公开(公告)号：US20170173492A1

公开(公告)日：2017-06-22

申请号：US15382073

申请日：2016-12-16

申请人： BASF SE

发明人： Ulrich HAMMON ,  Thomas WALTER

IPC分类号： B01D3/32 ,  C07C67/52 ,  B01D53/18 ,  B01D3/22 ,  B01D3/26

CPC分类号： B01D3/324 ,  B01D3/20 ,  B01D3/205 ,  B01D3/225 ,  B01D3/26 ,  B01D3/32 ,  B01D53/18 ,  C07C51/42 ,  C07C51/44 ,  C07C67/52 ,  C07C57/04

摘要： The present invention relates to a column (1) for thermal treatment of fluid mixtures, having a cylindrical, vertically aligned column body (2) which forms a column cavity (3), having a sequence of vertically spaced-apart dual-flow mass transfer trays (8) which are mounted in the column cavity (3) and which have orifices for passage of liquid and gas in countercurrent, and having at least one gas entry orifice (5) disposed below the lowermost of the sequence of dual-flow mass transfer trays (8). It is a characteristic feature of the column of the invention that a gas distribution tray (9) which is disposed between the lowermost of the sequence of dual-flow mass transfer trays (8) and the gas entry orifice (5) has orifices (32) for vertical passage of gas which can be introduced into the column cavity (3) via the gas entry orifice (5), the orifices (32) being formed so as to bring about equal gas distribution over the column cross section. The invention further relates to a process for thermal treatment of fluid mixtures in such a column (1).

公开(公告)号：US09314709B2

公开(公告)日：2016-04-19

申请号：US13819923

申请日：2011-09-01

申请人： Ichiro Minami ,  Masajiro Sakurai ,  Yasuo Suzuki

发明人： Ichiro Minami ,  Masajiro Sakurai ,  Yasuo Suzuki

IPC分类号： B01F3/04 ,  B01D3/32 ,  B01J19/32

CPC分类号： B01J19/32 ,  B01D3/26 ,  B01D3/28 ,  B01D3/32 ,  B01F3/04078 ,  B01J2219/3221 ,  B01J2219/32213 ,  B01J2219/32227 ,  B01J2219/32231 ,  B01J2219/32262 ,  B01J2219/32268 ,  B01J2219/32272 ,  B01J2219/32408 ,  B01J2219/3325

摘要： In existing structured packing, performance depends on effective contacting area. Performance decreases in cases having high surface tensions such mixtures containing a lot of water. Such mixtures are difficult to wet the packing surface. The present invention prevents liquid from intersecting the crease of the corrugation and from falling into a free space. Further, liquid flowing into the slot makes frequent liquid and vapor interfacial update resulting in positive utilization of the wetted area. The most important point of this invention is taking a positive utilization of the wetted area. The most important point of this invention is taking a large value of 3.5 or more of P/H (pitch/height of the crimp) and providing the horizontal slot on the crease, resulting in adding the flow reversal mechanism and frequent interfacial update.

摘要翻译： 在现有的结构化包装中，性能取决于有效的接触面积。 在具有高表面张力的情况下性能下降，这种混合物含有大量的水。 这种混合物难以润湿包装表面。 本发明防止液体与波纹褶皱相交并落入自由空间。 此外，流入狭槽的液体使液体和蒸气界面更新频繁，导致润湿区域的积极利用。 本发明最重要的一点是积极利用湿润区域。 本发明的最重要的一点是要获得3.5以上的P / H（压接高度），并且在折痕上提供水平槽，从而增加流动反转机构和频繁的界面更新。

公开(公告)号：US20160083267A1

公开(公告)日：2016-03-24

申请号：US14857998

申请日：2015-09-18

申请人： BASF SE

发明人： Ulrich HAMMON ,  Thomas WALTER ,  Christian RAITH

IPC分类号： C02F1/04 ,  B01D3/26 ,  B01D1/00 ,  C02F1/16

CPC分类号： C02F1/048 ,  B01D1/0058 ,  B01D3/26 ,  B01D3/346 ,  C02F1/16 ,  C02F2103/36 ,  C02F2303/10 ,  C07C51/44 ,  C07C57/04 ,  Y02W10/30

摘要： The present invention relates to a process for treating secondary components obtained in acrolein and/or (meth)acrylic acid production, comprising the steps of: a) contacting at least one wastewater stream (201) comprising at least a portion of the water of reaction removed in a first stage of a saturation column (101) with at least one process offgas stream (203), b) introducing energy by means of a first heat transferer (103) provided in a first saturation circuit (301) into the first stage of the saturation column (101), c) partly vaporizing the wastewater stream (201) into the process offgas stream (203) and passing the combined gas stream (205) into a second stage of the saturation column (101), d) drawing off a concentrated wastewater stream (207) from the bottom (1011) of the first stage of the saturation column (101) and feeding it to the top (1023) of the second stage of the saturation column (101), e) introducing energy by means of a second heat transferer (105) provided in a second circuit (303) into the second stage of the saturation column (101), f) partly vaporizing the concentrated wastewater stream (207) into the combined gas stream (205) to obtain an offgas stream (209), g) superheating the offgas stream (209), after it has been saturated, in a third heat transferer (113) to obtain a superheated offgas stream (211) and h) transferring the offgas stream (209) or the superheated offgas stream (211) from the saturation column (101) to a thermal aftertreatment. The present invention further relates to a plant (1) for treating the secondary components obtained in acrolein and/or (meth)acrylic acid production.

摘要翻译： 本发明涉及一种用于处理由丙烯醛和/或（甲基）丙烯酸生产获得的二次成分的方法，包括以下步骤：a）使至少一个包含至少一部分反应水的废水流（201） 在具有至少一个工艺废气流（203）的饱和塔（101）的第一级中去除，b）通过设置在第一饱和电路（301）中的第一热传递器（103）将能量引入第一级 的饱和塔（101），c）将废水流（201）部分蒸发到工艺废气流（203）中，并将组合气流（205）送入饱和塔（101）的第二级，d） 从饱和塔（101）的第一级的底部（1011）离开浓缩废水流（207）并将其供给到饱和塔（101）的第二级的顶部（1023），e）引入能量 通过设置在其中的第二传热器（105） 第二回路（303）进入饱和塔（101）的第二阶段，f）将浓缩废水流（207）部分汽化成合并气流（205）以获得废气流（209），g）使废气过热 （209）或过热废气流（211）从饱和塔（209）中转移出来，在第三热转移器（113）中， （101）进行热后处理。 本发明还涉及用于处理在丙烯醛和/或（甲基）丙烯酸生产中获得的二次成分的设备（1）。

公开(公告)号：US20150315106A2

公开(公告)日：2015-11-05

申请号：US14462083

申请日：2014-08-18

申请人： Ortloff Engineers, Ltd. ,  S.M.E. Products LP

发明人： Scott A. Miller ,  John D. Wilkinson ,  Joe T. Lynch ,  Hank M. Hudson ,  Kyle T. Cuellar ,  Andrew F. Johnke ,  W. Larry Lewis

IPC分类号： C07C7/09 ,  F25J1/00

CPC分类号： C07C7/09 ,  B01D3/26 ,  B01D3/32 ,  B01D3/322 ,  B01D5/0063 ,  C10G5/06 ,  C10L3/06 ,  C10L2290/06 ,  C10L2290/48 ,  C10L2290/541 ,  C10L2290/543 ,  C10L2290/545 ,  F25J1/0022

摘要： A process and an apparatus are disclosed for a compact processing assembly to remove C5 and heavier hydrocarbon components from a hydrocarbon gas stream. The hydrocarbon gas stream is expanded to lower pressure and supplied to the processing assembly between an absorbing means and a mass transfer means. A distillation vapor stream is collected from the upper region of the absorbing means and cooled in a first heat and mass transfer means inside the processing assembly to partially condense it, forming a residual vapor stream and a condensed stream. The condensed stream is supplied to the absorbing means at its top feed point. A distillation liquid stream is collected from the lower region of the mass transfer means and directed into a second heat and mass transfer means inside the processing assembly to heat it and strip out its volatile components.

摘要翻译： 公开了一种用于紧凑加工组件以从烃气流中除去C5和较重烃组分的方法和装置。 将烃气流膨胀到较低的压力，并在吸收装置和传质装置之间提供给加工组件。 蒸馏蒸汽流从吸收装置的上部区域收集，并在加工组件内部的第一热传质装置中冷却，以使其部分冷凝，形成残余蒸气流和冷凝流。 冷凝流在其顶部进料点处供应到吸收装置。 蒸馏液体流从质量传递装置的下部区域收集并且被引导到处理组件内部的第二热和质量传递装置中，以加热它并剥离其挥发性组分。

公开(公告)号：US08591704B2

公开(公告)日：2013-11-26

申请号：US12933130

申请日：2009-03-20

申请人： Stephen Shelley

发明人： Stephen Shelley

IPC分类号： B01D1/16 ,  B01D1/26 ,  B01D3/42 ,  B01D9/02 ,  C02F9/00 ,  C02F1/04

CPC分类号： B01D1/16 ,  B01D1/26 ,  B01D3/14 ,  B01D3/26 ,  B01D5/006

摘要： A fractionation process for producing at least two concentration fractions of a fluid including a solute, suspended or dissolved content using at least two fluidly connected evaporator units is provided. The process includes the steps of: feeding a feed fluid including a solute, suspended or dissolved content into at least a first evaporator unit; evaporating a first amount of fluid from the feed fluid in at least the first evaporator unit to produce a first concentrated fluid; feeding at least a portion of the first concentrated fluid into at least a second evaporator unit; and evaporating a second amount of fluid from the first concentrated fluid in at least the second evaporator unit to produce a second concentrated fluid.

摘要翻译： 提供了使用至少两个流体连接的蒸发器单元来产生包括溶质，悬浮或溶解内容物的流体的至少两个浓度分数的分馏方法。 该方法包括以下步骤：将包含溶质，悬浮或溶解的物质的进料流送入至少第一蒸发器单元; 在至少第一蒸发器单元中从进料流体蒸发第一量的流体以产生第一浓缩流体; 将至少一部分所述第一浓缩流体输送到至少第二蒸发器单元中; 并在至少第二蒸发器单元中从第一浓缩流体蒸发第二量的流体以产生第二浓缩流体。

公开(公告)号：US20040179982A1

公开(公告)日：2004-09-16

申请号：US10483811

申请日：2004-01-15

发明人： Tsunezo Inaba ,  Fumio Abe ,  Takeyoshi Kawahara ,  Yukio Miyairi

IPC分类号： B01J035/02

CPC分类号： B01D53/18 ,  B01D3/20 ,  B01D3/26 ,  B01J10/007 ,  B01J19/2485 ,  B01J19/32 ,  B01J2219/32296 ,  F28C3/06

摘要： There is provided a liquid-to-gas contact device comprising: a liquid-to-gas contact medium which is a honeycomb structural body formed of a porous material including a plurality of through channels defined by a plurality of partition walls and extending through the structural body in an axial direction, and including a plurality of flow passages extending through the honeycomb structural body from an outer peripheral surface side and formed isolatedly from the through channels; and a container which includes a gas inlet, a gas outlet, a liquid supply port, a storage tank for liquid, and, if desired, a liquid discharge port and in which the liquid-to-gas contact medium is to be stored. A capillarity phenomenon function possessed by the liquid-to-gas contact medium is used to provide the device which has a superior thermal efficiency and which can be constituted to be simple and compact.

摘要翻译： 提供了一种液 - 气接触装置，包括：液 - 气接触介质，其是由多孔材料形成的蜂窝结构体，所述多孔材料包括由多个隔壁限定并延伸穿过结构的多个通道 并且包括从外周面侧延伸穿过所述蜂窝结构体的多个流路，并且与所述通道隔离形成; 以及容器，其包括气体入口，气体出口，液体供应口，用于液体的储存罐，以及如果需要的话，液体排出口将存储液体与气体的接触介质。 使用液体 - 气体接触介质所具有的毛细管现象功能来提供具有优异的热效率并且可以被构造成简单紧凑的装置。

公开(公告)号：US20040065966A1

公开(公告)日：2004-04-08

申请号：US10267136

申请日：2002-10-08

发明人： Morten Muller

IPC分类号： C10J001/08

CPC分类号： C10G49/002 ,  B01D3/20 ,  B01D3/26 ,  B01J8/0278 ,  B01J8/0492

摘要： Vapor and liquid passing downward through a vessel are brought into contact within a plurality of distributor assemblies arranged across a horizontal distribution tray located within the vessel. The distributor assemblies have fluid flow paths with different resistances to fluid flow, as by having vapor inlets of at least two different sizes, with the differently sized inlets being located on different assemblies or on different upflow channels of the same assembly. This provides different vapor flow rates and liquid flow rates in different upflow channels. The invention improves the uniformity of liquid distribution over the cross section of the vessel despite elevational differences in liquid levels on the distribution tray or changes in the vapor and or liquid flow rates through the reactor.

摘要翻译： 通过容器向下流动的蒸气和液体在多个分配器组件内接触，多个分配器组件布置成横跨位于容器内的水平分配盘。 分配器组件具有对流体流动具有不同电阻的流体流动路径，如通过具有至少两个不同尺寸的蒸气入口，其中不同尺寸的入口位于不同组件上或同一组件的不同向上流动通道上。 这提供不同的上流通道中不同的蒸汽流速和液体流速。 本发明改善了在容器横截面上的液体分布的均匀性，尽管分配托盘上的液面高度差异或通过反应器的蒸汽和/或液体流速的变化。

公开(公告)号：US4863568A

公开(公告)日：1989-09-05

申请号：US55673

申请日：1987-05-29

申请人： Enno F. Wijn

发明人： Enno F. Wijn

IPC分类号： B01D3/10 ,  B01D3/00 ,  B01D3/26

CPC分类号： B01D3/008 ,  B01D3/26

摘要： An apparatus for the fractional distillation of a liquid under vacuum is disclosed in which first and second inlets are disposed in the upper portion of a normally vertically closed vessel for the entrance of a liquid to be distilled and a cooling liquid, respectively and outlets are provided in the bottom portion of the vessel for the residue for the liquid being distilled and for the cooling liquid. First and second distribution means are provided for establishing thin sheets of liquid to be distilled and cooling liquid wherein each thin sheet falls freely absent both support and guiding means. Means are also provided for separately collecting the liquid distillate with the cooling liquid in the residue of the liquid to be distilled.

摘要翻译： 公开了一种用于在真空下分馏液体的装置，其中第一和第二入口分别设置在正常垂直密封的容器的上部，用于分别输入待蒸馏的液体和冷却液体，并且提供出口 在容器的底部，用于待蒸馏的液体的残余物和冷却液体。 提供第一和第二分配装置用于建立要被蒸馏的液体的薄片和冷却液体，其中每个薄片在支撑和引导装置两者都自由地落下。 还提供了用于在待蒸馏的液体的残余物中单独收集液体馏出物与冷却液的装置。

公开(公告)号：US4152196A

公开(公告)日：1979-05-01

申请号：US762244

申请日：1977-01-25

申请人： Ulrich Buhlmann

发明人： Ulrich Buhlmann

IPC分类号： B01D3/26 ,  B01D1/14

CPC分类号： B01D3/26 ,  Y10S159/08

摘要： The column employs a head section with a counterflow column, a bottom section with a counterflow column and a plurality of reaction stages for stripping metal salts via steam from ammoniacal solutions or suspensions. Each reaction stage has a floor, a pipe defining a laterally confined chamber, an outlet and a valve in the outlet to control the discharge of liquid. At least one steam line communicates the upper end of each stage with the pipe in the next uppermost stage. Incrustation of the column by the stripped salts is reduced by the high velocity of flow in the bubble bed in each stage.

摘要翻译： 该柱采用具有逆流塔的顶部部分，具有逆流塔的底部部分和用于通过来自氨溶液或悬浮液的蒸汽汽提金属盐的多个反应阶段。 每个反应级具有底板，限定侧向限制室的管，出口和出口中的阀，以控制液体的排放。 至少一个蒸汽管线将每个阶段的上端与下一个最上段的管道连通。 通过在每个阶段的气泡床中的高速度流动，通过汽提的盐对塔柱的去除被降低。

公开(公告)号：US3779525A

公开(公告)日：1973-12-18

申请号：US3779525D

申请日：1971-08-19

申请人： MITSUI SHIPBUILDING ENG

发明人： TANIGAWA S ,  YOKOYAMA T ,  KARAKAWA K

IPC分类号： B01D3/26

CPC分类号： B01D3/26

摘要： A gas-liquid contacting apparatus provided with vertically spaced trays having gas flow aperture therein and a contacting structure provided on the trays surrounding the gas flow aperture. The contacting structure has a cover for preventing gas and liquid to ascending and a perforated plate for breaking gas and liquid mixing flow therein.

摘要翻译： 气液接触装置设置有在其中具有气流孔的垂直间隔的托盘，以及设置在围绕气体流通孔的托盘上的接触结构。 接触结构具有用于防止气体和液体上升的盖和用于破坏气体和液体混合流的多孔板。