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公开(公告)号：US4522761A
公开(公告)日：1985-06-11
申请号：US474999
申请日：1983-03-14
IPC分类号： C11C1/08
CPC分类号： C11C1/08
摘要： This invention comprises a process for separating a fatty acid from a mixture comprising a fatty acid and a rosin acid, which process comprises contacting the mixture at separation conditions with a molecular sieve comprising silicalite, thereby selectively retaining the fatty acid. The fatty acid is recovered from the molecular sieve by displacement with a displacement fluid comprising an aqueous solution of a ketone from the group comprising acetone, methyl-ethylketone, or di-ethylketone.
摘要翻译： 本发明包括从包含脂肪酸和松香酸的混合物中分离脂肪酸的方法，该方法包括使分离条件下的混合物与包含硅沸石的分子筛接触，从而选择性地保留脂肪酸。 通过用包含丙酮，甲基 - 乙基酮或二 - 乙基酮的酮的水溶液的置换流体置换从分子筛中回收脂肪酸。
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公开(公告)号：US4486548A
公开(公告)日：1984-12-04
申请号：US530337
申请日：1983-09-08
申请人： Santi Kulprathipanja
发明人： Santi Kulprathipanja
CPC分类号： C13B20/148
摘要： An adsorbent suitable for use in separating sucrose from a solution with potassium chloride and betaine. The adsorbent comprises activated carbon bound with a binder material consisting essentially of a water permeable organic polymer from the group cellulose nitrate, a cellulose ester and/or a mixture thereof. Another aspect of the invention is a method of manufacturing the adsorbent comprising (a) mixing together a powder of activated carbon, a powder of binder and a liquid organic solvent to form a malleable mixture; (b) forming the malleable mixture into discrete formations; (c) removing the solvent from the formations to obtain hard dry formations; and (d) breaking the hard dry formations into particles of desired sizes.
摘要翻译： 适用于从氯化钾和甜菜碱溶液中分离蔗糖的吸附剂。 吸附剂包括与基本上由硝酸纤维素组成的水可渗透有机聚合物，纤维素酯和/或其混合物组成的粘合剂材料结合的活性炭。 本发明的另一方面是制备吸附剂的方法，包括（a）将活性炭粉末，粘合剂粉末和液体有机溶剂混合在一起以形成可延展的混合物; （b）将可塑性混合物形成离散地层; （c）从地层中除去溶剂，得到硬干燥地层; 和（d）将硬干燥地层破碎成所需尺寸的颗粒。
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公开(公告)号：US4455445A
公开(公告)日：1984-06-19
申请号：US451525
申请日：1982-12-20
IPC分类号： C07C7/13
CPC分类号： C07C7/13
摘要： A process for the separation of normal C.sub.4 hydrocarbons from isobutylene. A mixture of the normal C.sub.4 hydrocarbons and isobutylene is contacted with a molecular sieve comprising silicalite which is selective for the normal C.sub.4 hydrocarbons. The isobutylene is then recovered in the raffinate stream and the normal C.sub.4 hydrocarbons recovered by displacement with pentene-1.
摘要翻译： 一种从异丁烯中分离出正常C 4烃的方法。 将常规C 4烃和异丁烯的混合物与包含对正常C 4烃选择性的硅沸石的分子筛接触。 然后在萃余液流中回收异丁烯，通过用戊烯-1置换回收正常的C4烃。
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公开(公告)号：US4433195A
公开(公告)日：1984-02-21
申请号：US471397
申请日：1983-03-02
申请人： Santi Kulprathipanja
发明人： Santi Kulprathipanja
IPC分类号： C07C7/12
CPC分类号： C07C7/12
摘要： A process for the separation of a trans-olefin from a cis-olefin. A mixture of the trans- and cis-olefins is contacted with an adsorbent comprising silicalite which is selective for the trans-olefin. The process is particularly suitable for the separation of trans-2-butene from cis-2-butene.
摘要翻译： 一种从顺式烯烃分离反应烯烃的方法。 反式和顺式 - 烯烃的混合物与含有对于反式烯烃有选择性的硅沸石的吸附剂接触。 该方法特别适用于从顺式-2-丁烯中分离反式-2-丁烯。
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125.发明授权Technique to reduce the zeolite molecular sieve solubility in an aqueous system 失效降低沸石分子筛在水性体系中的溶解度的技术
公开(公告)号：US4431456A
公开(公告)日：1984-02-14
申请号：US387381
申请日：1982-06-11
申请人： Santi Kulprathipanja
发明人： Santi Kulprathipanja
CPC分类号： B01J20/183
摘要： An improved process for separating a component from a feed mixture comprising an aqueous solution of a mixture of different components, such as a mixture of saccharides. In the process the mixture is contacted with a zeolite which selectively adsorbs a component from the feed mixture. The adsorbed component is then recovered by contacting the adsorbent with a desorbent material such as water to effect the desorption of the adsorbed component from the adsorbent. There is an undesirable tendency for the silicon constituent of the zeolite to dissolve in the aqueous system. The improvement to the process comprises the impregnation of the zeolite with a binder material comprising a water permeable organic polymer which substantially reduces the undesirable dissolution. The adsorbent is manufactured by mixing together powder of the zeolite, powders of the organic polymer binder, and a liquid organic solvent, extruding the mixture into an extrudate and drying the extrudate.
摘要翻译： 用于从包含不同组分的混合物的水溶液的进料混合物中分离组分的改进方法，例如糖的混合物。 在此过程中，混合物与选择性吸附组分的沸石接触。 然后通过使吸附剂与解吸材料如水接触来回收吸附的组分，以实现吸附组分从吸附剂的解吸附。 沸石的硅组分溶解在水性体系中是不希望的。 该方法的改进包括用包含水可渗透的有机聚合物的粘合剂材料浸渍沸石，其基本上减少了不期望的溶解。 吸附剂通过将沸石的粉末，有机聚合物粘合剂的粉末和液体有机溶剂混合在一起制造，将混合物挤出成挤出物并干燥挤出物。
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公开(公告)号：US4421567A
公开(公告)日：1983-12-20
申请号：US365434
申请日：1982-04-05
CPC分类号： B01J20/2803 , B01J20/28026 , B01J47/007
摘要： A process for separating a component from a feed blend comprising an aqueous solution of a mixture of different components, such as a blend of saccharides. In the process the blend is contacted with an adsorbent comprising a crystalline aluminosilicate and cation exchange resin mixture which selectively adsorbs a component from the feed blend. The adsorbed component is then recovered by contacting the adsorbent with a desorbent material such as water to effect the desorption of the adsorbed component from the adsorbent. There is an undesirable tendency for the silicon constituent of a crystalline aluminosilicate to dissolve in an aqueous system and for the volume of a cationic exchange resin to change with the ionic strength of an aqueous medium. The adsorbent of this invention is dispersed in a binder material comprising a water permeable organic polymer and the effect is a substantial reduction of the undesirable dissolution and volume changes. The adsorbent is manufactured by mixing together powder of the crystalline aluminosilicate, powder of the cationic exchange resin, powder of the organic polymer binder, and a liquid organic solvent, extruding the mixture into an extrudate and drying the extrudate.
摘要翻译： 用于从包含不同组分的混合物的水溶液的进料共混物中分离组分的方法，例如糖的共混物。 在该过程中，共混物与包含结晶硅铝酸盐和阳离子交换树脂混合物的吸附剂接触，其选择性地从进料共混物中吸附组分。 然后通过使吸附剂与解吸材料如水接触来回收吸附的组分，以实现吸附组分从吸附剂的解吸附。 结晶硅铝酸盐的硅组分溶解在水性体系中并且阳离子交换树脂的体积随水性介质的离子强度而变化是不期望的趋势。 本发明的吸附剂分散在包含水可渗透的有机聚合物的粘合剂材料中，其效果是不期望的溶解和体积变化的显着降低。 吸附剂通过将结晶硅铝酸盐的粉末，阳离子交换树脂的粉末，有机聚合物粘合剂的粉末和液体有机溶剂混合在一起来制造，将混合物挤出成挤出物并干燥挤出物。
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公开(公告)号：US4405378A
公开(公告)日：1983-09-20
申请号：US306262
申请日：1981-09-28
申请人： Santi Kulprathipanja
发明人： Santi Kulprathipanja
CPC分类号： C13B20/148
摘要： Sucrose which is found in molasses such as beet molasses or cane molasses may be selectively extracted therefrom by passing an aqueous solution of the molasses over an adsorbent comprising activated carbon powder bound with a binder material comprising a water permeable organic polymer. The sucrose will be selectively adsorbed thereon and separated from the mineral salts and betaine in the molasses. The sucrose is then removed from the adsorbent by treatment with a desorbent material comprising a water and methanol mixture.
摘要翻译： 可以通过使糖蜜的水溶液通过含有活性炭粉末的吸附剂选择性地提取糖蜜如甜菜糖蜜或甘蔗糖蜜中的蔗糖，所述活性炭粉末与包含透水性有机聚合物的粘合剂材料结合。 蔗糖将被选择性地吸附在其上并与糖蜜中的矿物盐和甜菜碱分离。 然后通过用包含水和甲醇混合物的解吸材料处理从吸附剂中除去蔗糖。
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公开(公告)号：US4386012A
公开(公告)日：1983-05-31
申请号：US344707
申请日：1982-02-01
CPC分类号： C13B20/123 , B01D15/206 , B01D15/34 , B01J20/183 , C13K13/007
摘要： An improved adsorbent comprising a crystalline aluminosilicate, method of manufacture of the adsorbent and improved process for separating a component from a feed mixture comprising an aqueous solution of a mixture of different components, such as a mixture of saccharides. In the process the mixture is contacted with the adsorbent, which selectively adsorbs a component from the feed mixture. The adsorbed component is then recovered by contacting the adsorbent with a desorbent material such as water to effect the desorption of the adsorbed component from the adsorbent. There is an undesirable tendency for the silicon constituent of the crystalline aluminosilicate to dissolve in the aqueous system. The improvement to the adsorbent and process comprises the coating of the adsorbent with a water permeable organic polymer which substantially reduces the undesirable dissolution. The adsorbent is manufactured by mixing together the uncoated precursor of the adsorbent with the organic polymer dissolved in a liquid organic solvent, and removing the solvent.
摘要翻译： 一种改进的吸附剂，包括结晶硅铝酸盐，制造吸附剂的方法以及用于从包含不同组分的混合物的水溶液如糖的混合物的进料混合物中分离组分的改进方法。 在该过程中，混合物与吸附剂接触，吸附剂从进料混合物中选择性吸附组分。 然后通过使吸附剂与解吸材料如水接触来回收吸附的组分，以实现吸附组分从吸附剂的解吸附。 结晶硅铝酸盐的硅成分溶解在水性体系中是不希望的。 对吸附剂和方法的改进包括用可渗透水的有机聚合物涂覆吸附剂，其基本上减少了不期望的溶解。 吸附剂通过将未涂覆的吸附剂前体与溶解在液体有机溶剂中的有机聚合物混合在一起并除去溶剂来制造。
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公开(公告)号：US4337171A
公开(公告)日：1982-06-29
申请号：US160521
申请日：1980-06-18
CPC分类号： B01J20/28026 , B01J20/28016 , B01J20/2803 , B01J47/007
摘要： An adsorbent comprising a crystalline aluminosilicate and cation exchange resin mixture, method of manufacture of the adsorbent and process for separating a component from a feed blend comprising an aqueous solution of a mixture of different components, such as a blend of saccharides. In the process the blend is contacted with the adsorbent, which selectively adsorbs a component from the feed blend. The adsorbed component is then recovered by contacting the adsorbent with a desorbent material such as water to effect the desorption of the adsorbed component from the adsorbent. There is an undesirable tendency for the silicon constituent of a crystalline aluminosilicate to dissolve in an aqueous system and for the volume of a cationic exchange resin to change with the ionic strength of an aqueous medium. The adsorbent of this invention is dispersed in a binder material comprising a water permeable organic polymer and the effect is a substantial reduction of the undesirable dissolution and volume changes. The adsorbent is manufactured by mixing together powder of the crystalline aluminosilicate, powder of the cationic exchange resin, powder of the organic polymer binder, and a liquid solvent, extruding the mixture into an extrudate and drying the extrudate.
摘要翻译： 一种包含结晶硅铝酸盐和阳离子交换树脂混合物的吸附剂，所述吸附剂的制备方法和用于从包含不同组分的混合物的水溶液如糖的混合物的进料共混物中分离组分的方法。 在该过程中，共混物与吸附剂接触，吸附剂选择性地从进料共混物中吸附组分。 然后通过使吸附剂与解吸材料如水接触来回收吸附的组分，以实现吸附组分从吸附剂的解吸附。 结晶硅铝酸盐的硅组分溶解在水性体系中并且阳离子交换树脂的体积随水性介质的离子强度而变化是不期望的趋势。 本发明的吸附剂分散在包含水可渗透的有机聚合物的粘合剂材料中，其效果是不期望的溶解和体积变化的显着降低。 吸附剂通过将结晶硅铝酸盐的粉末，阳离子交换树脂的粉末，有机聚合物粘合剂的粉末和液体溶剂混合在一起来制造，将混合物挤出成挤出物并干燥挤出物。
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130.发明授权Technique to reduce the zeolite molecular sieve solubility in an aqueous system 失效降低沸石分子筛在水性体系中的溶解度的技术
公开(公告)号：US4333768A
公开(公告)日：1982-06-08
申请号：US217945
申请日：1980-12-18
CPC分类号： C13B20/148 , B01D15/20 , B01D15/34 , B01J20/183 , C13K13/007 , B01D15/361
摘要： This invention relates to an improved adsorbent comprising a crystalline aluminosilicate, method of manufacture of the adsorbent and improved process for separating a component from a feed mixture comprising an aqueous solution of a mixture of different components, such as a mixture of saccharides. In the process the mixture is contacted with the adsorbent, which selectively adsorbs a component from the feed mixture. The adsorbed component is then recovered by contacting the adsorbent with a desorbent material such as water to effect the desorption of the adsorbed component from the adsorbent. There is an undesirable tendency for the silicon constituent of the crystalline aluminosilicate to dissolve in the aqueous system. The improvement to the adsorbent and process comprises the incorporation of a binder material in the adsorbent comprising a cellulose ether which substantially reduces the undesirable dissolution. The adsorbent is manufactured by mixing together powder of the crystalline aluminosilicate, powders of the binder, and a liquid organic solvent, extruding the mixture into an extrudate and drying the extrudate.
摘要翻译： 本发明涉及包含结晶硅铝酸盐的改进的吸附剂，制备吸附剂的方法和用于从包含不同组分的混合物的水溶液如糖的混合物的进料混合物中分离组分的改进方法。 在该过程中，混合物与吸附剂接触，吸附剂从进料混合物中选择性吸附组分。 然后通过使吸附剂与解吸材料如水接触来回收吸附的组分，以实现吸附组分从吸附剂的解吸附。 结晶硅铝酸盐的硅成分溶解在水性体系中是不希望的。 对吸附剂和方法的改进包括在包含纤维素醚的吸附剂中引入粘合剂材料，其基本上减少不期望的溶解。 吸附剂通过将结晶硅铝酸盐的粉末，粘合剂的粉末和液体有机溶剂混合在一起来制造，将混合物挤出成挤出物并干燥挤出物。
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