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公开(公告)号：US07790914B2
公开(公告)日：2010-09-07
申请号：US12656179
申请日：2010-01-20
申请人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
发明人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
IPC分类号： C07C69/96
CPC分类号： B01J27/053 , B01J27/16 , C07C68/04 , Y02P20/544 , C07C69/96
摘要： There is provided a catalyst for dimethyl carbonate synthesis which has a high conversion rate under the supercritical condition of CO2 and can be handled easily. The catalyst for dimethyl carbonate is obtained by loading SO42− or PO43− on a carrier composed of a compound having a solid acid site, and is used to produce dimethyl carbonate from acetone dimethyl carbonate and CO2 in a supercritical state. The component having a solid acid site is preferably one or more of ZrO2, Al2O3, and TiO2.
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公开(公告)号：US20100121093A1
公开(公告)日：2010-05-13
申请号：US12656179
申请日：2010-01-20
申请人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
发明人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
IPC分类号： C07C69/96
CPC分类号： B01J27/053 , B01J27/16 , C07C68/04 , Y02P20/544 , C07C69/96
摘要： There is provided a catalyst for dimethyl carbonate synthesis which has a high conversion rate under the supercritical condition of CO2 and can be handled easily. The catalyst for dimethyl carbonate is obtained by loading SO42− or PO43− on a carrier composed of a compound having a solid acid site, and is used to produce dimethyl carbonate from acetone dimethyl carbonate and CO2 in a supercritical state. The component having a solid acid site is preferably one or more of ZrO2, Al2O3, and TiO2.
摘要翻译： 提供了一种二甲基碳酸酯合成催化剂，其在二氧化碳的超临界条件下具有高转化率并且可以容易地处理。 碳酸二甲酯的催化剂是通过在由具有固体酸性部位的化合物构成的载体上加载SO42-或PO43-而获得的，并且用于从超临界状态的丙酮二甲基碳酸酯和CO 2生产碳酸二甲酯。 具有固体酸性部位的成分优选为ZrO 2，Al 2 O 3和TiO 2中的一种以上。
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公开(公告)号：US07674742B2
公开(公告)日：2010-03-09
申请号：US10553267
申请日：2004-04-16
申请人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
发明人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
IPC分类号： B01J21/00
CPC分类号： B01J27/053 , B01J27/16 , C07C68/04 , Y02P20/544 , C07C69/96
摘要： There is provided a catalyst for dimethyl carbonate synthesis which has a high conversion rate under the supercritical condition of CO2 and can be handled easily. The catalyst for dimethyl carbonate is obtained by loading SO42− or PO43− on a carrier composed of a compound having a solid acid site, and is used to produce dimethyl carbonate from acetone dimethyl carbonate and CO2 in a supercritical state. The component having a solid acid site is preferably one or more of ZrO2, Al2O3, and TiO2.
摘要翻译： 提供了一种二甲基碳酸酯合成催化剂，其在二氧化碳的超临界条件下具有高转化率并且可以容易地处理。 碳酸二甲酯的催化剂是通过在由具有固体酸性部位的化合物构成的载体上加载SO42-或PO43-而获得的，并且用于从超临界状态的丙酮二甲基碳酸酯和CO 2生产碳酸二甲酯。 具有固体酸性部位的成分优选为ZrO 2，Al 2 O 3和TiO 2中的一种以上。
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公开(公告)号：US07605285B2
公开(公告)日：2009-10-20
申请号：US10553009
申请日：2004-04-16
申请人： Kazuto Kobayashi , Hiroyuki Osora , Yoshio Seiki , Masaki Iijima
发明人： Kazuto Kobayashi , Hiroyuki Osora , Yoshio Seiki , Masaki Iijima
IPC分类号： C07C69/96
CPC分类号： C07C29/1518 , C07C29/152 , C07C68/04 , Y02P20/142 , C07C31/04 , C07C69/96
摘要： The present invention provides a method and apparatus for producing dimethyl carbonate, wherein carbon dioxide is recovered from combustion exhaust gas of a steam reformer 10 and a boiler; and some of the recovered carbon dioxide is used for methanol synthesis as a raw material for the steam reformer 10, and the remaining carbon dioxide is allowed to react with some of the yielded methanol to synthesize dimethyl carbonate. According to the present invention, CO2, which has conventionally been discharged, is returned to the steam reformer and is used effectively to produce DMC, and also devices for producing methanol and DMC can be simplified.
摘要翻译： 本发明提供一种生产二甲基碳酸酯的方法和装置，其中从蒸汽重整器10和锅炉的燃烧废气中回收二氧化碳; 一部分回收的二氧化碳用作甲醇合成用作蒸汽重整器10的原料，剩余的二氧化碳与一些生成的甲醇反应合成碳酸二甲酯。 根据本发明，通常排出的CO 2返回到蒸汽重整器中，并且有效地用于生产DMC，并且还可以简化用于生产甲醇和DMC的装置。
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15.发明申请公开(公告)号：US20070213557A1
公开(公告)日：2007-09-13
申请号：US11797983
申请日：2007-05-09
申请人： Yoshio Seiki , Kazuto Kobayashi , Yoshiyuki Takeuchi , Hiroyuki Osora , Keiichi Akimoto , Noritaka Matsumoto , Motoki Numata , Hiroaki Shimazu
发明人： Yoshio Seiki , Kazuto Kobayashi , Yoshiyuki Takeuchi , Hiroyuki Osora , Keiichi Akimoto , Noritaka Matsumoto , Motoki Numata , Hiroaki Shimazu
CPC分类号： B01J8/009 , B01D3/14 , B01D3/143 , B01D3/4205 , B01D53/268 , B01J2219/00006 , C07C51/265 , C07C51/44 , C07C51/47 , Y10S159/03 , Y10S159/27 , Y10S159/28 , C07C63/26
摘要： In a process for producing an aromatic carboxylic acid, it is a dehydrating process which can achieve compactification of a step for removing water from a mixture of acetic acid and water produced in the production process, and which can reduce the consumed energy. In a production process of an aromatic carboxylic acid having an oxidation reaction step for producing a slurry of an aromatic carboxylic acid by carrying out liquid-phase oxidation reaction of an alkyl aromatic compound with an oxygen-containing gas in a solvent containing acetic acid in the presence of an oxidation catalyst, at least a portion of a mixture containing acetic acid and water produced in the production steps is separated into a permeable gas mainly comprising water and nonpermeable substances mainly comprising acetic acid, using a separation membrane having water selectivity.
摘要翻译： 在芳香族羧酸的制造方法中，能够实现从生产过程中生成的乙酸和水的混合物中除去水分的步骤的压实，从而可以降低消耗能量的脱水方法。 在具有氧化反应步骤的芳族羧酸的制造方法中，通过在含有乙酸的溶剂中进行烷基芳族化合物与含氧气体的液相氧化反应，生成芳香族羧酸的浆料 存在氧化催化剂，使用具有水选择性的分离膜将至少一部分在制备步骤中生产的含有乙酸和水的混合物分离成主要包含水和主要包含乙酸的不渗透物质的渗透气体。
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公开(公告)号：US20070021297A1
公开(公告)日：2007-01-25
申请号：US10553267
申请日：2004-04-16
申请人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
发明人： Hiroyuki Osora , Kazuto Kobayashi , Yoshio Seiki , Toshinobu Yasutake , Masaki Iijima , Akira Oguchi
IPC分类号： B01J21/00
CPC分类号： B01J27/053 , B01J27/16 , C07C68/04 , Y02P20/544 , C07C69/96
摘要： There is provided a catalyst for dimethyl carbonate synthesis which has a high conversion rate under the supercritical condition of CO2 and can be handled easily. The catalyst for dimethyl carbonate is obtained by loading SO42− or PO43− on a carrier composed of a compound having a solid acid site, and is used to produce dimethyl carbonate from acetone dimethyl carbonate and CO2 in a supercritical state. The component having a solid acid site is preferably one or more of ZrO2, Al2O3, and TiO2.
摘要翻译： 提供了一种二甲基碳酸酯合成催化剂，其在CO 2的超临界条件下具有高的转化率，并且可以容易地处理。 碳酸二甲酯的催化剂是通过将载体组合的载体SO 2 - 2 - /或PO 4 - 3 - 3 - 的具有固体酸性位点的化合物，并且用于从超临界状态的丙酮二甲基碳酸酯和CO 2 H 2生产碳酸二甲酯。 具有固体酸性部位的组分优选为ZrO 2 2，Al 2 O 3 3和TiO 2， SUB>。
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公开(公告)号：US20100206789A1
公开(公告)日：2010-08-19
申请号：US12678673
申请日：2009-01-13
申请人： Atsuhiro Yukumoto , Hiroyuki Osora , Yoshio Seiki , Haruaki Hirayama , Yukio Tanaka , Hideo Kashiwagi , Katsufumi Inoue
发明人： Atsuhiro Yukumoto , Hiroyuki Osora , Yoshio Seiki , Haruaki Hirayama , Yukio Tanaka , Hideo Kashiwagi , Katsufumi Inoue
IPC分类号： B01D61/36
CPC分类号： B01D61/362 , B01D61/58 , B01D2313/24 , B01D2317/022 , C07C29/76 , C07C31/08
摘要： Provided is a dehydrator that requires no excessively large apparatus structure and achieves cost-saving while maintaining suction efficiency at a desired level by use of suction means. A dehydrator 100 for separating water from a target liquid 13 includes at least two water separation membrane units 1a and 1b which are provided in series in a flow direction of the target liquid 13. The water separation membrane unit 1a on an upstream side out of the water separation membrane units 1a and 1b is connected to suction means 7 for sucking a gas phase containing water through one condenser 4, and the one condenser 4 condenses water in the gas phase and thereby separates the water. The gas phase sucked by the suction means 7 from the one condenser 4 is transferred to at least one downstream condenser 8 provided downstream of the one condenser 4, and the downstream condenser 8 condenses water in the gas phase and thereby separates the water. The water separation membrane unit 1b on a downstream side of the water separation membrane unit 1a is connected to a steam ejector 3, and the condenser 4 for condensing water in a gas phase passed through the steam ejector 3 condenses water and thereby separates the water.
摘要翻译： 提供一种脱水机，其不需要过大的装置结构，并且通过使用抽吸装置将抽吸效率保持在期望的水平，从而节省成本。 用于从目标液体13分离水的脱水器100包括沿目标液体13的流动方向串联设置的至少两个水分离膜单元1a和1b。在上游侧的水分离膜单元1a 水分离膜单元1a和1b连接到抽吸装置7，用于通过一个冷凝器4吸入含有水的气相，并且一个冷凝器4冷凝气相中的水，从而分离水。 由抽吸装置7从一个冷凝器4吸入的气相被转移到设置在一个冷凝器4下游的至少一个下游冷凝器8，下游冷凝器8冷凝气体中的水分，从而分离出水分。 水分离膜单元1a的下游侧的水分离膜单元1b与蒸汽喷射器3连接，用于冷凝通过蒸汽喷射器3的气相中的水的冷凝器4冷凝水分，从而分离水。
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公开(公告)号：US20100314320A1
公开(公告)日：2010-12-16
申请号：US12743997
申请日：2008-03-14
申请人： Hiroyuki Osora , Yoshio Seiki , Atsuhiro Yukumoto
发明人： Hiroyuki Osora , Yoshio Seiki , Atsuhiro Yukumoto
CPC分类号： C07C29/82 , B01D3/004 , B01D3/36 , B01D53/268 , B01D61/36 , B01D67/0048 , B01D67/0083 , B01D71/027 , B01D2311/04 , B01D2311/10 , B01D2311/2669 , B01D2323/08 , B01D2323/12 , B01D2325/30
摘要： The present invention includes: a water separation membrane device 2 that separates a process-target fluid into a dehydrated product and water; and a temperature monitoring device 3 for the water separation membrane device 2. The temperature monitoring device 3 detects a temperature. Further, a temperature adjustment device 4 is provided in a previous stage of the water separation membrane device 2. The temperature adjustment device 4 controls a temperature of the process-target fluid on the basis of the temperature detected by the temperature adjustment device 3 to thereby optimize an amount of water permeation in a separation process in the water separation membrane device 2.
摘要翻译： 本发明包括：将过程目标流体分离成脱水产物和水分的水分离膜装置2; 和水分离膜装置2的温度监视装置3.温度监视装置3检测温度。 此外，在水分离膜装置2的前一级设置有温度调节装置4.温度调节装置4基于由温度调节装置3检测的温度来控制处理对象流体的温度，从而 在水分离膜装置2中在分离过程中优化水的渗透量。
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公开(公告)号：US20100288682A1
公开(公告)日：2010-11-18
申请号：US12465079
申请日：2009-05-13
申请人： Hiroyuki Osora , Yoshio Seiki , Atsuhiro Yukumoto , Yukio Tanaka , Shinji Ogino , Haruaki Hirayama
发明人： Hiroyuki Osora , Yoshio Seiki , Atsuhiro Yukumoto , Yukio Tanaka , Shinji Ogino , Haruaki Hirayama
CPC分类号： B01D61/362 , B01D65/08 , B01D2317/04 , B01D2321/20
摘要： A dehydrating system is designed to maintain the availability of a plant having the dehydrating system using a water separation membrane by allowing a water separation membrane unit to be replaced while the plant is in operation. The dehydrating system comprises at least two water separation membrane units in use arranged parallel to the direction of flow of a fluid to be processed, is configured so that at least one spare water separation membrane unit can be installed parallel to the direction of flow of the fluid to be processed with respect to the at least two water separation membrane units, having monitoring devices for the product fluid to be taken out, and maintains the properties of the product fluid by operating the spare water separation membrane unit depending on the properties of the product fluid monitored by the monitoring devices.
摘要翻译： 脱水系统被设计成通过在工厂运行时允许更换水分离膜单元来保持具有使用水分离膜的脱水系统的设备的可用性。 脱水系统包括至少两个平行于待处理流体的流动方向布置的水分离膜单元，其被配置成使得至少一个备用水分离膜单元可平行于流动方向 相对于至少两个水分离膜单元进行处理的流体，具有用于待取出的产品流体的监测装置，并且通过根据其特性来操作备用水分离膜单元来维持产品流体的性质 产品流体由监控设备监控。
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公开(公告)号：US09149769B2
公开(公告)日：2015-10-06
申请号：US12522831
申请日：2008-03-14
CPC分类号： B01D61/362 , B01D63/06 , B01D2311/04 , B01D2311/08 , B01D2313/08 , B01D2313/38 , B01D2317/04 , B01D2319/04 , C07C29/76 , C07C31/08 , B01D2311/103 , B01D2311/14 , B01D2311/16 , B01D2311/246
摘要： A dehydration system has improved membrane performance. The dehydration system includes a dehydrating apparatus 1 comprising, in a dehydrating apparatus body, a water separation membrane module in which a water separation membrane having at least one flow path extending in the up and down direction to cause a liquid 50 to pass through is provided with a liquid inlet at the bottom thereof and a liquid outlet at the top thereof; and a shell 11 defined by the outer surface of the water separation membrane module and the inner wall of the dehydrating apparatus body, wherein water in the liquid permeates the water separation membrane while the liquid rises in the water separation membrane, and moves in the shell, whereby the liquid is dehydrated; a pressure reducing device 13 for reducing the pressure of the shell 11; a pressure device for pressurizing the liquid before the liquid is fed to the water separation membrane module; and a heating device for heating the pressurized liquid.
摘要翻译： 脱水系统具有改进的膜性能。 脱水系统包括脱水装置1，该脱水装置1包括在脱水装置主体中的水分离膜组件，其中具有沿上下方向延伸以使液体50通过的至少一个流路的水分离膜 在其底部具有液体入口，在其顶部具有液体出口; 以及由水分离膜组件的外表面和脱水装置主体的内壁限定的壳体11，其中液体中的水在水分离膜中升高时渗透水分离膜，并在壳体内移动 从而使液体脱水; 用于降低壳体11的压力的减压装置13; 用于在将液体供给到水分离膜组件之前对液体加压的压力装置; 以及用于加热加压液体的加热装置。
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