APPARATUS FOR REMOVING RESIDUAL MONOMERS
    3.
    发明公开

    公开(公告)号:US20230295352A1

    公开(公告)日:2023-09-21

    申请号:US18006232

    申请日:2021-07-16

    摘要: The present disclosure relates to an apparatus for removing residual monomers and, more specifically, to an apparatus for removing residual monomers, the apparatus being capable of preventing, during the removal of volatile materials by supplying a gas to a flowing distillation material, the formation of dead zones in which the distillation material does not flow or the flow rate thereof decreases. The apparatus for removing residual monomers, of the present disclosure, comprises: a main body capable of supplying a gas to a distillation material accommodated therein; distillation material supply part which is provided at the upper part of the main body and through which the distillation material is injected; a gas inflow part which is provided at the lower part of the main body and through which the gas is injected; a discharge part which is provided at the upper part of the main body, and which discharges volatile materials separated, by means of the gas, from the distillation material; a recovery part, which is provided at the lower part of the main body and recovers the distillation material from which the volatile materials have been removed; a plurality of trays which are provided inside the main body, and each of which has through-holes and a spiral channel; and a downcomer which is provided between the trays, and which is a moving passage through which the distillation material moves downward from the upper part of the main body.

    METHOD FOR CLEANING AQUEOUS WASTEWATER STREAMS LOADED WITH NITROBENZENE

    公开(公告)号:US20230234859A1

    公开(公告)日:2023-07-27

    申请号:US17996954

    申请日:2021-04-24

    摘要: The present invention relates to a process for purifying a wastewater stream WW1 contaminated with nitrobenzene, comprising (I) stripping of the wastewater stream WW1 with a stripping gas SG1 in a continuously operated stripping column to obtain a wastewater stream WW2 which contains nitrobenzene in a concentration reduced relative to WW1 (cNB,WW2), (II) further purification of the wastewater stream WW2 in a wastewater treatment plant, wherein a target value (cNB,WW2,TARGET) is specified for the concentration of nitrobenzene in the wastewater stream WW2, which is greater than zero but takes into account the requirements of the wastewater treatment plant for the maximum content of nitrobenzene in the wastewater streams supplied thereto, wherein, for at least one combination of specified boundary conditions of (a) nitrobenzene concentration in WW1, (b) the temperature of WW1, and (c) the temperature of SG1, a set of linear mathematical relationships of the type mSG1=x·mWW1 is stored in a database, which linear mathematical relationships define a range of concentrations of nitrobenzene in WW2, wherein the set comprises, in addition to a mathematical relationship (0) which corresponds to the target value cNB,WW2,TARGET, at least a first mathematical relationship (1) for a first value of cNB,WW2, which corresponds to 98% of the target value cNB,WW2,TARGET, and a second linear mathematical relationship (2) for a second value of cNB,WW2, which corresponds to 102% of the target value cNB,WW2,TARGET, and wherein the flow rate of the stripping gas is adapted to the flow rate of the wastewater WW1 such that the flow rate of WW1 is within a range of values (AB) that is generated by the first mathematical relationship (1) and the second mathematical relationship (2) at the respective flow rate of WW1, and controlling the concentration of nitrobenzene in WW2 (cNB,WW2) by adjusting the flow rate of stripping gas SG1 accordingly in the event of a measured actual value of this concentration which is outside a window of >98% to

    STRUCTURED PACKING FOR GAS-LIQUID MASS TRANSFER UNIT
    6.
    发明申请
    STRUCTURED PACKING FOR GAS-LIQUID MASS TRANSFER UNIT 审中-公开
    用于气液传质装置的结构包装

    公开(公告)号:US20160250616A1

    公开(公告)日:2016-09-01

    申请号:US15053329

    申请日:2016-02-25

    IPC分类号: B01J19/32 B01D3/26

    摘要: In existing structured packing, performance depends on effective contacting area. Performance decreases in cases having high surface tensions such mixtures containing a lot of water. Such mixtures are difficult to wet the packing surface. The present invention prevents liquid from intersecting the crease of the corrugation and from falling into a free space. Further, liquid flowing into the slot makes frequent liquid and vapor interfacial update resulting in positive utilization of the wetted area. The most important point of this invention is taking a large value of 3.5 or more of P/H (pitch/height of the crimp) and providing the horizontal slot on the crease, resulting in adding the flow reversal mechanism and frequent interfacial update.

    摘要翻译: 在现有的结构化包装中,性能取决于有效的接触面积。 在具有高表面张力的情况下性能下降,这种混合物含有大量的水。 这种混合物难以润湿包装表面。 本发明防止液体与波纹褶皱相交并落入自由空间。 此外,流入狭槽的液体使液体和蒸气界面更新频繁,导致润湿区域的积极利用。 本发明的最重要的一点是要获得3.5以上的P / H(压接高度),并且在折痕上提供水平槽,从而增加流动反转机构和频繁的界面更新。

    Method for producing glycolide, which is provided with rectification step by means of gas-liquid countercurrent contact, and method for purifying crude glycolide
    7.
    发明授权
    Method for producing glycolide, which is provided with rectification step by means of gas-liquid countercurrent contact, and method for purifying crude glycolide 有权
    提供通过气液逆流接触的精馏步骤的乙交酯的制备方法和纯化粗乙交酯的方法

    公开(公告)号:US09365536B2

    公开(公告)日:2016-06-14

    申请号:US14433162

    申请日:2013-11-19

    摘要: A method for producing glycolide provided with: step (1) wherein a GAO composition, which preferably contains a high-boiling-point organic solvent or a solubilizing agent, is supplied into a reactor and heated to a temperature at which a depolymerization reaction of the GAO occurs; step (2) wherein the heating is continued to subject the GAO to the depolymerization reaction, thereby producing glycolide; step (3) wherein glycolide is distilled out of the reactor; step (4) wherein the distillate is introduced into a rectifier and is rectified by means of gas-liquid countercurrent contact; and step (5) wherein glycolide is recovered. A method for purifying crude glycolide provided with: step (i) wherein a crude glycolide composition, which preferably contains a high-boiling-point organic solvent or a solubilizing agent, is supplied into a reactor and heated so that glycolicde is distilled; step (ii) wherein the distillate is introduced into a rectifier and is rectified by means of gas-liquid countercurrent contact; and step (iii) wherein glycolide is recovered. A glycolide producing apparatus and a crude glycolide purifying apparatus, each of which is provided with a reactor and a rectifier.

    摘要翻译: 一种生产乙交酯的方法,其具有:步骤(1),其中将优选含有高沸点有机溶剂或增溶剂的GAO组合物供入反应器中,并加热至其中解聚反应的温度 GAO发生; 步骤(2),其中继续加热使GAO经历解聚反应,由此生成乙交酯; 步骤(3)其中将乙交酯从反应器中蒸出; 步骤(4),其中将馏出物引入整流器并通过气液逆流接触进行整流; 和回收乙交酯的步骤(5)。 提供粗品乙交酯的方法,其具有:步骤(i),其中将优选含有高沸点有机溶剂或增溶剂的粗乙醇酸组合物供入反应器中并加热使乙醇转化; 步骤(ii)其中将馏出物引入整流器并通过气液逆流接触进行精馏; 和回收乙交酯的步骤(iii)。 一种乙交酯生产装置和一种粗乙醇酸提纯装置,每个装置设有反应器和整流器。

    MARINE EXHAUST GAS SCRUBBER
    8.
    发明申请
    MARINE EXHAUST GAS SCRUBBER 有权
    海洋排气管

    公开(公告)号:US20160016109A1

    公开(公告)日:2016-01-21

    申请号:US14759802

    申请日:2014-02-21

    发明人: Peter STRANDBERG

    摘要: A vertical scrubber (1) for exhaust gas from a marine vessel is described. An exhaust gas tube (2) is substantially coaxially arranged through the bottom of a lower scrubbing chamber (3) and is released though an exhaust gas outlet (20) being coaxially arranged through the top of an upper scrubbing chamber (13). A lower scrubbing chamber deflection body (4) is arranged above the opening of the exhaust gas tube (2) for redirecting the exhaust gas towards the walls of the scrubber and create turbulent gas flow, where one or more lower chamber water injector(s) (6, 6′) is (are) arranged above the lower scrubbing chamber deflection body (4), to introduce scrubbing water, and where a lower chamber exhaust gas outlet (12) is arranged at the top of the lower scrubbing chamber (3) as a coaxial constriction, for withdrawing the partly scrubbed exhaust gas from the first scrubbing chamber and introducing the gas into the upper scrubbing chamber (13).

    摘要翻译: 描述了用于来自海洋船舶的废气的垂直洗涤器(1)。 排气管(2)通过下洗涤室(3)的底部基本上同轴地布置,并且通过排气出口(20)被释放,废气出口(20)通过上洗涤室(13)的顶部同轴布置。 下部洗涤室偏转体(4)布置在排气管(2)的开口上方,用于将废气朝向洗涤器的壁重新引导并产生湍流气流,其中一个或多个下室喷水器 (6,6')布置在下洗涤室偏转体(4)的上方,以引入洗涤水,并且其中下室排气出口(12)布置在下洗涤室(3)的顶部 )作为同轴收缩,用于从第一洗涤室中抽出部分洗涤的废气并将气体引入上洗涤室(13)。

    METHOD FOR PRODUCING GLYCOLIDE, WHICH IS PROVIDED WITH RECTIFICATION STEP BY MEANS OF GAS-LIQUID COUNTERCURRENT CONTACT, AND METHOD FOR PURIFYING CRUDE GLYCOLIDE
    9.
    发明申请
    METHOD FOR PRODUCING GLYCOLIDE, WHICH IS PROVIDED WITH RECTIFICATION STEP BY MEANS OF GAS-LIQUID COUNTERCURRENT CONTACT, AND METHOD FOR PURIFYING CRUDE GLYCOLIDE 有权
    通过气体反相电流接触装置进行修正步骤生产甘油的方法以及用于净化甘露糖的方法

    公开(公告)号:US20150259320A1

    公开(公告)日:2015-09-17

    申请号:US14433162

    申请日:2013-11-19

    IPC分类号: C07D319/12 B01J19/24

    摘要: A method for producing glycolide provided with: step (1) wherein a GAO composition, which preferably contains a high-boiling-point organic solvent or a solubilizing agent, is supplied into a reactor and heated to a temperature at which a depolymerization reaction of the GAO occurs; step (2) wherein the heating is continued to subject the GAO to the depolymerization reaction, thereby producing glycolide; step (3) wherein glycolide is distilled out of the reactor; step (4) wherein the distillate is introduced into a rectifier and is rectified by means of gas-liquid countercurrent contact; and step (5) wherein glycolide is recovered. A method for purifying crude glycolide provided with: step (i) wherein a crude glycolide composition, which preferably contains a high-boiling-point organic solvent or a solubilizing agent, is supplied into a reactor and heated so that glycolicde is distilled; step (ii) wherein the distillate is introduced into a rectifier and is rectified by means of gas-liquid countercurrent contact; and step (iii) wherein glycolide is recovered. A glycolide producing apparatus and a crude glycolide purifying apparatus, each of which is provided with a reactor and a rectifier.

    摘要翻译: 一种生产乙交酯的方法,其具有:步骤(1),其中将优选含有高沸点有机溶剂或增溶剂的GAO组合物供入反应器中,并加热至其中解聚反应的温度 GAO发生; 步骤(2),其中继续加热使GAO经历解聚反应,由此生成乙交酯; 步骤(3)其中将乙交酯从反应器中蒸出; 步骤(4),其中将馏出物引入整流器并通过气液逆流接触进行整流; 和回收乙交酯的步骤(5)。 提供粗品乙交酯的方法,其具有:步骤(i),其中将优选含有高沸点有机溶剂或增溶剂的粗乙醇酸组合物供入反应器中并加热使乙醇转化; 步骤(ii)其中将馏出物引入整流器并通过气液逆流接触进行精馏; 和回收乙交酯的步骤(iii)。 一种乙交酯生产设备和一种粗乙醇酸提纯设备,每个设备都设有电抗器和整流器。