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公开(公告)号：US20150007859A1
公开(公告)日：2015-01-08
申请号：US14371782
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
IPC: D01D10/06
Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid solution of pH 5 or lower; and c) rinsing the yarn.
Abstract translation: 本发明涉及从纱线中除去硫的方法，包括以下步骤：a）使未干燥的聚合纱线与碱水溶液接触，所述聚合物包含咪唑基团，所述包含硫原子的聚合物以硫酸根阴离子的形式表征; b）使纱线与pH5或更低的酸性水溶液接触; 和c）冲洗纱线。
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32.发明申请公开(公告)号：US20140325767A1
公开(公告)日：2014-11-06
申请号：US14371447
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
IPC: D06M11/11
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion-containing polymeric-fiber with an halide-containing acid to displace at least a portion of the sulfate ions with halide anions; and b) rinsing the fiber to remove the displaced sulfate ions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）使从未干燥的含硫酸根阴离子的聚合物纤维与含卤化物的酸接触以置换至少一部分 硫酸根离子与卤化物阴离子; 和b）冲洗纤维以除去置换的硫酸根离子。
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公开(公告)号：US08263221B2
公开(公告)日：2012-09-11
申请号：US11390897
申请日：2006-03-27
Applicant: Doetze Jakob Sikkema , David J. Rodini , Qinghong Fu Adkins , Steven R. Allen , Christopher William Newton
Inventor： Doetze Jakob Sikkema , David J. Rodini , Qinghong Fu Adkins , Steven R. Allen , Christopher William Newton
IPC: B32B19/00
CPC classification number: C08J3/097 , C08G73/18 , C08G73/22 , C08J2379/04 , D01F6/74 , Y10T428/29 , Y10T428/2913
Abstract: Disclosed are processes for preparing polyareneazole polymers characterized as providing polymer solutions having an inherent viscosity of at least about 22 dl/g at 30° C. at a polymer concentration of 0.05 g/dl in methane sulfonic acid. Polyareneazoles, filaments and yarns are also disclosed.
Abstract translation: 公开了制备聚are唑聚合物的方法，其特征在于提供聚合物溶液，其聚合物溶液在30℃下在甲烷磺酸中的聚合物浓度为0.05g / dl时具有至少约22dl / g的特性粘度。 还公开了聚芳ne唑，长丝和纱线。
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34.发明授权Processes for preparing high inherent viscosity polyareneazoles using metal powders 失效使用金属粉末制备高特性粘度聚芳唑的方法公开(公告)号：US07671171B2
公开(公告)日：2010-03-02
申请号：US11390849
申请日：2006-03-27
Applicant: Doetze Jakob Sikkema , David J. Rodini , Qinghong Fu Adkins , Steven R. Allen
Inventor： Doetze Jakob Sikkema , David J. Rodini , Qinghong Fu Adkins , Steven R. Allen
IPC: C08G73/00
Abstract: Disclosed are processes for preparing polyareneazole polymers that include contacting, in polyphosphoric acid, azole-forming monomers and metal powder, the metal powder added in an amount of from about 0.05 to about 0.9 weight percent, based on the total weight of the azole-forming monomers, and reacting the azole-forming monomers to form the polyareneazole polymers. Polyareneazoles, filaments and yarns are also disclosed.
Abstract translation: 公开了制备聚are唑聚合物的方法，其包括在多磷酸中形成吡唑形成单体和金属粉末，金属粉末的添加量为基于吡唑形成的总重量的约0.05至约0.9重量％ 单体，并使形成唑的单体反应形成聚芳腈聚合物。 还公开了聚芳ne唑，长丝和纱线。
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公开(公告)号：US5305593A
公开(公告)日：1994-04-26
申请号：US937037
申请日：1992-08-31
Applicant: David J. Rodini , Donald E. Hoffman
Inventor： David J. Rodini , Donald E. Hoffman
CPC classification number: D02G3/441 , D01H1/115 , D02G3/047 , D10B2101/12 , Y10S57/901
Abstract: Spun yarns are made at high speeds of up to 220 meters per minute, using spinning techniques in which air is used to twist the fibers of a three component blend, one component of which consists of staple fibers made from electrically conductive filaments having a denier no greater than 2.5 times the denier of the filaments of the other components.
Abstract translation: 纺丝纱线以高达220米/分钟的高速度制成，使用纺丝技术，其中使用空气来扭曲三组分共混物的纤维，其一种组分由具有旦数的导电丝制成的短纤维 大于其他组分长丝的旦数的2.5倍。
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Patent Agency Ranking
公开(公告)号：US09994974B2
公开(公告)日：2018-06-12
申请号：US14371768
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: D01F6/78 , D01F6/74 , D01F6/805 , Y10T428/249921
Abstract: The present invention concerns fiber made from a polymer comprising imidazole groups, the polymer further having: i) halide anions being present in an amount in the range of 0.05 to 20.1 weight percent, based on weight of fiber; ii) sulfur, wherein the sulfur is present in the fiber in an amount in the range of 0.05 to 3 weight percent, based on weight of fiber; and iii) alkali metal ion, wherein the alkali metal ion is present in the fiber in an amount in the range of 0.05 to 2 weight percent, based on weight of fiber.
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公开(公告)号：US09845553B2
公开(公告)日：2017-12-19
申请号：US14371782
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid solution of pH 5 or lower; and c) rinsing the yarn.
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公开(公告)号：US09469922B2
公开(公告)日：2016-10-18
申请号：US14371744
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from a fiber comprising the steps of: a) contacting never-dried sulfur-containing fiber in a yarn with an aqueous base having a pKa less than or equal to 11 to release at least a portion of said sulfur, said sulfur comprising, at least in part, sulfate anions and said yarn comprising fiber derived from polymer comprising imidazole groups; and b) rinsing said yarn to remove at least a portion of released sulfur.
Abstract translation: 本发明涉及用于从纤维中除去硫的方法，包括以下步骤：a）使纱线中未经干燥的含硫纤维与pKa小于或等于11的碱性水溶液接触，以释放至少部分所述 硫，所述硫至少部分地包含硫酸根阴离子，所述纱线包含衍生自包含咪唑基团的聚合物的纤维; 和b）冲洗所述纱线以除去至少一部分释放的硫。
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公开(公告)号：US09464370B2
公开(公告)日：2016-10-11
申请号：US14371451
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: contacting never-dried sulfate anion-containing polymeric-fiber with an aqueous acid having a pKa of less than 5 to displace at least a portion of the sulfate anions; and b) rinsing the fiber to remove the displaced sulfate ions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：将未干燥的含硫酸盐阴离子的聚合物纤维与pKa小于5的酸性水溶液接触，以至少 部分硫酸根阴离子; 和b）冲洗纤维以除去置换的硫酸根离子。
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40.发明申请公开(公告)号：US20150073118A1
公开(公告)日：2015-03-12
申请号：US14371467
申请日：2012-01-11
Applicant: Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Inventor： Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
CPC classification number: D01F6/805 , D01D10/06 , D10B2331/021
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion containing polymeric-fiber with an aqueous salt solution comprising halide anions to displace at least a portion of the sulfate anions with halide anions; and b) rinsing the fiber to remove displaced sulfate anions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）将含有聚合物纤维的未干燥硫酸根阴离子与含有卤化物阴离子的盐水溶液接触，以使至少一部分 具有卤化物阴离子的硫酸根阴离子; 和b）漂洗纤维以除去置换的硫酸根阴离子。
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