨基）二吡咯烷与（ⅱ）二吡咯甲烷缩合制备反应产物而进行的; 然后（b）任选地用氧化剂氧化所述反应产物; 然后（c）任选地使所述反应产物脱金属以产生卟啉。 还描述了制备式II化合物的方法。
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公开(公告)号：US07022862B2
公开(公告)日：2006-04-04
申请号：US10641412
申请日：2003-08-15
IPC分类号： C07D207/30
CPC分类号： C07D207/323
摘要： A (preferably nonaqueous) method of making a dipyrromethane is described. The comprises the steps of: (a) providing a reaction system consisting essentially of an aldehyde or acetal, excess pyrrole and a catalyst; (b) reacting the aldehyde or acetal with the pyrrole in the reaction system to form the dipyrromethane therein; (c) quenching the reaction system by adding a base thereto (preferably without simultaneously or concurrently adding water and/or an organic solvent thereto); (d) separating the catalyst from the reaction system; and then (e) separating the pyrrole from the reaction system to produce the dipyrromethane as a residual
摘要翻译： 描述了制备二吡咯甲烷的（优选非水性）的方法。 包括以下步骤：（a）提供基本上由醛或缩醛，过量吡咯和催化剂组成的反应体系; （b）在反应体系中使醛或缩醛与吡咯反应，形成其中的二吡咯烷; （c）通过向其中加入碱（优选不同时或同时向其中加入水和/或有机溶剂）淬灭反应体系; （d）将催化剂与反应体系分离; 然后（e）从反应体系中分离出吡咯以产生作为残余物的二吡咯烷
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