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    Recovery of fluorinated surfactants from a basic anion exchange resin having quaternary ammonium groups
    33.
    发明授权
    Recovery of fluorinated surfactants from a basic anion exchange resin having quaternary ammonium groups 有权
    从具有季铵基团的碱性阴离子交换树脂中回收氟化表面活性剂

    公开(公告)号：US07807726B2

    公开(公告)日：2010-10-05

    申请号：US11373430

    申请日：2006-03-10

    申请人： Andreas Maurer ,  Klaus Hintzer ,  Werner Schwertfeger ,  Egon Obermaier ,  Astrid Weber

    发明人： Andreas Maurer ,  Klaus Hintzer ,  Werner Schwertfeger ,  Egon Obermaier ,  Astrid Weber

    IPC分类号： C08J5/20

    CPC分类号： C08F6/16 ,  B01J41/05 ,  B01J49/57 ,  C02F2001/422 ,  C02F2101/14 ,  C02F2101/301 ,  C02F2103/38 ,  C08L27/12

    摘要： The invention provides a method for recovery of a fluorinated anionic surfactant from a basic anion exchange resin having quaternary ammonium groups, the method comprising eluting the anion exchange resin with a composition comprising an ammonium salt and a water miscible organic solvent. The method according to the invention may provide one or more of the following advantages. For example, the method can be designed to allow for recovery of substantially all of the fluorinated surfactant from a basic anion exchange resin having quaternary ammonium groups. Also, the liquid used for recovering the surfactant from the anion exchange resin is a simple liquid that can be readily and cost effectively manufactured. Further the process may be carried out in a convenient and easy manner. Furthermore, the method generally does not require large amounts of the eluting composition.

    摘要翻译： 本发明提供了从具有季铵基团的碱性阴离子交换树脂中回收氟化阴离子表面活性剂的方法，该方法包括用包含铵盐和水混溶性有机溶剂的组合物洗脱阴离子交换树脂。 根据本发明的方法可以提供一个或多个以下优点。 例如，该方法可被设计成允许从具有季铵基团的碱性阴离子交换树脂中恢复基本上所有的氟化表面活性剂。 此外，用于从阴离子交换树脂中回收表面活性剂的液体是可以容易且成本有效地制造的简单液体。 此外，该方法可以以方便和容易的方式进行。 此外，该方法通常不需要大量的洗脱组合物。

    Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
    34.
    发明授权
    Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant 有权
    使用氟化表面活性剂的氟化单体的水乳液聚合

    公开(公告)号：US07776946B2

    公开(公告)日：2010-08-17

    申请号：US11457502

    申请日：2006-07-14

    申请人： Klaus Hintzer ,  Harald Kaspar ,  Andreas R. Maurer ,  Werner Schwertfeger ,  Tilman Zipplies

    发明人： Klaus Hintzer ,  Harald Kaspar ,  Andreas R. Maurer ,  Werner Schwertfeger ,  Tilman Zipplies

    IPC分类号： C08K5/09

    CPC分类号： C08F14/18 ,  C08F2/22

    摘要： The present invention provides an aqueous emulsion polymerization of fluorinated monomers including gaseous fluorinated monomers using a perfluoro ether surfactant as an emulsifier. The perfluoro ether surfactants correspond to formula (I) Rf—O—CF2CF2—X  (I) wherein Rf represents a linear or branched perfluoroalkyl group having 1, 2, 3 or 4 carbon atoms and X represents a carboxylic acid group or salt thereof. In a further aspect, the invention also provides an aqueous fluoropolymer dispersion comprising the perfluoro ether surfactant and the use of such dispersion in the coating or impregnation of substrates.

    摘要翻译： 本发明提供使用全氟醚表面活性剂作为乳化剂的氟化单体的水乳液聚合，包括气态氟化单体。 全氟醚表面活性剂对应于式（I）Rf-O-CF 2 CF 2 -X（I），其中R f表示具有1,2,3或4个碳原子的直链或支链全氟烷基，X表示羧酸基团或其盐。 另一方面，本发明还提供一种包含全氟醚表面活性剂的含氟聚合物水分散体和在底物的涂布或浸渍中使用这种分散体。

    EXPLOSION TAMING SURFACTANTS FOR THE PRODUCTION OF PERFLUOROPOLYMERS
    36.
    发明申请
    EXPLOSION TAMING SURFACTANTS FOR THE PRODUCTION OF PERFLUOROPOLYMERS 有权
    用于生产全氟聚合物的爆炸性表面活性剂

    公开(公告)号：US20080015319A1

    公开(公告)日：2008-01-17

    申请号：US11457236

    申请日：2006-07-13

    申请人： Klaus Hintzer ,  Michael Jurgens ,  Harald Kaspar ,  Andreas R. Maurer ,  Werner Schwertfeger ,  Tilman C. Zipplies

    发明人： Klaus Hintzer ,  Michael Jurgens ,  Harald Kaspar ,  Andreas R. Maurer ,  Werner Schwertfeger ,  Tilman C. Zipplies

    IPC分类号： C08F16/24

    CPC分类号： C08F14/26 ,  C08F2/22

    摘要： A process comprising polymerizing tetrafluoroethylene in an aqueous emulsion in the presence of a non-telogenic surfactant having an anionic portion with the general formula (I): Rf—O-L-CO2—   (I) wherein Rf is selected from a partially fluorinated alkyl group, a perfluorinated alkyl group, a partially fluorinated alkyl group interrupted by one or more oxygen atoms, and a perfluorinated alkyl group interrupted by one or more oxygen atoms, wherein Rf has from 1 to 10 carbon atoms; and L is an alkylene group having the general formula (CX2)n wherein each X is independently selected from Rf, fluorine, and hydrogen and n is selected from 1 to 5, with the proviso that the surfactant contains at least one unit selected from a —CH2— unit and a —CHF— unit. Also provided are aqueous dispersions comprising these surfactants and methods of coating substrates with the aqueous dispersions.

    摘要翻译： 在具有通式（I）的阴离子部分的非脱落剂表面活性剂的存在下，在水乳液中聚合四氟乙烯的方法：<？在线式描述=“在线式”末端=“铅” （I）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中 R f选自部分氟化的烷基，全氟化烷基，被一个或多个氧原子间隔的部分氟化烷基和被一个或多个氧原子间隔的全氟烷基，其中 R 1具有1至10个碳原子; 并且L是具有通式（CX 2）n N的亚烷基，其中每个X独立地选自R 1，R 2，R 3， 并且n选自1至5，条件是表面活性剂含有至少一个选自-CH 2 - 单元和-CHF-单元的单元。 还提供了包含这些表面活性剂的水分散体和用水分散体涂覆底物的方法。

    RECOVERY OF FLUORINATED CARBOXYLIC ACID FROM ADSORBENT PARTICLES
    38.
    发明申请
    RECOVERY OF FLUORINATED CARBOXYLIC ACID FROM ADSORBENT PARTICLES 审中-公开
    从吸附颗粒中回收氟化的羧酸

    公开(公告)号：US20070025902A1

    公开(公告)日：2007-02-01

    申请号：US11420413

    申请日：2006-05-25

    申请人： Klaus Hintzer ,  Michael Jurgens ,  Harald Kaspar ,  Herbert Koenigsmann ,  Kai Lochhaas ,  Andreas Maurer ,  Werner Schwertfeger ,  Tilman Zipplies ,  George Moore ,  Jay Schulz ,  Richard Flynn

    发明人： Klaus Hintzer ,  Michael Jurgens ,  Harald Kaspar ,  Herbert Koenigsmann ,  Kai Lochhaas ,  Andreas Maurer ,  Werner Schwertfeger ,  Tilman Zipplies ,  George Moore ,  Jay Schulz ,  Richard Flynn

    IPC分类号： B01D53/70

    CPC分类号： C08L27/12 ,  C08L71/02 ,  Y02C20/30 ,  C08L2666/22

    摘要： A process for the recovery of fluorinated carboxylic acid or derivative thereof from adsorbent particles on which fluorinated carboxylic acid or a salt thereof is adsorbed. The process includes contacting the adsorbent particles with a liquid composition capable of removing at least part of the fluorinated carboxylic acid or salt thereof from the adsorbent particles. The fluorinated carboxylic acid or salt thereof is selected from the group consisting of fluorinated carboxylic acids or salts thereof that correspond to the general formula: [RfO-L-COO−]iXi+  (I) wherein L represents a linear partially or fully fluorinated alkylene group or an aliphatic hydrocarbon group, Rf represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one or more oxygen atoms, Xi− represents a cation having the valence i and i is 1, 2 or 3.

    摘要翻译： 从其上吸附氟化羧酸或其盐的吸附剂颗粒中回收氟化羧酸或其衍生物的方法。 该方法包括使吸附剂颗粒与能够从吸附剂颗粒中除去至少部分氟化羧酸或其盐的液体组合物接触。 氟化羧酸或其盐选自对应于以下通式的氟化羧酸或其盐：<？in-line-formula description =“In-line Formulas”end =“lead”→> （I）＆lt;＆lt;＆lt;＆lt; i＆lt; i＆lt; i＆lt; “直链式”末端=“尾”→其中L表示直链部分或完全氟化的亚烷基或脂族烃基，R f表示直链部分或完全氟化的脂肪族基团或 被一个或多个氧原子间断的直链部分或完全氟化的脂肪族基团，X i表示i价和i为1,2或3的阳离子。

    POLYMERIZATION OF HEXAFLUOROPROPYLENE OXIDE
    39.
    发明申请
    POLYMERIZATION OF HEXAFLUOROPROPYLENE OXIDE 审中-公开
    六氟丙烯氧化物的聚合

    公开(公告)号：US20060199942A1

    公开(公告)日：2006-09-07

    申请号：US11276416

    申请日：2006-02-28

    申请人： Werner Schwertfeger ,  Klaus Hintzer ,  Egon Obermaier

    发明人： Werner Schwertfeger ,  Klaus Hintzer ,  Egon Obermaier

    IPC分类号： C08G65/22

    CPC分类号： C08G65/226

    摘要： The present invention provides a process for oligomerization of hexafluoropropylene oxide, the process comprising polymerizing a mixture of hexafluoropropylene oxide and hexafluoropropene in the presence of an aprotic organic solvent using KF as a catalyst.

    摘要翻译： 本发明提供六氟环氧丙烷低聚方法，该方法包括在非质子有机溶剂的存在下使用KF作为催化剂聚合六氟环氧丙烷和六氟丙烯的混合物。

    Removal of fluorinated surfactants from waste water
    40.
    发明授权
    Removal of fluorinated surfactants from waste water 有权
    从废水中除去氟化表面活性剂

    公开(公告)号：US07018541B2

    公开(公告)日：2006-03-28

    申请号：US11034188

    申请日：2005-01-12

    申请人： Klaus Hintzer ,  Egon Obermaier ,  Werner Schwertfeger

    发明人： Klaus Hintzer ,  Egon Obermaier ,  Werner Schwertfeger

    IPC分类号： B01D15/04 ,  C02F1/28

    CPC分类号： C02F1/583 ,  C02F1/281 ,  C02F2101/301 ,  C02F2101/36 ,  C02F2103/38 ,  Y10S210/91 ,  Y10S210/915

    摘要： The present invention provides a method of removing a fluorinated surfactant from waste water comprising fluoropolymer particles. The method comprises (i) adding a non-fluorinated surfactant to the waste water (ii) contacting the thus obtained waste water with adsorbent particles to adsorb at least a portion of the fluorinated surfactant to the adsorbent particles and (iii) separating the waste water and the adsorbent particles.

    摘要翻译： 本发明提供从含氟聚合物颗粒的废水中除去氟化表面活性剂的方法。 该方法包括：（i）向废水中加入非氟化表面活性剂（ⅱ）使得到的废水与吸附剂颗粒接触，将至少一部分氟化表面活性剂吸附到吸附剂颗粒上，和（iii）将废水 和吸附剂颗粒。