Combustion synthesis continuous flow reactor
    12.
    发明授权
    Combustion synthesis continuous flow reactor 失效
    燃烧合成连续流动反应器

    公开(公告)号:US5705132A

    公开(公告)日:1998-01-06

    申请号:US366941

    申请日:1994-12-30

    摘要: The present invention is a reactor for combustion synthesis of inorganic powders. The reactor includes a reaction vessel having a length and a first end and a second end. The reaction vessel further has a solution inlet and a carrier gas inlet. The reactor further has a heater for heating both the solution and the carrier gas. In a preferred embodiment, the reaction vessel is heated and the solution is in contact with the heated reaction vessel. It is further preferred that the reaction vessel be cylindrical and that the carrier gas is introduced tangentially into the reaction vessel so that the solution flows helically along the interior wall of the reaction vessel. As the solution evaporates and combustion produces inorganic material powder, the carrier gas entrains the powder and carries it out of the reactor.

    摘要翻译: 本发明是用于燃烧合成无机粉末的反应器。 反应器包括具有长度和第一端和第二端的反应容器。 反应容器还具有溶液入口和载气入口。 反应器还具有用于加热溶液和载气两者的加热器。 在优选的实施方案中,加热反应容器并使溶液与加热的反应容器接触。 进一步优选地,反应容器是圆柱形的,并且载气被切向地引入反应容器中,使得溶液沿着反应容器的内壁螺旋地流动。 当溶液蒸发并且燃烧产生无机材料粉末时,载气夹带粉末并将其送出反应器。

    Method of making metal oxide ceramic powders by using a combustible
amino acid compound
    13.
    发明授权
    Method of making metal oxide ceramic powders by using a combustible amino acid compound 失效
    通过使用可燃性氨基酸化合物制备金属氧化物陶瓷粉末的方法

    公开(公告)号:US5114702A

    公开(公告)日:1992-05-19

    申请号:US599273

    申请日:1990-10-16

    IPC分类号: C01B13/18 C01B13/32

    摘要: This invention is directed to the formation of homogeneous, aqueous precursor mixtures of at least one substantially soluble metal salt and a substantially soluble, combustible co-reactant compound, typically an amino acid. This produces, upon evaporation, a substantially homogeneous intermediate material having a total solids level which would support combustion. The homogeneous intermediate material essentially comprises highly dispersed or solvated metal constituents and the co-reactant compound. The intermediate material is quite flammable. A metal oxide powder results on ignition of the intermediate product which combusts same to produce the product powder.

    摘要翻译: 本发明涉及形成至少一种基本上可溶的金属盐和基本上可溶的可燃共助反应物化合物(通常为氨基酸)的均匀的水性前体混合物。 这在蒸发时产生具有将支持燃烧的总固体含量的基本均匀的中间体材料。 均匀的中间体材料主要包含高度分散或溶剂化的金属组分和共反应物。 中间材料是非常易燃的。 金属氧化物粉末导致燃烧相同的中间产物的点燃以产生产品粉末。

    Preparation of thin ceramic films via an aqueous solution route
    14.
    发明授权
    Preparation of thin ceramic films via an aqueous solution route 失效
    通过水溶液路线制备薄陶瓷膜

    公开(公告)号:US4880772A

    公开(公告)日:1989-11-14

    申请号:US204643

    申请日:1988-06-09

    IPC分类号: C01B13/18 C01B13/32

    摘要: A new chemical method of forming thin ceramic films has been developed. An aqueous solution of metal nitrates or other soluble metal salts and a low molecular weight amino acid is coated onto a substrate and pyrolyzed. The amino acid serves to prevent precipitation of individual solution components, forming a very viscous, glass-like material as excess water is evaporated. Using metal nitrates and glycine, the method has been demonstrated for zirconia with various levels of yttria stabilization, for lanthanum-strontium chromites, and for yttrium-barium-copper oxide superconductors on various substrates.

    摘要翻译: 已经开发了形成薄陶瓷膜的新的化学方法。 将金属硝酸盐或其它可溶性金属盐和低分子量氨基酸的水溶液涂覆在基材上并热解。 氨基酸用于防止各种溶液成分的沉淀,形成非常粘稠的玻璃状材料,因为过量的水被蒸发。 使用金属硝酸盐和甘氨酸,已经证明了用于各种氧化钇稳定化的氧化锆,铬酸镧 - 锶钡和用于各种衬底上的钇钡钡氧化物超导体的方法。