Use of diol alkoxylates as additives for the production of pigment concentrates
    43.
    发明授权
    Use of diol alkoxylates as additives for the production of pigment concentrates 有权
    使用二醇烷氧基化物作为颜料浓缩物生产的添加剂

    公开(公告)号:US06312514B1

    公开(公告)日:2001-11-06

    申请号:US09530840

    申请日:2000-08-31

    IPC分类号: C09D1700

    CPC分类号: C09D17/001 C09B67/006

    摘要: Pigment concentrates comprising a pigment, a liquid carrier medium and a diol alkoxylate of the general formulae (I), (II) and/or (III) are described in conjunction with methods of preparing the same. The diol alkoxylates described and used herein are of the general formulae (I), (II) and/or (III): wherein each of R1, R2, R3, R5, R7 and R8 independently represents a hydrogen atom or an alkyl group having from 1 to about 36 carbon atoms, with the proviso that both R1 and R2 are not simultaneously hydrogen atoms and the total number of carbon atoms in R1 and R2 is from about 6 to about 38, and with the proviso that both R3 and R5 are not simultaneously hydrogen atoms and the total number of carbon atoms in R3 and R5 is from about 6 to about 38, wherein R4 represents a linear or branched alkylene group having from about 2 to about 12 carbon atoms or (—CH2—CHR6—O)z—, wherein R6 represents a hydrogen atom or a methyl group, wherein each of x and y independently represent a number of from about 1 to about 200, z represents a number of from about 1 to about 20, n represents a number of from about 2 to about 12, and wherein the sum of x+y is a number of from about 5 to about 200.

    摘要翻译: 结合其制备方法描述了包含通式(I),(II)和/或(III)的颜料,液体载体介质和二醇烷氧基化物的颜料浓缩物。 本文所述和使用的二醇烷氧基化物具有通式(I),(II)和/或(III):其中R 1,R 2,R 3,R 5,R 7和R 8各自独立地表示氢原子或具有 1至约36个碳原子,条件是R1和R2不同时为氢原子,R1和R2中的碳原子总数为约6至约38,条件是R3和R5均为 不同时氢原子,R3和R5中的碳原子总数为约6至约38,其中R4表示具有约2至约12个碳原子的直链或支链亚烷基或(-CH2-CHR6-O) z-,其中R 6表示氢原子或甲基,其中x和y各自独立地表示约1至约200的数,z表示约1至约20的数,n表示 约2至约12,并且其中x + y的总和为约5至约200的数量。

    Process for the production of ammonium fatty acid hydroxyalkanesulfonates
    46.
    发明授权
    Process for the production of ammonium fatty acid hydroxyalkanesulfonates 失效
    生产铵型脂肪酸羟基烷基磺酸盐的方法

    公开(公告)号:US5473089A

    公开(公告)日:1995-12-05

    申请号:US227846

    申请日:1994-04-14

    CPC分类号: C07C303/32

    摘要: Ammonium fatty acid hydroxyalkanesulfonates are made by a process in which (a) ammonium hydroxyalkanesulfonate corresponding to general formula (I):HO--(C.sub.n H.sub.2n)--SO.sub.3 NH.sub.4 (I)wherein n=2 to 4, is subjected to the esterification reaction with a fatty acid corresponding to the formula (II)R--COOH (II)wherein RCO is an aliphatic, linear or branched acyl radical containing 6 to 18 carbon atoms, in the presence of an esterification catalyst, characterized in that (a) before the esterification reaction, the starting compounds corresponding to formulae (I) and (II) are dried at a temperature of 120.degree. C. to 160.degree. C. and under a pressure of 100 to 700 mbar; (b) the esterification reaction is carried out at a temperature above 160.degree. C. to 195.degree. C. and under a pressure of 250 mbar to atmospheric pressure; (c) water of solution and water of reaction formed are directly removed from the reaction mixture; (d) the catalyst is neutralized with a base on completion of the reaction.

    摘要翻译: 脂肪酸羟基烷基磺酸铵通过以下方法制备:(a)对应于通式(I)的羟基链烷磺酸铵:其中n = 2至4的HO-(CnH2n)-SO3NH4(I)与脂肪进行酯化反应 对应于式(II)R-COOH(II)的酸,其中RCO是含有6至18个碳原子的脂族,直链或支链酰基,在酯化催化剂存在下,其特征在于(a)酯化反应 对应于式(I)和(II)的起始化合物在120℃至160℃的温度和100至700毫巴的压力下干燥; (b)酯化反应在160℃至195℃和250毫巴至大气压的压力下进行; (c)直接从反应混合物中除去所形成反应的溶液和水; (d)催化剂在反应完成时用碱中和。