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31.发明授权Process for augmenting or enhancing the aroma of perfumed articles by adding thereto triconjugated dienones 失效通过向其中加入三环酮二烯酮来增强或增强香料制品香气的方法
公开(公告)号：US4504398A
公开(公告)日：1985-03-12
申请号：US551482
申请日：1983-11-14
IPC分类号： C07C45/67 , C07C49/203 , C11B9/00 , C11D3/50 , D06M13/20
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C07C67/297 , C11B9/0015 , C11B9/0061
摘要： Described is a process for augmenting or enhancing the aroma of a perfumed article which is a solid or liquid anionic, cationic, nonionic or zwitterionic detergent or a fabric softener composition or a dryer-added fabric softener article comprising the step of adding to said perfumed article at least one compound having a structure selected from the group consisting of: ##STR1##
摘要翻译： 描述了一种用于增强或增强作为固体或液体阴离子，阳离子，非离子或两性离子洗涤剂或织物柔软剂组合物或干衣剂添加的织物柔软剂制品的香料的香气的方法，其包括将所述香料 至少一种具有选自以下的结构的化合物：（i）和（iii）（ii）
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公开(公告)号：US4107197A
公开(公告)日：1978-08-15
申请号：US783495
申请日：1977-03-31
IPC分类号： C07C45/63 , C07C45/70 , C07C49/175 , C07C49/813 , C07C327/22 , C11B9/00 , C07C153/09
CPC分类号： C07C327/00 , C07C323/00 , C07C45/63 , C07C45/70 , C11B9/0011 , C11B9/0015
摘要： Described are .alpha.-oxy(oxo) sulfides and ethers having the generic structure: ##STR1## wherein X is one of: ##STR2## Z is one of sulfur or oxygen; when R.sub.1 and R.sub.2 are taken separately, R.sub.1 is hydrogen or methyl, and R.sub.2 is methyl; and when R.sub.1 and R.sub.2 are taken together, R.sub.1 and R.sub.2 form phenyl moieties; and Y is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, acetyl, methoxycarbonylmethyl, or 1,3-diethylacetonyl.Addition of one or more .alpha.-oxy(oxo) sulfides and ethers to foodstuff flavorings or foodstuffs is indicated to produce the following aroma and flavor characteristics, in the alternative or taken together:AromaGreen/spicey, Sweet, Fruity, Fresh/fruity, Gooseberry, Concord grape, Grape, Almond, Nutty, Cereal-like, Lachrymatory onion-like, Oniony, Green onion-like, Leek, Broccoli-like, Grapefruit, Celery stalk-like, Floral, Rosey, Woody, Blackcurrant, Buchu leaf oil-like, Citronellal-like, Neroli-like, Bergamot-like, Violet leaves-like, Jasmin-like, Melony, Cucumber-like, Green, Vegetable, Sweet/floral.FlavorSpicey, Sweet, Fruity, Milk caramel-like (dulce de leche-like), Gooseberry, Broccoli-like, Nutty, Cereal-like, Oniony, Grape, Concord grape, Citrusy, Grapefruit-like, Green fruit-like, Mandarin-like, Petitgrain-like, Blackcurrant, Minty, Astringent, Coriander-like, Green, Piney, Citronellal-like, Violet leaves-like, Melony, Green fruit-like, Cucumber, Green, Floral, Floral/green, Vegetable, Garlic.With lasting mouthfeel and with, in many cases, an oniony aftertaste. The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of berry flavors, cereal-like flavors, nut flavors, broccoli flavors, onion flavors, citrus flavors (including neroli, bergamot, lime), jasmin flavors, grapefruit flavors, concord grape flavors, blackcurrant flavors, milk caramel flavors (e.g., dulce de leche-like flavors), vegetable flavors, cucumber flavors, celery flavors and spice flavors.Addition of a number of these .alpha.-oxy(oxo)sulfides and ethers -- in perfumes, colognes or perfumed articles imparts thereto sweet, green, floral, herbal, vegetative, basil-like, minty, melony, grapefruit, fruity and alliaceous aromas with yara, neroli and/or verdima-like nuances.
摘要翻译： 描述了具有以下通用结构的α-氧代（氧代）硫化物和醚：其中X是以下之一：Z是硫或氧之一; 当R1和R2分开取代时，R1是氢或甲基，R2是甲基; 当R 1和R 2一起时，R 1和R 2形成苯基部分; Y是C 1 -C 4烷基，C 3或C 4链烯基，乙酰基，甲氧羰基甲基或1,3-二乙基丙酰基之一。
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公开(公告)号：US4094824A
公开(公告)日：1978-06-13
申请号：US819961
申请日：1977-07-28
CPC分类号： C11B9/0011 , C07C323/00 , C07C327/00
摘要： Perfume and fragrance compositions and perfumed articles including soaps, detergents, powders as well as colognes containing .alpha.-oxy(oxo) sulfides having the structure: ##STR1## wherein R is methyl or hydrogen; X is one of ##STR2## and Y is one of methyl, methallyl (having the structure: ##STR3## 1-propyl, 2-methyl-1-propyl and acetyl which impart thereto sweet, green, floral, herbal, vegetative, basil-like, minty, melony, grapefruit, fruity and alliaceous aromas with yara, neroli and/or verdima-like nuances.
摘要翻译： 香料和香料组合物和包含肥皂，洗涤剂，粉末以及含有具有以下结构的α-氧代（氧代）硫化物）的古龙香水制品：其中R是甲基或氢; X是
之一，Y是甲基，甲代烯丙基（具有以下结构：具有以下结构：赋予甜，绿，花，草药，营养，罗勒的1-丙基，2-甲基-1-丙基和乙酰基 类似，微小，融合，葡萄柚，水果和亚麻香气与雅加，橙花和/或verdima的细微差别。 -
公开(公告)号：US4070308A
公开(公告)日：1978-01-24
申请号：US723529
申请日：1976-09-15
IPC分类号： C11B9/00
CPC分类号： C11B9/0011 , C07C323/00
摘要： Perfume and fragrance compositions and perfumed articles including soaps, detergents, powders as well as colognes containing .alpha.-oxy(oxo)mercaptans having the structure: ##STR1## wherein R is any of ethyl, 1-propyl, 2-propyl or 1-butyl; and X is one of: ##STR2## which imparts thereto grapefruit-like, green fruity, concord grape and buchu-leaf oil-like aromas.
摘要翻译： 香料和香料组合物和香料制品，包括肥皂，洗涤剂，粉末以及含有具有以下结构的α-氧代（氧代）硫醇的古龙水：其中R是乙基，1-丙基，2-丙基或1-丁基 ; X是以下之一：
或 ，赋予葡萄柚样，绿色水果，和谐葡萄和buchu-leaf油样香气。 -
35.发明授权Foodstuff flavor compositions comprising 3-furyl alkyl sulfides and processes 失效包含3-呋喃基烷基硫化物的食品风味组合物和方法
公开(公告)号：US4031256A
公开(公告)日：1977-06-21
申请号：US723531
申请日：1976-09-15
IPC分类号： A23L27/20 , C07D307/64 , A23L1/231
CPC分类号： C07D307/64 , A23L27/2052
摘要： 3-Furyl alkyl sulfides having the formula: ##STR1## wherein R.sub.1 is C.sub.1 -C.sub.5 lower alkyl and R.sub.2 is selected from the group consisting of hydrogen and methyl, are described as being useful in altering, modifying or enhancing the organoleptic properties of foodstuffs.
摘要翻译： 具有下式的3-呋喃基烷基硫化物：其中R1是C1-C5低级烷基，R2选自氢和甲基，被描述为可用于改变，改进或增强食品的感官特性。
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36.发明授权Synthesis of triconjugated dienones and novel intermediates used in said process 失效三氯联二烯酮的合成和所述方法中使用的新型中间体
公开(公告)号：US4560802A
公开(公告)日：1985-12-24
申请号：US620086
申请日：1984-06-13
IPC分类号： C07C45/67 , C07C49/203 , C11B9/00 , C11D3/50 , C07C45/65
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C07C67/297 , C11B9/0015 , C11B9/0061
摘要： Described is a process for preparing triconjugated dienones defined according to the structure: ##STR1## wherein R.sub.1 represents C.sub.1 -C.sub.8 alkyl, phenyl or phenyl methyl and wherein R.sub.2 represents hydrogen or C.sub.1 -C.sub.5 lower alkyl; and wherein the wavy lines are indicative of a "cis" or a "trans" juxtaposition of the R.sub.2, methyl, acyl or vinyl moieties about one or both of the carbon-carbon double bonds which process involves the reaction of an acyl halide having the structure: ##STR2## (wherein X represents chloro) with a substituted or unsubstituted prenyl ester having the structure: ##STR3## wherein R.sub.3 represents C.sub.1 -C.sub.5 alkyl in the presence of an aluminum chloride catalyst and a methylene dichloride solvent in order to form the novel intermediate genus defined according to the structure: ##STR4## then dehydrohalogenating the compound defined according to the structure: ##STR5## using an alkali metal carbonate and a dimethylformamide solvent in order to form the novel compound genus having the structure: ##STR6## wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; and then dehydrocyloxylating the compound having the structure: ##STR7## in order to form the compound having the structure: ##STR8## the dehydroacyloxylation step taking place in the presence of an alkali metal carbonate and dimethylformamide solvent.
摘要翻译： 描述了根据以下结构定义的三结合双酮的方法：其中R 1表示C 1 -C 8烷基，苯基或苯基甲基，并且其中R 2表示氢或C 1 -C 5低级烷基; 并且其中波浪线表示R2，甲基，酰基或乙烯基部分在一个或两个碳 - 碳双键上的“顺式”或“反式”并置，该方法涉及具有 结构：其中X表示氯，具有以下结构的取代或未取代的异戊二烯基酯：其中R 3表示C 1 -C 5烷基，在氯化铝催化剂和二氯甲烷溶剂的存在下，形成 根据以下结构定义的新型中间体：然后使用碱金属碳酸盐和二甲基甲酰胺溶剂将根据结构定义的化合物脱卤化氢，以形成具有以下结构的新颖化合物：其中 虚线中的一条代表碳 - 碳双键，另一条虚线表示碳 - 碳单键; 然后脱氢甲基化具有以下结构的化合物：
以形成具有以下结构的化合物：在碱金属碳酸盐和二甲基甲酰胺溶剂的存在下进行脱氢甲酰化步骤。 -
公开(公告)号：US4119788A
公开(公告)日：1978-10-10
申请号：US783487
申请日：1977-03-31
IPC分类号： C07C45/63 , C07C45/70 , C07C49/175 , C07C49/813 , C07C327/22 , C11B9/00 , C07C149/20
CPC分类号： C07C327/00 , C07C323/00 , C07C45/63 , C07C45/70 , C11B9/0011 , C11B9/0015
摘要： Described are .alpha.-oxy(oxo) sulfides and ethers having the generic structure: ##STR1## wherein X is one of: ##STR2## Z is one of sulfur or oxygen; when R.sub.1 and R.sub.2 are taken separately, R.sub.1 is hydrogen or methyl, and R.sub.2 is methyl; and when R.sub.1 and R.sub.2 are taken together, R.sub.1 and R.sub.2 form phenyl moeities; and Y is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, acetyl, methoxycarbonylmethyl, or 1,3-diethylacetonyl.Addition of one or more .alpha.-oxy(oxo) sulfides and ethers to foodstuff flavorings or foodstuffs is indicated to produce the following aroma and flavor characteristics, in the alternative or taken together:AromaGreen/spicey, Sweet, Fruity, Fresh/fruity, Gooseberry, Concord grape, Grape, Almond, Nutty, Cereal-like, Lachrymatory onion-like, Oniony, Green onion-like, Leek, Broccoli-like, Grapefruit, Celery stalk-like, Floral, Rosey, Woody, Blackcurrant, Buchu leaf oil-like, Citronellal-like, Neroli-like, Bergamot-like, Violet leaves-like, Jasmin-like, Melony, Cucumber-like, Green, Vegetable, Sweet/floral.FlavorSpicey, Sweet, Fruity, Milk caramel-like (dulce de leche-like), Gooseberry, Broccoli-like, Nutty, Cereal-like, Oniony, Grape, Concord grape, Citrusy, Grapefruit-like, Green fruit-like, Mandarin-like, Petitgrain-like, Blackcurrant, Minty, Astringent, Coriander-like, Green, Piney, Citronellal-like, Violet leaves-like, Melony, Green fruit-like, Cucumber, Green, Floral, Floral/green, Vegetable, Garlic.with lasting mouthfeel and with, in many cases, an oniony aftertaste. The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of berry flavors, cereal-like flavors, nut flavors, broccoli flavors, onion flavors, citrus flavors (including neroli, bergamot, lime), jasmin flavors, grapefruit flavors, concord grape flavors, blackcurrant flavors, milk caramel flavors (e.g., dulce de leche-like flavors), vegetable flavors, cucumber flavors, celery flavors and spice flavors.Addition of a number of these .alpha.-oxy(oxo) sulfides and ethers in perfumes, colognes or perfumed articles imparts thereto sweet, green, floral, herbal, vegetative, basil-like, minty, melony, grapefruit, fruity and alliaceous aromas with yara, neroli and/or verdima-like nuances.
摘要翻译： 描述了具有以下通用结构的α-氧代（氧代）硫化物和醚：其中X是以下之一：Z是硫或氧之一; 当R1和R2分开取代时，R1是氢或甲基，R2是甲基; 当R 1和R 2一起时，R 1和R 2形成苯基; Y是C 1 -C 4烷基，C 3或C 4链烯基，乙酰基，甲氧羰基甲基或1,3-二乙基丙酰基之一。
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38.发明授权
公开(公告)号：US4097396A
公开(公告)日：1978-06-27
申请号：US819986
申请日：1977-07-28
CPC分类号： C11B9/0011 , C07C323/00 , C07C327/00
摘要： Perfumed articles which are soaps or detergents containing alpha oxo sulfides having the structure: ##STR1## wherein R is methyl or hydrogen and X is a ketone having the structure: ##STR2## and Y is one of methyl, methallyl having the structure: ##STR3## 1-propyl, 2-methyl-1-propyl and acetyl which have imparted thereto sweet, green, floral, herbal, vegetative, basil-like, minty, melony, grapefruit, fruity and alliaceous aromas with yara, neroli and/or verdima-like nuances.
摘要翻译： 具有以下结构的肥皂或洗涤剂的含有α-氧代硫化物的香料制品：其中R是甲基或氢，X是具有以下结构的酮：Y和Y是具有以下结构的甲基，甲代烯丙基之一：
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公开(公告)号：US4088697A
公开(公告)日：1978-05-09
申请号：US783486
申请日：1977-03-31
IPC分类号： C07C45/63 , C07C45/70 , C07C49/175 , C07C49/813 , C07C327/22 , C11B9/00 , C07C149/18
CPC分类号： C07C327/00 , C07C323/00 , C07C45/63 , C07C45/70 , C11B9/0011 , C11B9/0015
摘要： Described are .alpha.-oxy(oxo) sulfides and ethers having the generic structure: ##STR1## wherein X is one of: ##STR2## Z is one of sulfur or oxygen; when R.sub.1 and R.sub.2 are taken separately, R.sub.1 is hydrogen or methyl, and R.sub.2 is methyl; and when R.sub.1 and R.sub.2 are taken together, R.sub.1 and R.sub.2 form phenyl moieties; and Y is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, acetyl, methoxycarbonylmethyl, or 1,3-diethylacetonyl.Addition of one or more .alpha.-oxy(oxo) sulfides and ethers to foodstuff flavorings or foodstuffs is indicated to produce the following aroma and flavor characteristics, in the alternative or taken together:Aroma: Green/spicey, Sweet, Fruity, Fresh/fruity, Gooseberry, Concord grape, Grape, Almond, Nutty, Cereal-like, Lachrymatory onion-like, Oniony, Green onion-like, Leek, Broccoli-like, Grapefruit, Celery stalk-like, Floral, Rosey, Woody, Blackcurrant, Buchu leaf oil-like, Citronellal-like, Neroli-like, Bergamot-like, Violet leaves-like, Jasmin-like, Melony, Cucumber-like, Green, Vegetable, Sweet/floral.Flavor: Spicey, Sweet, Fruity, Milk caramel-like (dulce de leche-like), Gooseberry, Broccoli-like, Nutty, Cereal-like, Oniony, Grape, Concord grape, Citrusy, Grapefruit-like, Green fruit-like, Mandarin-like, Petitgrain-like, Blackcurrent, Minty, Astringent, Coriander-like, Green, Piney, Citronellal-like, Violet leaves-like, Melony, Green fruit-like, Cucumber, Green, Floral, Floral/green, Vegetable, Garlic.With lasting mouthfeel and with, in many cases, an oniony aftertaste. The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of berry flavors, cereal-like flavors, nut flavors, broccoli flavors, onion flavors, citrus flavors (including neroli, bergamot, lime), jasmin flavors, grapefruit flavors, concord grape flavors, blackcurrant flavors, milk caramel flavors (e.g., dulce de leche-like flavors), vegetable flavors, cucumber flavors, celery flavors and spice flavors.Addition of a number of these .alpha.-oxy(oxo)sulfides and ethers in perfumes, colognes or perfumed articles imparts thereto sweet, green, floral, herbal, vegetative, basil-like, minty, melony, grapefruit, fruity and alliaceous aromas with yara, neroli and/or verdima-like nuances.
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公开(公告)号：US4083373A
公开(公告)日：1978-04-11
申请号：US730535
申请日：1976-10-07
CPC分类号： A24B15/36 , A23L27/2022 , A23L27/205 , A24B15/32
摘要： Described is a tobacco product having added thereto an amount sufficient to augment or enhance the flavor or aroma of the tobacco product particularly on smoking, of one or more sulfide compounds having the generic structure: ##STR1## wherein, when A is: ##STR2## B is: ##STR3## AND WHEN A is: ##STR4## B is: ##STR5## processes for producing such tobacco products and flavor formulations for use in conjunction with tobacco products containing one or more of such sulfide compounds.
摘要翻译： 描述了一种烟草制品，其具有足以增加或增强烟草产品的香味或特别是吸烟的量的一种或多种具有以下通用结构的硫化物的量：其中，当A为：
B是： 和A是： B是： 生产这样的烟草制品和风味制剂的方法，其与含有一种或多种这样的硫化物的烟草制品结合使用。
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