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    O-(oximino)ethylcyclohexenone oxime ethers and their use as herbicides
    23.
    发明授权
    O-(oximino)ethylcyclohexenone oxime ethers and their use as herbicides 失效
    O-（肟基）乙基环己烯酮肟醚及其作为除草剂的用途

    公开(公告)号：US5739085A

    公开(公告)日：1998-04-14

    申请号：US435450

    申请日：1995-05-05

    Applicant: Ulf Misslitz ,  Albrecht Harreus ,  Hartmann Konig ,  Helmut Walter ,  Karl-Otto Westphalen ,  Matthias Gerber

    Inventor： Ulf Misslitz ,  Albrecht Harreus ,  Hartmann Konig ,  Helmut Walter ,  Karl-Otto Westphalen ,  Matthias Gerber

    IPC: A01N35/10 ,  A01N41/06 ,  A01N43/16 ,  A01N43/18 ,  A01N43/56 ,  A01N43/80 ,  C07C251/38 ,  C07C251/52 ,  C07C251/54 ,  C07C251/58 ,  C07C311/05 ,  C07C323/19 ,  C07C323/47 ,  C07D231/12 ,  C07D261/08 ,  C07D309/06 ,  C07D335/02 ,  A01N33/24

    CPC classification number: A01N35/10 ,  A01N43/16 ,  A01N43/18 ,  C07C251/38 ,  C07C251/52 ,  C07C251/58 ,  C07C323/19 ,  C07C323/47 ,  C07D309/06 ,  C07D335/02 ,  C07C2101/02 ,  C07C2101/16

    Abstract: O-(Oximino)ethylcyclohexenone oxime ethers I ##STR1## (R.sup.1 and R.sup.2 =C.sub.1 -C.sub.6 -alkyl; R.sup.3 =unsubstituted or substituted phenyl, C.sub.1 -C.sub.4 -alkyl, C.sub.3 -C.sub.4 -alkenyl or C.sub.3 -C.sub.4 -alkynyl, which in each case can be substituted by halogen, C.sub.1 -C.sub.3 -alkyl, unsubstituted or substituted phenyl or unsubstituted or substituted phenoxy; R.sup.4 =C.sub.1 -C.sub.4 -alkoxy-C.sub.1 -C.sub.6 -alkyl or C.sub.1 -C.sub.4 -alkylthio-C.sub.1 -C.sub.6 -alkyl, unsubstituted or substituted phenylthio-C.sub.1 -C.sub.6 -alkyl, N-(C.sub.1 -C.sub.4 -alkylsulfonyl)-N-(C.sub.1 -C.sub.4 -alkyl)aminomethyl, unsubstituted or substituted C.sub.3 -C.sub.7 -cycloalkyl or C.sub.5 -C.sub.7 -cycloalkenyl, 5-membered saturated heterocyclyl having one or two oxygen and/or sulfur atoms, which can carry one to three substituents, saturated or unsaturated 6-/7-membered heterocyclyl having 1 or 2 non-adjacent oxygen and/or sulfur atoms, which can carry 1 to 3 substituents, 5-membered heteroaryl, containing 1 to 2 nitrogen atoms and an oxygen or sulfur atom, where the heteroaromatic can carry 1 to 3 substituents, phenyl or pyridyl, which can carry 1 to 3 of the following substituents: halogen, nitro, cyano, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -alkylthio, C.sub.1 -C.sub.4 -haloalkyl, C.sub.3 -C.sub.6 -alkenyloxy, C.sub.3 -C.sub.6 -alkynyloxy and --NR.sup.a R.sup.b ; R.sup.a =H, C.sub.1 -C.sub.4 -alkyl, C.sub.3 -C.sub.6 -alkenyl or C.sub.3 -C.sub.6 -alkynyl; R.sup.b =H, C.sub.1 -C.sub.4 -alkyl, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.6 -alkynyl, C.sub.1 -C.sub.6 -acyl or unsubstituted or substituted benzoyl) and their agriculturally utilizable salts and esters are described.

    Abstract translation: O-（肟基）乙基环己烯酮肟醚I（R1和R2 = C1-C6-烷基; R3 =未取代或取代的苯基，C1-C4-烷基，C3-C4-烯基或C3-C4-炔基，其中 在每种情况下可以被卤素，C 1 -C 3 - 烷基，未取代或取代的苯基或未取代或取代的苯氧基取代; R 4 = C 1 -C 4 - 烷氧基-C 1 -C 6烷基或C 1 -C 4 - 烷硫基-C 1 -C 6烷基 ，未取代或取代的苯硫基-C 1 -C 6烷基，N-（C 1 -C 4 - 烷基磺酰基）-N-（C 1 -C 4 - 烷基）氨基甲基，未取代或取代的C 3 -C 7 - 环烷基或C 5 -C 7 - 环烯基， 具有一个或两个氧和/或硫原子的五元饱和杂环基，其可以携带一至三个取代基，具有1或2个不相邻的氧和/或硫原子的饱和或不饱和的6-元/ 7元杂环基，其可携带1 包含1至2个氮原子和氧或硫原子的3个取代基，5元杂芳基，其中杂芳族可以带有1-3个取代基，苯基或吡啶基，其可以携带1至3个 C 1 -C 4烷氧基，C 1 -C 4 - 烷硫基，C 1 -C 4卤代烷基，C 3 -C 6 - 烯氧基，C 3 -C 6 - 炔氧基和-NR a R b;取代基：卤素，硝基，氰基， R a = H，C 1 -C 4 - 烷基，C 3 -C 6 - 烯基或C 3 -C 6炔基; 描述了Rb = H，C 1 -C 4 - 烷基，C 3 -C 6 - 烯基，C 3 -C 6炔基，C 1 -C 6酰基或未取代或取代的苯甲酰基）和它们的农业可利用的盐和酯。

    5-hydroxypyrazol-4-ylcarbonyl-substituted saccharin derivatives
    24.
    发明授权
    5-hydroxypyrazol-4-ylcarbonyl-substituted saccharin derivatives 失效
    5-羟基吡唑-4-基羰基取代的糖精衍生物

    公开(公告)号：US5723415A

    公开(公告)日：1998-03-03

    申请号：US776576

    申请日：1997-02-03

    Applicant: Peter Plath ,  Wolfgang von Deyn ,  Stefan Engel ,  Uwe Kardorff ,  Hartmann Konig ,  Harald Rang ,  Matthias Gerber ,  Helmut Walter ,  Karl-Otto Westphalen

    Inventor： Peter Plath ,  Wolfgang von Deyn ,  Stefan Engel ,  Uwe Kardorff ,  Hartmann Konig ,  Harald Rang ,  Matthias Gerber ,  Helmut Walter ,  Karl-Otto Westphalen

    IPC: A01N43/80 ,  A01P13/00 ,  C07D417/06

    CPC classification number: C07D417/06 ,  A01N43/80

    Abstract: 5-Hydroxypyrazol-4-ylcarbonyl-substituted saccharin derivatives of the formula I ##STR1## where the substituents have the following meanings: L and M are hydrogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -alkylthio, chlorine, cyano, methylsulfonyl, nitro or trifluoromethyl; Z is hydrogen, C.sub.1 -C.sub.4 -alkyl, C.sub.3 -C.sub.8 -cycloalkyl, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.5 -alkynyl, C.sub.1 -C.sub.4 -acyl, benzyl or phenyl, the phenyl rings in each case being unsubstituted or substituted by halogen or C.sub.1 -C.sub.4 -alkyl; Q is a radical CO--J, J is a 4-linked 5-hydroxypyrazole ring of the formula II ##STR2## where R .sup.1 is C.sub.1 -C.sub.4 -alkyl and R .sup.2 is hydrogen or methyl, and agriculturally customary salts of the compounds I are described.

    Abstract translation: PCT No.PCT / EP95 / 02974 Sec。 371日期1997年2月3日 102（e）日期1997年2月3日PCT提交1995年7月27日PCT公布。 出版物WO96 / 05197 日期：1992年2月22日 - 式I的羟基吡唑-4-基羰基取代的糖精衍生物其中取代基具有以下含义：L和M是氢，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基， C 1 -C 4 - 烷硫基，氯，氰基，甲基磺酰基，硝基或三氟甲基; Z是氢，C 1 -C 4 - 烷基，C 3 -C 8 - 环烷基，C 3 -C 6 - 烯基，C 3 -C 5 - 炔基，C 1 -C 4 - 酰基，苄基或苯基，每种情况下的苯环是未取代的或被卤素 或C 1 -C 4烷基; Q是基团CO-J，J是式II其中R 1是C 1 -C 4 - 烷基和R 2是氢或甲基的4-连接的5-羟基吡唑环，以及化合物的农业常规盐 我被描述

    Preparation of 1-(het) aryl-3-hydroxypyrazoles
    25.
    发明授权
    Preparation of 1-(het) aryl-3-hydroxypyrazoles 失效
    1-（het）芳基-3-羟基吡唑的制备

    公开(公告)号：US5559244A

    公开(公告)日：1996-09-24

    申请号：US429322

    申请日：1995-04-26

    Applicant: Hartmann Konig ,  Norbert Gotz ,  Reinhard Kirstgen ,  Bernd Muller ,  Klaus Oberdorf

    Inventor： Hartmann Konig ,  Norbert Gotz ,  Reinhard Kirstgen ,  Bernd Muller ,  Klaus Oberdorf

    IPC: C07D231/18 ,  C07D231/22 ,  C07D231/14 ,  C07D231/16 ,  C07D401/04

    CPC classification number: C07D231/22

    Abstract: A process for preparing 1-(het)aryl-3-hydroxypyrazoles of the formula I ##STR1## where R is an unsubst. or subst. aromatic or heteroaromatic radical,n is 0, 1 or 2 andR' is a group which is stable under the reaction conditions, from propiolic acid esters of the formula IIR'--C.tbd.C--CO.sub.2 R.sup.1 IIwhere R.sup.1 is an alkyl, cycloalkyl or aryl group, and (het)arylhydrazines of the formula IIIR--NH--NH.sub.2 IIIin a solvent in the presence of a base, which comprises first mixing II and III with one another in a solvent and then treating this mixture with the base at from 0.degree. C. to 60.degree. C. is described.

    Abstract translation: 制备式I的1-（het）芳基-3-羟基吡唑的方法，其中R是未取代的。 或subst。 芳族或杂芳族基团，n为0,1或2，R'为在反应条件下稳定的基团，其由式II R'-C 3BOND C-CO 2 R II的丙炔酸酯，其中R 1为烷基，环烷基 或芳基，和式III R-NH-NH 2 III（（het））芳基肼在溶剂中在碱的存在下，其包括首先在溶剂中混合II和III，然后用碱处理该混合物 描述于0℃至60℃。

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