Process for the preparation of copper phthylocyanine
    21.
    发明授权
    Process for the preparation of copper phthylocyanine 失效
    铜酞菁的制备方法

    公开(公告)号:US4102892A

    公开(公告)日:1978-07-25

    申请号:US778117

    申请日:1977-03-16

    IPC分类号: C09B47/06

    CPC分类号: C09B47/06

    摘要: The chemical yield and the space-time yield of copper phthalocyanine obtained according to the "baking process" is improved if urea and phthalic anhydride, or its reaction products with ammonia, or the dehydration products thereof, are fed in the liquid form to the reaction vessel.

    摘要翻译: 如果将尿素和邻苯二甲酸酐或其与氨的反应产物或其脱水产物以液体形式进料到反应中,则根据“烘焙过程”获得的铜酞菁的化学产率和时空产率得到改善 船只。

    Process for the preparation of dyestuff formulations
    25.
    发明授权
    Process for the preparation of dyestuff formulations 失效
    染料配方的制备方法

    公开(公告)号:US4295849A

    公开(公告)日:1981-10-20

    申请号:US775898

    申请日:1977-03-09

    CPC分类号: C09B67/0092 D06P5/004

    摘要: The invention relates to the preparation of pulverulent formulations of transfer printing dyestuffs.The process is characterized in that the aqueous dispersions of these dyestuffs are mixed with compounds of the formulaR--ZwhereinR denotes a hydrophobic radical with at least 5 C atoms andZ denotes the groups --COOH, --NH.sub.2, --O(C.sub.2 H.sub.4 O).sub.n H, --NX.sub.1 X.sub.2 or --NH(CH.sub.2).sub.m NX.sub.1 X.sub.2,in whichn is 0, 1 or 2,m is 2-6 andX.sub.1 /X.sub.2 is H or C.sub.1 -C.sub.4 -alkyl,with the proviso that R represents a non-cyclic aliphatic radical when Z represents COOH,and the aqueous mixtures are converted into dry pulverulent form in a manner which is in itself known.The preparation can easily be dispersed in organic media, for example in organic solvents such as those customary in the preparation of printing pastes, and are outstandingly suitable for the preparation of printing inks for printing temporary supports for heat transfer printing.

    摘要翻译: 本发明涉及转印印花染料的粉末制剂的制备。 该方法的特征在于将这些染料的水分散体与式RZ化合物混合,其中R表示具有至少5个C原子的疏水基团,Z表示基团-COOH,-NH 2,-O(C 2 H 4 O)n H, -NX1X2或-NH(CH2)mNX1X2,其中n为0,1或2,m为2-6,X1 / X2为H或C1-C4-烷基,条件是R表示非环状脂族基团 当Z表示COOH时,并且水性混合物以本身已知的方式转化为干粉状。 该制剂可以容易地分散在有机介质中,例如在诸如印刷浆料制备中常用的有机溶剂中,并且非常适用于制备用于印刷传热印刷的临时载体的印刷油墨。

    Process for the preparation of copper phthalolcyanine
    28.
    发明授权
    Process for the preparation of copper phthalolcyanine 失效
    铜酞菁铜的制备工艺

    公开(公告)号:US4118391A

    公开(公告)日:1978-10-03

    申请号:US778154

    申请日:1977-03-16

    CPC分类号: C09B47/06 B01F7/042 B01J19/20

    摘要: The production of copper phthalocyanine in accordance with German Offenlegungsschrift No. 2,432,564 is improved by the process which is characterized in that the reaction product formed at 130.degree.-300.degree. C from optionally substituted phthalic anhydride, reaction products of optionally substituted phthalic anhydride with ammonia, or the dehydration products thereof, urea and, optionally, a catalyst is reacted with a copper salt and, optionally, a catalyst at temperatures of 150.degree.-350.degree. C and preferably 170.degree.-300.degree. C with the proviso that the catalyst is added either during the preparation of the starting material or during the reaction with the copper salt.

    摘要翻译: 根据德国Offenlegungsschrift No.2,432,564的铜酞菁的生产方法得到改进,其特征在于在130-300℃从任选取代的邻苯二甲酸酐,任选取代的邻苯二甲酸酐与氨的反应产物形成的反应产物, 或其脱水产物,脲和任选的催化剂与铜盐和任选的催化剂在150-350℃,优选170-300℃的温度下反应,条件是加入催化剂 在制备原料或在与铜盐反应期间。

    Aqueous pigment dispersions
    30.
    发明授权
    Aqueous pigment dispersions 失效
    水性颜料分散体

    公开(公告)号:US3998652A

    公开(公告)日:1976-12-21

    申请号:US571864

    申请日:1975-04-25

    CPC分类号: C09B67/006 C09B67/0085

    摘要: Aqueous pigment dispersions which contain organic or inorganic pigments and water-soluble oxalkylation products of compounds which are obtainable by condensation of aromatic compounds, containing phenolic OH groups, or their ethers, especially lower alkyl ethers, with formaldehyde and amines which contain at least 2 NH groups which are reactive towards formaldehyde, or derivatives of such oxalkylation products are suitable for pigmenting natural or synthetic materials.

    摘要翻译: 含有有机或无机颜料的水性颜料分散体和化合物的水溶性烷氧基化产物,其可通过含有酚OH基团或其醚,特别是低级烷基醚的芳族化合物与含有至少2个NH的甲醛和胺缩合而获得 对甲醛具有反应性的基团或这些烷氧基化产物的衍生物适于着色天然或合成材料。