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    Azaaromatic compounds having azafluoranthene skeletons and organic electroluminescent devices made by using the same
    162.
    发明授权
    Azaaromatic compounds having azafluoranthene skeletons and organic electroluminescent devices made by using the same 有权
    具有氮杂芳烃骨架的氮杂芳族化合物和使用它们的有机电致发光器件

    公开(公告)号：US07662487B2

    公开(公告)日：2010-02-16

    申请号：US11931374

    申请日：2007-10-31

    申请人： Toshihiro Iwakuma

    发明人： Toshihiro Iwakuma

    IPC分类号： H01L51/54 ,  C07D241/36 ,  C07D495/00 ,  C09K11/00

    CPC分类号： H01L51/5012 ,  C07D241/38 ,  C07D487/06 ,  C09K11/06 ,  C09K2211/1011 ,  C09K2211/1029 ,  C09K2211/1044 ,  H01L51/007 ,  H01L51/0072 ,  H01L51/008 ,  H01L51/0085 ,  H01L51/0087 ,  H01L51/009 ,  H05B33/14 ,  Y10S428/917

    摘要： The invention aims at providing a novel azaaromatic compound having an azafluoranthene skeleton which is useful as the constituent of organic EL devices and at realizing a long lifetime, high-efficiency and practical organic EL device by using the compound in at least one of the organic compound layers. The invention provides azaaromatic compounds having azafluoranthene skeletons as represented by the general formula (1): wherein R1 to R12 are each independently hydrogen, substituted or unsubstituted alkyl having 1 to 30 carbon atoms, substituted or unsubstituted alkoxy having 1 to 30 carbon atoms, substituted or unsubstituted aryl having 6 to 40 carbon atoms, trialkylsilyl (wherein each alkyl has 1 to 20 carbon atoms and may be substituted), aryloxy (wherein the aryl has 6 to 40 carbon atoms and may be substituted), halogen atom, or cyano group, with the proviso that at least two of R1 to R12 are each cyano group, trifluoromethyl group, or fluorine atom and adjacent two of R1 to R12 may be linked together to form a ring structure.

    摘要翻译： 本发明旨在提供一种具有氮杂芳族化合物，其具有可用作有机EL器件的组成部分的氮氧杂骨架，并且通过在至少一种有机化合物中使用化合物实现长寿命，高效率和实用的有机EL器件 层。 本发明提供具有由通式（1）表示的氮杂芳烃骨架的氮杂芳族化合物：其中R 1至R 12各自独立地为氢，取代或未取代的具有1至30个碳原子的烷基，取代或未取代的具有1至30个碳原子的烷氧基，取代的 或未取代的碳原子数为6〜40的芳基，三烷基甲硅烷基（其中，各烷基具有1〜20个碳原子，可以被取代），芳氧基（其中芳基具有6〜40个碳原子并可被取代），卤素原子或氰基 条件是R 1至R 12中的至少两个各自为氰基，三氟甲基或氟原子，并且R 1至R 12中相邻的两个可以连接在一起形成环结构。

    METHOD FOR PRODUCING AROMATIC AMINO COMPOUND
    165.
    发明申请
    METHOD FOR PRODUCING AROMATIC AMINO COMPOUND 审中-公开

    公开(公告)号：US20070249861A1

    公开(公告)日：2007-10-25

    申请号：US11764896

    申请日：2007-06-19

    申请人： Toshihiro Iwakuma ,  Fumio Moriwaki

    发明人： Toshihiro Iwakuma ,  Fumio Moriwaki

    IPC分类号： C07C229/52

    CPC分类号： C07C211/54 ,  C07C209/10 ,  C07C209/62 ,  C07C211/55

    摘要： A method for producing aromatic amino compound (V): by synthesizing intermediate compound (IV): by the reaction of compound (I): H2N—R1 with a mixture of halogenated aryl compounds (II): Ar1-X and (III): Ar2-X in the presence of a noble metal catalyst, followed by eliminating the substituent R1 from the nitrogen atom in compound (IV) under an acidic condition or an alkaline condition or by addition of a reducing agent or an oxidizing agent. (R1: a substituent having 2 to 50 carbon atoms; Ar1 and Ar2: a substituted or unsubstituted hydrocarbon group or heterocyclic group having 6 to 50 carbon atoms and the same with or different from each other; and X: a halogen group). The aromatic amino compound useful as the charge transporting material can be produced efficiently at a great yield without using highly toxic raw materials.

    Aromatic compounds and organic electroluminescent devices made by using the same
    167.
    发明授权
    Aromatic compounds and organic electroluminescent devices made by using the same 有权
    芳香族化合物和使用它们的有机电致发光器件

    公开(公告)号：US07235312B2

    公开(公告)日：2007-06-26

    申请号：US10483990

    申请日：2002-07-12

    申请人： Toshihiro Iwakuma ,  Takashi Arakane ,  Tadashi Kusumoto

    发明人： Toshihiro Iwakuma ,  Takashi Arakane ,  Tadashi Kusumoto

    IPC分类号： H01J1/62 ,  C07C211/00

    CPC分类号： H05B33/14 ,  C07C211/61 ,  C07C217/94 ,  C07C2603/54 ,  C09K11/06 ,  C09K2211/1007 ,  C09K2211/1011 ,  C09K2211/1014 ,  H01L51/0055 ,  H01L51/0056 ,  H01L51/006 ,  H01L51/5012 ,  H01L51/5048 ,  Y10S428/917

    摘要： A novel aromatic compound represented by following general formula (I): among X1 to X20 in general formula (I), (1) at least four each independently represent a linear or branched alkoxyl group having 1 to 6 carbon atoms, and others each represent hydrogen atom; (2) at least one represents a linear or branched alkyl group having 1 to 6 carbon atoms, at least one represents a linear or branched alkoxyl group having 1 to 6 carbon atoms, a total of a number of the alkyl group and a number of the alkoxyl group being 4 or greater, and others each represent hydrogen atom; (3) at least six each independently represent a linear or branched alkyl group having 1 to 6 carbon atoms, and others each represent hydrogen atom; or (4) at least four each independently represent a linear or branched alkyl group having 1 to 6 carbon atoms, two among said alkyl groups having 3 to 6 carbon atoms, and others each represent hydrogen atom; and an organic electroluminescence device using the aromatic compound, are provided. The device exhibits excellent purity of color, provides great luminance of emitted light and efficiency of light emission even at a small driving voltage, has a long lifetime and emits reddish light.

    摘要翻译： 由通式（I）表示的新型芳族化合物：通式（I）中的X 1〜X 20中，（1）中，至少4个各自独立地表示 具有1〜6个碳原子的直链或支链烷氧基，各自表示氢原子; （2）至少一个表示具有1至6个碳原子的直链或支链烷基，至少一个表示具有1至6个碳原子的直链或支链烷氧基，总数为烷基数 烷氧基为4以上，各自表示氢原子; （3）至少6个各自独立地表示具有1至6个碳原子的直链或支链烷基，其它各自表示氢原子; 或（4）至少4个各自独立地表示碳原子数1〜6的直链或支链烷基，所述碳原子数3〜6的烷基中的2个，各自表示氢原子。 和使用该芳香族化合物的有机电致发光元件。 该装置表现出优异的颜色纯度，即使在小的驱动电压下也能提供发光的高亮度和发光效率，寿命长并且发出微红光。