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公开(公告)号：US20160010917A1
公开(公告)日：2016-01-14
申请号：US14700993
申请日：2015-04-30
IPC分类号： F25J3/02
CPC分类号： F25J3/0214 , F25J3/0209 , F25J3/0233 , F25J3/0266 , F25J3/0295 , F25J2200/02 , F25J2200/30 , F25J2200/50 , F25J2200/74 , F25J2205/04 , F25J2205/20 , F25J2210/62 , F25J2235/60 , F25J2245/02 , F25J2280/10 , F25J2280/40 , F25J2290/40 , F25J2290/62 , Y02C10/12
摘要： A method and system for separating fluids in a distillation tower. The method may include feeding a stream to the distillation tower, wherein the stream includes carbon dioxide, reducing a carbon dioxide concentration of the stream received by the rectifier section by feeding a first cryogenic fluid to the controlled freeze zone section and accumulating rectifier section stream in at least one of a holding vessel and a sump of the rectifier section, and terminating reducing the carbon dioxide concentration when the carbon dioxide concentration of the stream travelling from the controlled freeze zone section to the rectifier section is less than or equal to a maximum carbon dioxide concentration. The first cryogenic fluid may comprise a substantially carbon-dioxide-free fluid.
摘要翻译： 用于分离蒸馏塔中的流体的方法和系统。 该方法可以包括将物流送入蒸馏塔，其中物流包括二氧化碳，通过将第一低温流体送入控制的冻结区段并将整流器部分流聚集在一起，从而减少由整流部分接收的物流的二氧化碳浓度 整流器部分的保持容器和贮槽中的至少一个，并且当从控制的冻结区段传播到整流器部分的流的二氧化碳浓度小于或等于最大碳时，终止减少二氧化碳浓度 二氧化碳浓度。 第一低温流体可以包含基本上不含二氧化碳的流体。
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32.发明申请公开(公告)号：US20150159946A1
公开(公告)日：2015-06-11
申请号：US14516718
申请日：2014-10-17
申请人： Jaime A. Valencia
发明人： Jaime A. Valencia
CPC分类号： F25J3/0233 , B01D3/4211 , C07C7/05 , C10L3/101 , C10L3/104 , C10L3/106 , C10L3/107 , C10L2290/543 , C10L2290/58 , F25J1/0022 , F25J1/0027 , F25J3/0209 , F25J3/0266 , F25J3/0295 , F25J3/061 , F25J3/0635 , F25J3/08 , F25J2200/02 , F25J2200/30 , F25J2200/50 , F25J2200/74 , F25J2205/04 , F25J2205/20 , F25J2210/04 , F25J2210/80 , F25J2220/66 , F25J2235/60 , F25J2245/02 , F25J2280/10 , F25J2280/40 , F25J2290/12 , F25J2290/40 , Y02C10/12
摘要： The present disclosure provides a method for separating a feed stream in a distillation tower. The method includes operating a controlled freeze zone section in a distillation tower that separates a feed stream at a temperature and pressure at which the feed stream forms a solid in the controlled freeze zone section, wherein the feed stream includes a first contaminant; maintaining a melt tray assembly in the controlled freeze zone section; introducing the feed stream to the controlled freeze zone section; and accumulating a liquid in the melt tray assembly until the liquid is at a predetermined liquid level in the controlled freeze zone section, by: feeding a second contaminant to the controlled freeze zone section; and adding the second contaminant to the melt tray assembly, wherein the liquid comprises the second contaminant.
摘要翻译： 本公开提供了分离蒸馏塔中的进料流的方法。 该方法包括在蒸馏塔中操作控制的冷冻区段，其在进料流在受控冷冻区段中形成固体的温度和压力下分离进料流，其中进料流包括第一污染物; 将熔体托盘组件保持在受控冷冻区段中; 将进料流引入受控冷冻区段; 并且在所述熔体塔盘组件中积聚液体直到所述液体处于所述受控冷冻区段中的预定液位，通过：将第二污染物供给到所述受控冷冻区段; 以及将所述第二污染物添加到所述熔体塔盘组件，其中所述液体包括所述第二污染物。
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33.发明申请公开(公告)号：US20150159939A1
公开(公告)日：2015-06-11
申请号：US14516686
申请日：2014-10-17
申请人： Jaime A. Valencia
发明人： Jaime A. Valencia
IPC分类号： F25J1/00
CPC分类号： F25J3/0266 , B01D3/324 , C07C7/05 , C10L3/101 , C10L2290/543 , C10L2290/545 , C10L2290/58 , F25J1/0022 , F25J1/0027 , F25J3/0209 , F25J3/0233 , F25J3/061 , F25J3/0635 , F25J3/067 , F25J3/08 , F25J2200/02 , F25J2200/30 , F25J2200/50 , F25J2200/74 , F25J2200/90 , F25J2205/04 , F25J2205/20 , F25J2220/66 , F25J2235/60 , F25J2280/40 , F25J2290/12 , F25J2290/40 , Y02C10/12
摘要： The present disclosure provides a distillation tower that may include a stripper section constructed and arranged to separate a feed stream at a temperature and pressure at which the feed stream forms no solid; a controlled freeze zone section constructed and arranged to separate the feed stream at a temperature and pressure at which the feed stream forms a solid; a melt tray assembly in the controlled freeze zone section that includes a liquid; an underflow weir in the controlled freeze zone section that alters a flow of the liquid in the melt tray assembly; an overflow weir in the controlled freeze zone section that works with the underflow weir to alter the flow of the liquid in the melt tray assembly and is adjacent to the underflow weir; and a covering element in the controlled freeze zone section that is connected to and extends from the underflow weir.
摘要翻译： 本公开提供了一种蒸馏塔，其可以包括构造和布置成在进料流不形成固体的温度和压力下分离进料流的汽提段; 构造和布置成在进料流形成固体的温度和压力下分离进料流的受控冷冻区段; 包括液体的受控冷冻区段中的熔体塔盘组件; 在控制的冻结区段中的下溢堰改变熔体塔盘组件中的液体流; 在控制的冻结区段中的溢流堰，其与下溢堰一起工作，以改变熔体塔板组件中的液体的流动，并且与下溢堰相邻; 以及受控冻结区段中的覆盖元件，其连接并从下溢堰延伸。
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34.发明授权Method and apparatus for cryogenic separation of carbon dioxide and other acid gases from methane 失效从甲烷中低温分离二氧化碳和其他酸性气体的方法和装置
公开(公告)号：US4923493A
公开(公告)日：1990-05-08
申请号：US234366
申请日：1988-08-19
IPC分类号： F25J3/02
CPC分类号： F25J3/0233 , F25J3/0209 , F25J3/0266 , F25J2200/02 , F25J2200/74 , F25J2205/20 , F25J2220/66 , F25J2280/40 , Y02C10/12 , Y10S62/929
摘要： A method for conditioning the freezing zone liquid feedstream in the cryogenic separation of carbon dioxide and other acid gases from methane by use of distillation and a controlled freezing zone, including the step of sub-cooling the freezing zone liquid feedstream, so that this freezing zone liquid feedstream remains close to, but not quite at, carbon dioxide solidification conditions.
摘要翻译： 一种通过使用蒸馏和控制的冷冻区域在二氧化碳和其它酸性气体从甲烷的低温分离中调节冷冻区液体进料流的方法，包括冷却冷冻区液体进料流的步骤，使得该冷冻区 液态进料流保持接近二氧化碳凝固条件，但不完全相当。
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35.发明授权Method of separating acid gases, particularly carbon dioxide, from methane by the addition of a light gas such as helium 失效通过添加轻质气体如氦将酸性气体，特别是二氧化碳与甲烷分离的方法
公开(公告)号：US4511382A
公开(公告)日：1985-04-16
申请号：US532343
申请日：1983-09-15
CPC分类号： F25J3/029 , C07C7/05 , F25J3/0209 , F25J3/0233 , F25J3/0266 , F25J2200/02 , F25J2200/74 , F25J2210/04 , F25J2245/02 , F25J2280/02 , Y02C10/12 , Y02P20/152 , Y10S62/929
摘要： A method of separating acid gases, particularly carbon dioxide, from methane by cryogenic distillation. The method includes the step of adding helium to the stream to be separated to increase the critical pressure of the methane-carbon dioxide present. The cryogenic distillation tower may then be operated at a higher pressure and without the formation of solid carbon dioxide.
摘要翻译： 通过低温蒸馏从甲烷中分离酸性气体，特别是二氧化碳的方法。 该方法包括将氦添加到待分离的物流以增加存在的甲烷 - 二氧化碳的临界压力的步骤。 然后可以在更高压力下操作低温蒸馏塔，而不形成固体二氧化碳。
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