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公开(公告)号：US11279800B2
公开(公告)日：2022-03-22
申请号：US14371443
申请日：2012-01-11
Applicant: Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Inventor： Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Abstract: The present invention concerns yarn comprising polymer, the polymer comprising imidazole groups, the yarn having a sulfur content of 0.01 to 3.0 percent by weight, based on weight of the yarn, the yarn having a tenacity of 30 cN/dtex (33.3 gpd) or higher.
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公开(公告)号：US10240282B2
公开(公告)日：2019-03-26
申请号：US14371760
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid comprising a halide; and c) rinsing the yarn.
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公开(公告)号：US09988514B2
公开(公告)日：2018-06-05
申请号：US14371742
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: C08K3/30 , C08K2003/309 , D01D10/06 , D01F6/74 , D01F6/805 , D01F11/08 , Y10T428/249921
Abstract: The present invention concerns fiber made from a polymer comprising imidazole groups, fiber further having: i) a halide anion, the halide anion being present in an amount of 0.05 to 20.1 weight percent, based on weight of fiber; and ii) sulfur, wherein the sulfur is present in the fiber in an amount of 0.05 to 3 weight percent.
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公开(公告)号：US09903051B2
公开(公告)日：2018-02-27
申请号：US13349605
申请日：2012-01-13
Applicant: Steven R. Allen , Christopher William Newton
Inventor： Steven R. Allen , Christopher William Newton
Abstract: The present invention concerns processes for reducing water in never-dried fiber comprising copolymer derived from the copolymerization of para-phenylenediamine, 5(6)-amino-2-(p-aminophenyl)benzimidazole; and terephthaloyl dichloride, the process having the following steps in a continuous process, (a) a step of drying a never-dried fiber at less than 100 C until the moisture content of the fiber is less than 60 weight percent; and (b) a step of further drying the fiber above 150° C. while the moisture content of the fiber is no more than 40 weight percent; and the fiber being further heated to at least 350° C. in either an additional continuous or separate step.
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45.发明授权公开(公告)号：US09464380B2
公开(公告)日：2016-10-11
申请号：US14371447
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion-containing polymeric-fiber with an halide-containing acid to displace at least a portion of the sulfate ions with halide anions; and b) rinsing the fiber to remove the displaced sulfate ions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）使从未干燥的含硫酸根阴离子的聚合物纤维与含卤化物的酸接触以置换至少一部分 硫酸根离子与卤化物阴离子; 和b）冲洗纤维以除去置换的硫酸根离子。
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Patent Agency Ranking
46.发明授权公开(公告)号：US09284665B2
公开(公告)日：2016-03-15
申请号：US14371467
申请日：2012-01-11
Applicant: Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
Inventor： Christopher William Newton , David J. Rodini , Joseph Lenning Lowery , Steven R. Allen , Vlodek Gabara
CPC classification number: D01F6/805 , D01D10/06 , D10B2331/021
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion containing polymeric-fiber with an aqueous salt solution comprising halide anions to displace at least a portion of the sulfate anions with halide anions; and b) rinsing the fiber to remove displaced sulfate anions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）将含有聚合物纤维的未干燥硫酸根阴离子与含有卤化物阴离子的盐水溶液接触，以使至少一部分 具有卤化物阴离子的硫酸根阴离子; 和b）漂洗纤维以除去置换的硫酸根阴离子。
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47.发明申请PROCESS FOR PREPARING YARN DERIVED FROM ARAMID COPOLYMER FIBER HAVING LOW RESIDUAL SULFUR 有权用于制备具有低残留硫磺的芳族共聚物纤维制备纱线的方法公开(公告)号：US20150021812A1
公开(公告)日：2015-01-22
申请号：US14371444
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
CPC classification number: D01F8/16 , D01D5/06 , D01D10/06 , D01F6/74 , D01F6/805 , D01F11/08 , D10B2331/14
Abstract: The present invention concerns processes for producing a yarn comprising polymer comprising imidazole groups, the process having the following steps: (a) spinning a solution of polymer in sulfuric acid to give rise to a plurality of dope filaments; (b) coagulating the plurality of dope filaments into a multi-filament as-spun yarn; and (c) washing the as-spun multi-filament yarn with an aqueous acid comprising a halide or an aqueous salt comprising a halide or combination thereof.
Abstract translation: 本发明涉及生产包含咪唑基团的聚合物的纱线的方法，该方法具有以下步骤：（a）将聚合物溶液在硫酸中纺丝以产生多个涂料丝; （b）将多根纺丝原丝凝结成纺丝纱; 和（c）用包含卤化物或包含卤化物或其组合的盐水的含水酸洗涤初纺复丝纱线。
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公开(公告)号：US20150007859A1
公开(公告)日：2015-01-08
申请号：US14371782
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Christopher William Newton , David J. Rodini , Andrew J. Sitter
IPC: D01D10/06
Abstract: The present invention concerns methods for removing sulfur from yarn comprising the steps of: a) contacting never-dried polymeric yarn with an aqueous base, the polymer comprising imidazole groups and said polymer comprising sulfur atoms characterized as being in the form of sulfate anions; b) contacting the yarn with an aqueous acid solution of pH 5 or lower; and c) rinsing the yarn.
Abstract translation: 本发明涉及从纱线中除去硫的方法，包括以下步骤：a）使未干燥的聚合纱线与碱水溶液接触，所述聚合物包含咪唑基团，所述包含硫原子的聚合物以硫酸根阴离子的形式表征; b）使纱线与pH5或更低的酸性水溶液接触; 和c）冲洗纱线。
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49.发明申请公开(公告)号：US20140325767A1
公开(公告)日：2014-11-06
申请号：US14371447
申请日：2012-01-11
Applicant: Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
Inventor： Steven R. Allen , Vlodek Gabara , Joseph Lenning Lowery , Steven Raymond Lustig , Christopher William Newton , David J. Rodini , Andrew J. Sitter
IPC: D06M11/11
Abstract: The present invention concerns methods for removing sulfur from a fiber made from a polymer comprising imidazole groups, said method comprising: a) contacting never-dried sulfate anion-containing polymeric-fiber with an halide-containing acid to displace at least a portion of the sulfate ions with halide anions; and b) rinsing the fiber to remove the displaced sulfate ions.
Abstract translation: 本发明涉及从由包含咪唑基团的聚合物制成的纤维中除去硫的方法，所述方法包括：a）使从未干燥的含硫酸根阴离子的聚合物纤维与含卤化物的酸接触以置换至少一部分 硫酸根离子与卤化物阴离子; 和b）冲洗纤维以除去置换的硫酸根离子。
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公开(公告)号：US08263221B2
公开(公告)日：2012-09-11
申请号：US11390897
申请日：2006-03-27
Applicant: Doetze Jakob Sikkema , David J. Rodini , Qinghong Fu Adkins , Steven R. Allen , Christopher William Newton
Inventor： Doetze Jakob Sikkema , David J. Rodini , Qinghong Fu Adkins , Steven R. Allen , Christopher William Newton
IPC: B32B19/00
CPC classification number: C08J3/097 , C08G73/18 , C08G73/22 , C08J2379/04 , D01F6/74 , Y10T428/29 , Y10T428/2913
Abstract: Disclosed are processes for preparing polyareneazole polymers characterized as providing polymer solutions having an inherent viscosity of at least about 22 dl/g at 30° C. at a polymer concentration of 0.05 g/dl in methane sulfonic acid. Polyareneazoles, filaments and yarns are also disclosed.
Abstract translation: 公开了制备聚are唑聚合物的方法，其特征在于提供聚合物溶液，其聚合物溶液在30℃下在甲烷磺酸中的聚合物浓度为0.05g / dl时具有至少约22dl / g的特性粘度。 还公开了聚芳ne唑，长丝和纱线。
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